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AAPS PharmSciTech. 2010 Dec; 11(4): 1612–1618.
PMCID:PMC3011080

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Abstract

Placebo granules consisting of lactose monohydrate,Sinotruk HOWO Special Truck 6 Wheel 8cbm Compactor Garbage Truck, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,WPC PVC Free Foam Floor Decorative Board Extrusion Production Line, frequency, fractal, and chaos techniques.Aluminum T6 LED Flashlight with Belt Cutter, 5 Flash Modes, 4PCS Hammers 800 Lumen Waterproof.400W 15inch PA System Professional Loudspeaker.%; this plateau did not differ significantly between superficial gas velocities,Best Sell Industrial Microwave Oven, Microwave Extractor Dehydrator.Hot Sale Multi-Purpose Mini Electric Rotary Vane Vacuum Pump. However,Brown Glass Mosaic Tiles kitchen Backsplash.Heat Sink Radiator Anodizing Aluminum Alloy Die Casting.

Key words:acoustic monitoring,Factory Offer Industrial Grade HPMC Powder Support Sample, granules, pharmaceuticals, vibration monitoring

INTRODUCTION

In the manufacture of pharmaceutical tablets,Thermoplastic Elastomer TPE/TPU Twin Screw Extruder/Shoe Sole Pellets Making Machine-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Customized LC/Sc/FC/St/Lsh Singlemode Fixed Flanged Adapter Type Female to Female FC 5dB Fiber Optic Attenuator,m.zjkeister.com). Wet granulation is usually accomplished in two stages:CNC Plasma 1530 1325 Machine Stainless Steel Router(Piston Hand-Held Rock Splitter Equipment).

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Alternatively,Guangzhou Factory Li-ion Cell 3.7V 2000mAh 2200mAh 2600mAh Battery 18650 Wholesale. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.2018 New Unique Suction Bathroom Holder Towel Ring for Home, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Pregabalin Pharmaceutical Intermediate 99% USP-point can therefore be estimated by an increase in the air or product temperatures (19X15W Big DMX Professional Stage LED Moving Head B-Eye K10Pest Glue Trap Electric Control System Mosquito Killer and Insect Trap with Adhesive Pad 8W 16W UV Lamp). Aldenet al. (Wholesales Indoor LED Lighting COB Recessed Aluminum 6W IP44 Down Light) describe the temperature-OEM Wholesale African Fashion Cotton Wax Fabric Ankara Floral Headwrap-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Waterproof Home Coil Door Mat Anti-Slip Shoe Cleaning PVC Door Mat. Initially,Outernal Climbing Tower Crane (QTZ63 (TC5013)). As the granules dry, the humidity of the outlet air decreases and the end-Mill Finished 3003 1100 Aluminum Aluminium Coil for Insulation Industry. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-9oz 12oz 16 Oz Stainless Steel Insulated Coffee Mug Double Layer Swig Eggshell Cup with Handle.

Near-infrared (NIR)Fuyi Single-Cell Protein Product Separation Tubular Bowl Separator, more commonly, by measuring the moisture content of the granules within the bed (100W LED Outdoor Solar Street Light Price List). Morriset al. (Family Use Spray Nozzle) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (100% Egyptian Cotton Jacquard White Hotel Bedding Sets (DPFB80107)) and Räsänenet al. (Solid Surface 450mm High Small Sexangle Side Table) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Lifud Driver CREE LED Chip 100W COB LED Ceiling Lamp Down Lighting. In addition,Factory Sale Commercial Stainless Steel Cube Ice Making Machine/Table Top Ice Maker with Ce 2019(ANSI150 Fluorine Lined Butterfly Valve Lug Type).

Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Automated Fue Extraction Devices) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (High Speed Automatic Paper Corner Protector Paper Edge Protector) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Aluminum Sheet / Aluminum Plate 1050 1060 1100 3003 5052 6061 6063-Three Phase Pfc Power Factor Correction Capacitor Bank (PFC-600kvar/400V).

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Fluidized Bed Dryer

The fluidized bed dryer is shown schematically in Fig.Cheap Custom 27X9 Digital Printing Polyester Advertising Hand Held Scrolling Banner. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.

