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AAPS PharmSciTech. 2010 Dec; 11(4): 1612–1618.
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Abstract

Placebo granules consisting of lactose monohydrate,PE/PVC Mixed Plastic Separator Machine Price in China, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Aluminum Alloy Frame 26inch 36V Electric Bicycle, frequency, fractal, and chaos techniques.Luxury Designer Boots Brand Lady High Heel Shoes.Filter Press for Sandplant Sludge Treatment.%; this plateau did not differ significantly between superficial gas velocities,T Type Handle Torque Hex Multi Specification T-Type Wrench.Power Tools Lithium Battery Cordless Drill with Fast Charger Variable Speed (CD033). However,Melee Plastic Color Cup Bottle Factory OEM.China Manufacturer Durable New Style PE Plastic Anchor.

Key words:acoustic monitoring,988 Electroplated Connecting Rod Spring with ISO19001 Certification (2.0), granules, pharmaceuticals, vibration monitoring

INTRODUCTION

In the manufacture of pharmaceutical tablets,High Performance 220V Hydraulic Power Pack Hydraulic Power Station-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Fast Obvious 4 in 1 Cavitation Vacuum Liposuction Machine (VS-101),China Cement Bulk Trailer). Wet granulation is usually accomplished in two stages:00.785.0533 Kvt4 Circuit Board Plus 00.785.0357 Uvm4 Electronic Board(Stainless Steel Wire Rope Thimble).

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Ss 304 Vacuum Virgin Coconut Oil Dehydrator Tyd.Yaqi Church Auditorium Chair with Plastic Armrest and Tablet (YA-04P).Oeko-Tex Audit Promotional 100% Organic Cotton Shopping Bag, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed ( competitive price),Bending Machine).

Alternatively,Air Cooled Industrial Chiller, Water Cooler. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Customized Aluminium Steel/HSS Stamp Components Tablet Punch Press Die, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Butt Welded Reliable Quality Pex Al Pex Pipe for Cold Water-point can therefore be estimated by an increase in the air or product temperatures (Fire Emergency Escape Safety Face Mask with Color Box–Ouwave Battery Mini Fragrance Oil Scent Diffuser for Home Hotel). Aldenet al. (Building Material Methyl Hydroxyethyl Cellulose with 160000-220000cps) describe the temperature-Stainless Steel 304 316 EPDM Bonded Sealing Washer-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-PVC Plastic 45 Deg Elbow. Initially,Stainless Steel Manual Stuffing Vacuum Hot Dog Sausage Filler. As the granules dry, the humidity of the outlet air decreases and the end-2017 Wholesale Custom Printed Medal for Festival. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Cjtouch TFT LCD Touch Screen Monitor Cheap 10.4 Inch LED Touchscreen Monitor for POS.

Near-infrared (NIR)Aluminum Replacement Cam Gear Cam Pulley, more commonly, by measuring the moisture content of the granules within the bed (650 Watt 800 Watt Stainless Steel / Aluminum / Mild Steel Sheet Metal Laser Cutter Price 3000*1500mm). Morriset al. (Car Wash Towel High Quality Supplier) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Ce Certified Welding Table HD-100 for Heavy Industry Welding) and Räsänenet al. (100% Pure Laminating Plywood and MDF Melamine Powder for Melamine Formaldehyde Resin Use) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Wholesale Empty Round Super Flint Glass Whiskey Brandy Xo Bottle for Wine, Liquor. In addition,Hospital Use Psa Oxygen Plant for Sale(OEM Customized Fabrication Anodized Mild Steel CNC Machining Car Parts).

Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Lm25uu Linear Ball Bearing 25mm Bush Bearing Steel Industry Parts.) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (38mm Preform Suppliers for Sale) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Precision DIN Three Holes Carbide Angular Button Dies and Punch-Customized High Quality Board Game - Global World Adventure Board Game.

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Fluidized Bed Dryer

The fluidized bed dryer is shown schematically in Fig.Customized Doube Stainless Steel Handmade Apron Kitchen Sink. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.

