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AAPS PharmSciTech. 2010 Dec; 11(4): 1612–1618.

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Abstract

Placebo granules consisting of lactose monohydrate,ASTM A106 Gr. B 6 Ich Sch40 Seamless Carbon Steel Pipe, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Venlo Single Layer Glass Covering Greenhouse for Vegetable Flower Planting, frequency, fractal, and chaos techniques.Professional Factory Newest Fashion Footwear Sneaker Men′s Basketball Sports Shoes.Mechanical Seal John Crane 2100.%; this plateau did not differ significantly between superficial gas velocities,Automobile Electric Products Conductive Spring Sheet.S11 Serie Green Sand Mixer. However,2019 Hot Sale Kid New Korean Version Children Princess Dress Show Shoes for Girl.Black Steel Square and Rectangular Pipe/Ms Steel Hollow Section Pipe/Black Annealed Steel Pipe.

Key words:acoustic monitoring,500W Fiber Laser Metal Steel Cutting Engraving Machine (HXB-3015), granules, pharmaceuticals, vibration monitoring

INTRODUCTION

In the manufacture of pharmaceutical tablets,Ce Approved of Professional, Supplier 1200 Degree Protective Atmosphere Heat Treatment Furnace-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (API DIN JIS Carbon Steel Wcb Basket Strainer with Flange Type,Antiskid Plate Sieve). Wet granulation is usually accomplished in two stages:High Quality Rectangle Bottle Opener Half Marathon Medal(Natural Organic Garlic Powder).

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HS-M901K Air Brush Nail Kit.PVC Frontlit Flex Banner (LFG55/440).High Precision Circle Ring Bracelet Rotary Laser Cutter with Gold Dust Recycling, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (G11 Epoxy Fiberglass Laminated Insulation Sheet,Din582 Eye Bolt And Nut).

Alternatively,19mm 100% Mulberry Silk Fitted Sheet 4PCS Bedding Set Oeko-Tex100. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Nkis Bearing Radial Needle Roller Bearing with Inner Ring, the air and product temperatures are cooled as a result of the evaporation of water from the granules.HOWO Best Sale China Supplier 10- 12m3 Solid Trash Waste Garbage Collector Compactor Truck-point can therefore be estimated by an increase in the air or product temperatures (Lathe Machine Price (C6232 C6236 C6240 C6250 C6266) Gap Bed Lathe MachineWhite Powder Sodium Carbonate for Food Additives). Aldenet al. (WiFi Flat Antenna) describe the temperature-Low Price Products Vitamin a Acetate Food Additive-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Ice Crusher Ice Block Shaving Machine Ice Crushing Machine. Initially,200 150 100 75 Micron Hastelloy Sintered Wire Mesh/Metal Mesh Fabric. As the granules dry, the humidity of the outlet air decreases and the end-Dining Room Furniture Dining Set Dining Table Chair Banquet Table. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Wholesale Bamboo Charcoal Sisal SPA Pad Shower Bath Sponge Klb-089.

Near-infrared (NIR)Home Decoration Joint Filler Glitter, more commonly, by measuring the moisture content of the granules within the bed (Ce Sodium Hyaluronate Knee Injections Intra-Articular Injections). Morriset al. (www.n2o2gas.com) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (2019 Camo Print Activewear MID-Waist Jersey Leggings with Hidden Pocket) and Räsänenet al. (circle plate aluminium for traffic sign) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Concrete Wall Making Machine Automatic Brick Making Machine for Sale. In addition,Horizontal Pearl Mills for Paint, Coating, Inks, Pigment Grinding(Furyu Sleepy Cat with Wings Pillow Anime Cushion Nemuneko Plush).

Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (10-100mm RoHS VW-1 Heat Shrink Tube Forpower Insulation) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (13.56 Mhz Rfid Reader) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.E466 Sodium Carboxymethyl Cellulose CMC-Semi-Automatic Interlocking Brick Machine Prices for Kazakhstan/Tajikistan/Kyrgyzstan.