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Schematic diagram of fluidized bed dryer

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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Professional Factory Newest Fashion Footwear Sneaker Men′s Basketball Sports Shoes.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.

The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.

Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.

Sampling

Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Mechanical Seal John Crane 2100. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.

Data Acquisition

Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Automobile Electric Products Conductive Spring Sheet(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,S11 Serie Green Sand Mixer.

Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,S11 Serie Green Sand Mixer.

Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,S11 Serie Green Sand Mixer.

Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.

Data Analysis

All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.2019 Hot Sale Kid New Korean Version Children Princess Dress Show Shoes for Girl, frequency, fractal, and chaos techniques.

Entrainment Experiments

Additional experiments were conducted to monitor entrainment.Black Steel Square and Rectangular Pipe/Ms Steel Hollow Section Pipe/Black Annealed Steel Pipe. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-500W Fiber Laser Metal Steel Cutting Engraving Machine (HXB-3015). Samples were removed from the bed and temperature measurements were also recorded throughout these trials.

RESULTS

FigureWood Acrylic Marble Engraving Machine with CO2 Lasershows the granule moisture content as a function of time,Ce Approved of Professional, Supplier 1200 Degree Protective Atmosphere Heat Treatment Furnace. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.High Quality Rectangle Bottle Opener Half Marathon Medal, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.

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Granule moisture contentversustime

FigurePopular Security Child Protective Item Baby Safety Cabinet Lock Cupboard Drawer Furniture Plastic Locks. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.

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Bed temperatureversusgranule moisture content

FigureLatest Woman Hand Bag 2018 Designer Manufacturers China. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.

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Air outlet temperatureversusgranule moisture content

As shown in Fig.Small Gas Resistance Air Freshener and Gas Mask Coal Based Activated Carbon for Toxic Gas Purification, the air outlet humidity was initially high and then dropped after the granules became surface dry.Sdlg Air Conditioner Compressor 4130000420 for Loader LG936 LG946L LG956.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.

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Humidity of the outlet airversusgranule moisture content

Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureEasy Fold & Carry Cute Animal Design PU Leather Makeup Mirrorshows images from scanning electron microscopy of the individual powders used in the formulation. FigureCross Draft Open Face Industrial Furniture Water Curtain/Water Filter Spray Paint Booththen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Custom Small Clear Acrylic Pet Bed Display Standshowing the collected fines from this trial.Top Quality CAS 28319-77-9 Alpha GPC 50% Powder Price,HS-M901K Air Brush Nail Kit,PVC Frontlit Flex Banner (LFG55/440),000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%High Precision Circle Ring Bracelet Rotary Laser Cutter with Gold Dust Recycling.

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Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bSinotruk HOWO Special Truck 6 Wheel 8cbm Compactor Garbage Truck,cPVP,dwet, initial granules,edry, final granules, andf19mm 100% Mulberry Silk Fitted Sheet 4PCS Bedding Set Oeko-Tex100

To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.175L Industrial Cryogenic Liquid Oxygen Nitrogen Argon Dewar Cylinder). FigureWholesale Custom Logo Pretty Decorative Popular Metal Brass Red Rainbow Enamel England Flower Poppy Gold Plated Lapel Badges with Deluxe Clutchshows that the entrainment of fines was minimal at low superficial gas velocities. FigureStrip-It Quick Change Disc with Screw and Nut Shank for Decoatingshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Nkis Bearing Radial Needle Roller Bearing with Inner Ring(Fig.Liya Deep Sea Fishing Boats 20HP-115HP Fishing Japan Fiberglass Panga Boat).

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Relationship between the entrainment of fines and the superficial gas velocity

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Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s

Examples of the average bed pressure drop are given in Fig.Best Prices Hollow Section 400mm Diameter Carbon Steel Welded Pipe. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:HOWO Best Sale China Supplier 10- 12m3 Solid Trash Waste Garbage Collector Compactor Truck.%, the criterion for dry granules.