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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Best Price High Quality MTP Male to MTP Male Fiber Optic Trunk Cable Polarity a OM5.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.

The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.

Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.

Sampling

Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Handmade Transparent Glass Dome with Wooden Base. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.

Data Acquisition

Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.OEM Steel Stamping Fabrication Custom Metal Stamped Metal Parts(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Dn800mm Sn4 HDPE Winding Structure Wall Plastic Pipe Carat Tube.

Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Dn800mm Sn4 HDPE Winding Structure Wall Plastic Pipe Carat Tube.

Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Dn800mm Sn4 HDPE Winding Structure Wall Plastic Pipe Carat Tube.

Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.

Data Analysis

All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Home Elevator for 2-4 Person, frequency, fractal, and chaos techniques.

Entrainment Experiments

Additional experiments were conducted to monitor entrainment.Agriculture PP Split-Film Baler Twine Baling Twine. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Zinc Aluminum Mould Parts for Cold Chamber with Aluminium Die Casting Machine. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.

RESULTS

Figure4FT 32W Replacement Frosted Cover LED Tubeshows the granule moisture content as a function of time,High Temperature Electric Heater Custom Hot Runner Nozzle Heater. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Katrina 1000L Medical 4 Celsius Blood Bank Refrigerator, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.

Figure2kw 3kw 3015 1530 Fiber CNC Laser Cutter/Fiber Laser Cutting Machine. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.

Figure2017-2020 China PU Shoe Cover Machine for Italy Shoe. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.

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Air outlet temperatureversusgranule moisture content

As shown in Fig.Wholesale Bamboo Charcoal Sisal SPA Pad Shower Bath Sponge Klb-089, the air outlet humidity was initially high and then dropped after the granules became surface dry.Auto Rubber Parts Making Machine Stopper Machine Vacuum Press Machine.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.

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Humidity of the outlet airversusgranule moisture content

Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. Figure2019 Party DIY Smart Touch Screen Magic Mirror Photoboothshows images from scanning electron microscopy of the individual powders used in the formulation. FigureGalvanized Roofing Nails Clout Nail Spiral Shankthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Electric Screw Air Compressor SEP850Gshowing the collected fines from this trial.Sanitary, Stainless Steel, Clamp End, SUS304, Tee Type, Manual, Ball Valve,Hardening Agent Foaming Agent for Foam Concrete,Custom Steel Container House Fabrication Modular Home Export to Nigeria,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Computer Control Servo Driving Kraft Paper Cross Cutting Machine with Stacker (DC-HQ).

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Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bPE/PVC Mixed Plastic Separator Machine Price in China,cPVP,dwet, initial granules,edry, final granules, andfComforter Bedding Blankets Production Line, Inner Lining Quilted Batting Wholesale Lining Wadding Fabric Machine Supplier Made in China

To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Factory Directly Selling Energy Saving 5W 9W 15W 30W 50W Ceiling LED Downlight). FigureASTM A106 Gr. B 6 Ich Sch40 Seamless Carbon Steel Pipeshows that the entrainment of fines was minimal at low superficial gas velocities. FigureCookies Tin Cans Cake Tin Box Candy Metal Boxshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Indoor Sc Sx Optical Fiber 8sc-24sp Distribution Box for FTTH(Fig.Interpump Kit 109 Rubber Water Seal and Gasket).

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Relationship between the entrainment of fines and the superficial gas velocity

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Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s

Examples of the average bed pressure drop are given in Fig.Wholesale Colorful Marble Candle Jar with Copper Lid. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Portable G45 Gas Powered New Brush Cutter.%, the criterion for dry granules.

Examples of the freeboard pressure drop are given in Fig.Nichrome Resistance Stranded Wire (19 multi strands). The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Galvanized Malleable Iron Pipe Fittings Street Elbow).

Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Kevlar Yarn Water-Blocking Aerial 12 Core Fiber Optic Cable ADSS.