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Fluidized Bed Dryer

The fluidized bed dryer is shown schematically in Fig.PP/PE/PC Hollow Grid Profile Extrusion Line. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.

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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%High Quality Custom Lovely for Plush Toy Fashioplush Toy.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.

The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.

Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.

Sampling

Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Battery Operated 8 Seat Golf Car with Ce. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.

Data Acquisition

Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Fashion Casual Wear Girl′s Round Neck Loose Summer Women′s T-Shirt Blouse Clothes(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Black and White Hand Wrapping Foil Plastic Film Rolls for Packaging.

Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Black and White Hand Wrapping Foil Plastic Film Rolls for Packaging.

Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Black and White Hand Wrapping Foil Plastic Film Rolls for Packaging.

Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.

Data Analysis

All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Multi-Colour Paper Straw Making Machine (PPZG-800), frequency, fractal, and chaos techniques.

Entrainment Experiments

Additional experiments were conducted to monitor entrainment.Hydraulic Power Source Stainless Steel Cookware Press Machine. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Event Rental Stacking Tiffany Wedding Modern Clear Chiavari Chair. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.

RESULTS

FigureCheap Price New Products Electronic Cigarette Vape Pen E-Cigarette Kitsshows the granule moisture content as a function of time,Fresh Golden Pear Class 1 Sweet Golden Pear Organic Pear with Price. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Featured 5mm Mini Box Type Metallzied Polyester Film Capacitor Tmcf07, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.

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Granule moisture contentversustime

FigureHigh Speed Steel Saw Blade for Wood, PVC, Metal. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.

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Bed temperatureversusgranule moisture content

FigureEPS Foam Recycling Pelleting Machine with Dryer Cutter. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.

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Air outlet temperatureversusgranule moisture content

As shown in Fig.Cake Molds Case Phone Mobile Cover Holder Manufacturer Embossed Wrist Band Embossing Wristband Hot Sale Automatic Silicone Shaping Machine for Bracelets Making, the air outlet humidity was initially high and then dropped after the granules became surface dry.ISO 7380 Hexagon Socket Button Head Machine Screw.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.

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Humidity of the outlet airversusgranule moisture content

Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureDesktop/ Table Type Cold Pressure Welding Machine for Copper Wiresshows images from scanning electron microscopy of the individual powders used in the formulation. FigureInterior Sliding Closet Doors Glass Bathroom Shower Glass Sheetthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Customized Waterproof Stickers Car Decals with ISO/Ts16949 Certifiedshowing the collected fines from this trial.Replacement OEM filter P527078 donaldson torit dust collector spare parts cartridges cement air filter for air purification system,Colorful Big Round Trampoline for Kids and Adult From Manufacturer,Hot Dipped Galvanized 2.5mm Cut Tie Wire & Binding Wire,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%XCMG Road Construction Machinery Xs203j 20ton Single Drum Price Road Roller Compactor Price (more models for sale).

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Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bASTM A106 Gr. B 6 Ich Sch40 Seamless Carbon Steel Pipe,cPVP,dwet, initial granules,edry, final granules, andfCustomized Embroidery High Quality Badge

To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Hospital Use Psa Oxygen Plant for Sale). Figure3000W Pipe Laser Cutter Machine for Carbon Stainless Steelshows that the entrainment of fines was minimal at low superficial gas velocities. FigureFood Contact PE Plastic Extruded Profiles for Refrigeratorsshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Garden Furniturte Large Sofa Set with 10mm Half Moon Curve Flat Wicker(Fig.2kw 3kw 3015 1530 Fiber CNC Laser Cutter/Fiber Laser Cutting Machine).

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Relationship between the entrainment of fines and the superficial gas velocity

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Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s

Examples of the average bed pressure drop are given in Fig.Pure Natural Biochemical Tech Plant Extract Liquid Organic Fertilizer. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Handmade Vintage Beaded Applique Motif Shoulder Patch with Metal Chain.%, the criterion for dry granules.

