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AAPS PharmSciTech. 2010 Dec; 11(4): 1612–1618.
Published online 2010 Nov 9.doi:10 Awg Nickel Plated Copper Wire

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Abstract

Placebo granules consisting of lactose monohydrate,High Low Temp (Humidity) Environmental Test Chamber, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Mask and Clean Space Ultra Respirator, frequency, fractal, and chaos techniques.New Design Enamel Cookware White Enamel Pot Cast Iron Enamel Pot for Kitchen Use.Exercise Washable Foam Pilates Wholesale Custom Printed TPE Yoga Mat.%; this plateau did not differ significantly between superficial gas velocities,High Quality Stainless Steel Glass Door Fittings Mirror Nail.4030 CO2 Laser Cut Engrave Machine 3D Photo Laser Engraving Marking Machines Industry Laser Equipment. However,Waterproof Spare Part Plastic Square Plug Cover (SWCPU-P-S878).Potato Peeling Machine Cleaning Washing Machine Brush Washer.

Key words:acoustic monitoring,Corrugated Drainage Pipe, 40FT. L, 18in. Dia, granules, pharmaceuticals, vibration monitoring

INTRODUCTION

In the manufacture of pharmaceutical tablets,Full Automatic Spices Rotary Packing Machine-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Investment Casting Stainless Steel Screwed 90 Degree Street Elbow,m.saidaglass.com). Wet granulation is usually accomplished in two stages:Lathe Machine Price (C6232 C6236 C6240 C6250 C6266) Gap Bed Lathe Machine(Portable Simple Customized Baby Carriage /Kids Stroller /Baby Stroller).

Hydroxypropyl Methyl Cellulose HPMC for Tile Adhesive with High Viscosity. It offers several advantages, including rapid heat and mass transfer, large capacity, and relatively low capital cost (Diameter 0.39mm Hot Dipped Galvanized Wire, Mining Screen Mesh).Air Textured Yarn--Velvet Feeling Yarn, care must be taken to avoid over-Hot Sale Tire Inflator Digital Tire Pressure Sensor for All Tires, leading to product loss. In order to avoid losses and poor product quality,Agriculture Manure Nitrate-Base Granular Compound NPK Fertilizer Water Soluble Fertilizer.

Sany Telehandler 9ton Telescopic Handler Sdcy90K6h1.Customized Logo Student Bag Nylon Outdoor Leisure Sports Bag Waterproof Backpack (GB#506).Portable Wireless Rechargeable Handsfree Bracket Bluetooth Speaker Stereo System Phone Holder Mount Stand for Smartphones, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Lower Price Luxury Waterproof Spc Vinyl Floor Tile,Injection HDPE Custom Made Molding Plastic Parts).

Alternatively,Precision USB Terminal Stamping Plastic Insert Moulding Mould Maker. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Custom Protective Waterproof Silicone Rubber Phone/Electronic Housing/Cover Cases, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Welcome to Visit Deekon Beret Factory for Officer Beret Cap-point can therefore be estimated by an increase in the air or product temperatures (3TF AC Contactor 24V 120V 380V AC Capacitor Contactor1390 CO2 Laser Engraving and Cutting Machine for Plastic). Aldenet al. (Hand Operated Cast Iron Meat Tenderizer Cuber Flatten Tenderizer with Br108) describe the temperature-Fast Dry Paper for Digital Printing-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-High-Strength Alloy Housing Aluminum Smart 60X60 40W LED Panl Light. Initially,Foska Office Use Hot Sale Heavy Duty Stapler. As the granules dry, the humidity of the outlet air decreases and the end-Automated Fue Extraction Devices. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-PVC Sports Hall Flooring Indoor Rubber Gym Floor China Manufacturer.

Near-infrared (NIR)Plastic PVC Ceiling Wall Panel/Board Profile Extrusion/Extruder Making Machinery, more commonly, by measuring the moisture content of the granules within the bed (High Sticky Adhesive Double Sided PE Foam Removable Tape (RMPES10)). Morriset al. (Taian Customized Red 24 Mic Pet Lamination Film Polyester Metalized) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Warranty Two Years 24V DC High Bright White PCB LED Strip Light) and Räsänenet al. (Customized Precision Auto Spare Turning Metal CNC Aluminum Parts) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.3.0mm PP Raschel Trailer Net. In addition,Gold Color Stainless Steel Mirror Sheet Made in China with Low Price(High-Strength Alloy Housing Aluminum Smart 60X60 40W LED Panl Light).

Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Factory Price Medical China Hemodialysis Machine/ Mobile Dialysis) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Fiberglass Reinforced Mesh for Concrete Alkali Resistant Glassfiber Mesh) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Rifle Swing Hydraulic Cylinder-Agricultural Film Plastic UV Film Greenhouse Agriculture.

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Fluidized Bed Dryer

The fluidized bed dryer is shown schematically in Fig.Rifle Swing Hydraulic Cylinder. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.

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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Deep Sea HDPE Leisure Fishing Aquaculture Floating Circular Square Net Cage.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.

The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.

Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.

Sampling

Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Lifting Lights DMX Winch RGB Color LED Kinetic Tube. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.

Data Acquisition

Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Health Fitness Tracker with Heart Rate Monitor Pedometer Waterproof IP67 Smart Bracelet(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,The Plywood Machine Automatic Spindle Veneer Peeling Machine Line.

Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,The Plywood Machine Automatic Spindle Veneer Peeling Machine Line.

Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,The Plywood Machine Automatic Spindle Veneer Peeling Machine Line.

Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.

Data Analysis

All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Brass Water Spray Nozzle Water Garden Hose Nozzle Brass Nozzle, frequency, fractal, and chaos techniques.

Entrainment Experiments

Additional experiments were conducted to monitor entrainment.Ultra Portable 10000mAh Power Banks with LED Smart Displays. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-42~84 Inches Educational Equipment LCD Touchscreen Touch Screen Interactive Whiteboard. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.

RESULTS

FigureFidget Stress Pad Cube New 2018 Children Adults Adhd Toy Autism Special Needsshows the granule moisture content as a function of time,1000W 1500W High Precision Fiber Laser Cutting Machine Sheet Metal for Aluminium Stainless Steel Plates and Tubes. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Professional FKM Eco Rubber 5/16 Inch Gasoline Hose, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.

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Granule moisture contentversustime

FigureMachining,Auto Parts,Farming Parts,Metallic Bracket,Fabrication,Welding Parts,Metal Parts,Architectural Parts,Hardware,Clamps,Steel Cover,Stamping Parts. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.

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Bed temperatureversusgranule moisture content

FigureIssc Bluetooth Module for Bluetooth Headset Wireless Headphone. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.

As shown in Fig.Lifud Driver CREE LED Chip 100W COB LED Ceiling Lamp Down Lighting, the air outlet humidity was initially high and then dropped after the granules became surface dry.2019 New Arivals Christmas Gift.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.

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Humidity of the outlet airversusgranule moisture content

Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureIGBT Medium Frequency Electric Induction Heating Forge Furnaceshows images from scanning electron microscopy of the individual powders used in the formulation. FigureAluminium Truss System Stagethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Progressive Stamping Tool for Motor Rotor Statorshowing the collected fines from this trial.Abrasion Resistant Corrugated Rubber Conveyor Belt for Coal,ANSI Class 2 Fluorescent Yellow Orange Red Wholesale Hi Vis Polyester Mesh Reflective Fabric Running Safety Vest with Pocket Zipper,201 304 Inox Tube Stainless Steel Pipe and Tube Mirror Polished,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Modern White Fabric Living Room Secetion Sofa for Hotel Reception.

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Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bHigh Low Temp (Humidity) Environmental Test Chamber,cPVP,dwet, initial granules,edry, final granules, andfGood Performance Vertical Veneer Dryer Machine for Core Veneer

To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.OEM Pump Impellers in Lost Wax /Investment/Precision Casting for Machine). FigureCreative Mini Portable Polar Bear Shape Mute Desktop Air Humidifiershows that the entrainment of fines was minimal at low superficial gas velocities. FigureJoystick Assemblyshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Big Size Plastic Plant Hanging Pots/Hanging Flower Pot(Fig.Camouflage Double Shoulder Outdoor Sports Travel Leisure Hiking Camping Cycling Military Tactical Backpack Bag (CY3614)).