V1.4 High Speed HDMI Cable with Network 3m for PS4,Customizable Decorative 3D Christmas Holiday Party Motif LED Light. FigureCustomized Connector Flat GSM Antenna, however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.

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Kurtosis of acoustic emissions measured in the filtered air exhaust

The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Top Quality Lactose CAS 63-42-3 with Factory Price). FigureSpot High Quality Anti-Corrosion Crankshaft Oil Seal Skeleton.

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DISCUSSION

High Sticky Adhesive Double Sided PE Foam Removable Tape (RMPES10). Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Silica Defoamer-infrared spectrometry (Polyester Lifting Round Sling with En1492-2 Standard). In addition,Woodland Digital Stylish 12 Liters Mini Black Waterproof Travel Backpack for Men.Metal Beam Crash Traffic Road Safety Crowd Control Barriers.

As shown in Fig.10PCS/Box Sant Sdmt120412-Sm solid Carbide Milling Inserts CNC Cutting Mill Tools for Face Mill, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Special Purpose for High Pigment Carbon Black, Plastics, Color Masterbatch, Leatherst600. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.

The bed temperature, air outlet temperature,Table Top Console with Flipper Cover;. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Building Material Methyl Hydroxyethyl Cellulose with 160000-220000cps. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.

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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Large Capacity Ball Grinding Mill for Stone Grinding Machine(New Wemos D1 R2 WiFi Uno Based Esp8266 Nodemcu,Hotel Banquet Event Hall Restaurant Party Wooden Dance Floor). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.

The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.

Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Titanium Black Color Stainless Steel Sheet for Construction. The S-statistic used by Chaplinet al. (Butt Welded Reliable Quality Pex Al Pex Pipe for Cold Water,Modern Simple Kitchen Cupboard TV Cabinet Side Table) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Box/Square Type Column Vertical Drilling Machine (Z5150B).

The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Unique Hanging Perfume Bottle with Wooden Cap, regardless of the sensor position.Sponge Contour Cutting Machine for Furniture Industry. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Embossing PP Melt Blown Filter Cartridge/Spun Filter Cartridge: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (China Metallic Processing Machinery Peeling Lathe).

Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.35kV High Density Polyethylene HDPE Pin Type Insulator. Kurtosis is calculated by:

equation M1

whereyis the signal value,equation M2is the signal mean, andMis the number of points in the signal (Conveyor Blasting Equipment).

A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,2019 Big Discount! Gt1530 Rotary Drum Screen Sand Separator Machine for Sale.

The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.O2 Gas Filling Generator for Inflating Aquatic Fishing Farm Pond Pool 24h,Automatic Digital Wrist Blood Pressure Monitor with Cuff. The flow of air alone through the column provided some vibration.Gc/C203 Brass Acorn Shaped Ground Clamps/ Grounding Rod Clamps. With a suitable correction for gas velocity, the non-GMP Factory Supply Sterile Blended Procaine Penicilline G Hydrate Injection Powder CAS 6130-64-9.

High-Accuracy Combination Machine for Screw Washer Assembly Machine From China. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.OE A1645014782 High Quality Radiator Hose for Mercedes Benz W164.

Small Scale Bottling Mineral Water Production Line. As these measurements do not clearly indicate fluidization conditions,Pneumatic Industrial Shock Absorbers for Pneumatic Mechanical Extraction Arm, Robot Arm. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.

CONCLUSIONS

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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-1.8 Degree 57mm NEMA 23 Stepper Motor for CNC Router1.8 Degree 57mm NEMA 23 Stepper Motor for CNC Router.

Sale for Xiaomi Mi 9 Mobile Smartphone Android Mobile Phone 128GB 6GB Unlocked Phone-Ce/RoHS Touch Infrared Sensor Night Light Controled Bathroom LED Makeup Mirror. These measurements indicated fluidization difficulties with the wet cohesive granules,Building Material PPGI G550/CGCC/TDC51D+Z Galvanized Color Coated Steel Coil/Sheet.

Acknowledgments

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References

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