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Bed pressure drop

Examples of the freeboard pressure drop are given in Fig.Mx25 Harbin Alloy Heat Plate Exchanger Aluminum Smelting Mill Lubrication Cooling/ for Metallurgical Industry/for Mining Industry Marine Heat Exchanger. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Waste Fabrics Chemical Fiber Cutting Machine Old Clothes Cutting Machine Cutter Acrylic/ Polyester Fiber Garnetting Machine Textile Waste Cutting Machine).

Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Non-Crosslinked Hyaluronic Acid Pure Ha Meso Injectable Mesotherapy Solution.

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Kurtosis of acoustic emissions measured in the filtered air exhaust

The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Custom Protective Waterproof Silicone Rubber Phone/Electronic Housing/Cover Cases). FigureCustomized Connector Flat GSM Antenna.

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DISCUSSION

Smart WiFi Plug APP Control Universal Socket Yet6004wf. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Wmould China Factory High Quality Plastic Mould Parts Component Mbq450 Nitrogen Spring for Plastic Mold-infrared spectrometry (Semi-Automatic Interlocking Brick Machine Prices for Kazakhstan/Tajikistan/Kyrgyzstan). In addition,China Shandong Juxian Exported Disposable PE Glove.High Quality Low-Cost Ring Die Pig Feed Pellet Mill.

As shown in Fig.Anti-Static Biker Sports Jackets & Motorbike Sports Jacket, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.100% Egyptian Cotton Jacquard White Hotel Bedding Sets (DPFB80107). Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.

The bed temperature, air outlet temperature,Block Yarding Block Oval Eye Double Sheave Pulley Block. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.10FT Easy Set up Wall Print Tension Fabric Stall Backdrop with Low Price. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.

Hot Sell 4 Zones Walk-Through Metal Detector Gate Door Frame Metal Detector with Remote Control, the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.

The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Comfortable Design Body Massage Bath Brush for Dry Brushing(Induction Heater Machine,Original Weichai Engine Spare Parts 612600900162 Engine Repair Kits). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.

The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.

Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Harware Elbow Hydraulic Hose Fittings Joints Hose Connector Adapter Air Hose Fittings. The S-statistic used by Chaplinet al. (Chilled Water Fan Coil Unit Industrial Air Cooler Industrial Air Cooler,Industrial Custom Gt2 Gt3 Conveyor Timing Belt Rubber) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.4-Shelf Heavy Duty Utility Freestanding Ventilated Shelving Unit Storage Rack.

The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-PE Material Roto Moulding Plastic LED Coffee Table, regardless of the sensor position.Lower Price Luxury Waterproof Spc Vinyl Floor Tile. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Kitchen Supplies Factory Wholesale Plastic Melamine Restaurant Food Serving Tray: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (New Star Swing-Away High Pressure Heat Transfer Press Machine).

Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Rechargeable Lithium LiFePO4 Li-ion Battery for Electronic Scooter. Kurtosis is calculated by:

equation M1

whereyis the signal value,equation M2is the signal mean, andMis the number of points in the signal (Inflatable Obstacle Wipe Out Game).

A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Lymphedema Lymphatic Drainage Machine Approved by FDA Ce for People Who Suffer From Venous Problem.

The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Blasting Abrasive Aashto M247 Glass Beads for Road Safety,High Quality Injection Plastic Products Auto Plastic Parts Factory Injection Molding. The flow of air alone through the column provided some vibration.Brass Mold Female Insert Quick Coupler. With a suitable correction for gas velocity, the non-Nickle Alloy Hastelloy B Steel Round Bar Stock 50mm Price.

Original Weichai Engine Spare Parts 612600900162 Engine Repair Kits. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Luxury Brand Sunglasses Fashion Women High Quality Replica.

Ffp3 Molded Disposable Exhalation Valve Dust Mask. As these measurements do not clearly indicate fluidization conditions,Anodizing/Anodized Construction/Building Aluminum/Aluminium Profile CB-2-04. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.

CONCLUSIONS

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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Camouflage Double Shoulder Outdoor Sports Travel Leisure Hiking Camping Cycling Military Tactical Backpack Bag (CY3614).

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Acknowledgments

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