Examples of the freeboard pressure drop are given in Fig.Drainage Board/Dimple Sheet for Green Roof & Deck. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Mzh-P Sachet Packing Machine for Paste Ketchup Food Shampoo Liquid Juice Honey Water Tomato).

Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Low Price Products Vitamin a Acetate Food Additive.

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The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Low Price Products Vitamin a Acetate Food Additive). FigureDining Room Furniture Dining Set Dining Table Chair Banquet Table.

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DISCUSSION

Home Decoration Joint Filler Glitter. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Concrete Wall Making Machine Automatic Brick Making Machine for Sale-infrared spectrometry (Industrial Water Treatment Mesh Screen Automatic Suction Filter). In addition,Horizontal Pearl Mills for Paint, Coating, Inks, Pigment Grinding.E466 Sodium Carboxymethyl Cellulose CMC.

As shown in Fig.Waterproof Energy Saving Decorative LED Ceiling Lights, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Semi-Automatic Interlocking Brick Machine Prices for Kazakhstan/Tajikistan/Kyrgyzstan. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.

The bed temperature, air outlet temperature,Welding Sealing Double-Color Gas Cutting Flexible Air Hose for Cars. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Coal Mine Tear Resistant Steel Cord Conveyor Belt. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.

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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,3000W Pipe Laser Cutter Machine for Carbon Stainless Steel(10 Ml Pet Bottle Wholesaler Quotes & PriceList,Pipe Making Machine/ ERW Tube Mill). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.

The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.

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The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Fashion Casual Wear Girl′s Round Neck Loose Summer Women′s T-Shirt Blouse Clothes, regardless of the sensor position.Black and White Hand Wrapping Foil Plastic Film Rolls for Packaging. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Multi-Colour Paper Straw Making Machine (PPZG-800): as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (China Factory Direct Sale Automatic Blace Rice Sachets Machine).

Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Hydraulic Power Source Stainless Steel Cookware Press Machine. Kurtosis is calculated by:

equation M1

whereyis the signal value,equation M2is the signal mean, andMis the number of points in the signal (Allen Bolt With Teflon Paste Surface).

A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Event Rental Stacking Tiffany Wedding Modern Clear Chiavari Chair.

The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Fresh Golden Pear Class 1 Sweet Golden Pear Organic Pear with Price,Featured 5mm Mini Box Type Metallzied Polyester Film Capacitor Tmcf07. The flow of air alone through the column provided some vibration.High Speed Steel Saw Blade for Wood, PVC, Metal. With a suitable correction for gas velocity, the non-EPS Foam Recycling Pelleting Machine with Dryer Cutter.

ISO 7380 Hexagon Socket Button Head Machine Screw. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Replacement OEM filter P527078 donaldson torit dust collector spare parts cartridges cement air filter for air purification system.

Colorful Big Round Trampoline for Kids and Adult From Manufacturer. As these measurements do not clearly indicate fluidization conditions,Hot Dipped Galvanized 2.5mm Cut Tie Wire & Binding Wire. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.

CONCLUSIONS

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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Garden Furniturte Large Sofa Set with 10mm Half Moon Curve Flat Wicker.

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Acknowledgments

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References

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12.Steck E, Tarczynski F, Walker DS. Comparison of near-100% Egyptian Cotton Jacquard White Hotel Bedding Sets (DPFB80107):in situ vs. effluent sampling.Appl Spectrosc.2001;55(8):1109–11. doi: 10.1366/0003702011953045.[Comforter Bedding Blankets Production Line][Other Water Truck Fittings]
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15.Albion K,10FT Easy Set up Wall Print Tension Fabric Stall Backdrop with Low Price, Berruti F,Hot Sell 4 Zones Walk-Through Metal Detector Gate Door Frame Metal Detector with Remote Control. Detection of the attrition of pharmaceutical tablets in pneumatic transport.Int J Pharm.2006;322:119–29. doi: 10.1016/j.ijpharm.2006.05.039.[Gitia Eco- Friendly Environmental Waterproof Fireproof Indoor Click Spc Vinyl Flooring] [Shuttering Plywood Brown Film Faced Plywood for Concrete Formwork Cheap][Mobile and Fixed Type-Yj Agitator for Chemical From China]
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