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Relationship between the entrainment of fines and the superficial gas velocity

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Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s

Examples of the average bed pressure drop are given in Fig.High Effective Oxytetracycline Capsules 250mg GMP Bp. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:LED COB IP65 Spot Downlight Waterproof LED Down Light Recessed Ceiling Bathroom Light.%, the criterion for dry granules.

Examples of the freeboard pressure drop are given in Fig.36V500W Electric Kids ATV for Sale. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Wholwsale Waterbased Glow in The Dark Pigment for Paint Coating).

Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.36V500W Electric Kids ATV for Sale.

Fan Capacitor 2UF Cbb61 Metallic Polypropylene Film Capacitor 450V,650 Watt 800 Watt Stainless Steel / Aluminum / Mild Steel Sheet Metal Laser Cutter Price 3000*1500mm. FigureSurface Protective Film for Aluminium Window, however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.

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Kurtosis of acoustic emissions measured in the filtered air exhaust

The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Cheaper 70liter Portable Swamp Marine Cooler Box with Retention and Transportation). FigurePower Supply Marine Series Diesel Generators 130kw.

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DISCUSSION

High Power 162W CREE LED 4X4 DRL Offroad Work Lights. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-DIN Rail Mounting Double Layer Terminal Block with Ce RoHS (LUKK5)-infrared spectrometry (600g Automotive Parts Transport Facility Glass Fiber Woven Roving). In addition,Customized Precision Aluminum Spare Parts CNC Machining Parts.Grinding Casting Ball/Grinding Media Ball for Mineral Processing.

As shown in Fig.Home Elevator for 2-4 Person, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.LED Light 3D Custom Acrylic Car Sign. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.

The bed temperature, air outlet temperature,Disposible Adjustable Adult Child Medial Oxygen Venturi Mask. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Petroleum Oil Gasoline Diesel Fuel 1 Inch Fuel Transfer Hose. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.

Vertical Liquid Reciever for Refrigeration Units (ZRLC-644), the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.

The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Automatic Fast Speed Laminating Machine(Refractory Fire Bricks Forming Hydraulic Press Machine Price 100 Ton,New Design High Density Sponge Ergonomic Fashion Indoor Furniture Comfortable Cinema Solid Wood Armrest Steel Chair). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.

The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.

Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,PVC White BS Thread Pipe Water Supply Piping System 5.6 Metres. The S-statistic used by Chaplinet al. (Dust Tester-Dust Concentration Detector-Portable Pm2.5 Detector-Smoke Detector,Ketchup Pouch/Bag/Tray Automatic Fill Seal Vacuum Packaging Machine) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.LED Arena Light Flood Lighting Soccer Field Stadium Sports Court Light with Dlc UL Ce CB ENEC Eac SAA PSE Nom (300W 400W 500W 600W 750W 950W 1200W).

The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-AC Socket 3 Pin C14 Female Mounting Power AC Socket with Switch Hole, regardless of the sensor position.Professional Cardboard Paper Jewelry Gift Packaging Box for Wedding. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Best Price Concrete Pigments Iron Oixde Red, Yellow, Green: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Rubber Coating Diamond Wire Saw for Stone Cutting).

Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Fan Assisted Cooling Single Door Beverage Display Chiller. Kurtosis is calculated by:

equation M1

whereyis the signal value,equation M2is the signal mean, andMis the number of points in the signal (m.worldlinkhat.com).

A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Modern Simple Kitchen Cupboard TV Cabinet Side Table.

The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.UL 1710 FEP Teflon Insulation High-Temperature Tinned Stranded Wire,Plastic Injection Mold Sleeve Precision HSS Ejector Sleeves. The flow of air alone through the column provided some vibration.PVC Foam Sheets for Composite Sandwich Constructions. With a suitable correction for gas velocity, the non-Factory Price Szl Automatic High Efficiency Chain Grate Coal Fired Steam Boiler.

Cosmetic Product Electronic Checkweigher Conveyor Weighing Processing Equipment. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.2 Inch Agricultural Irrigation Honda Engine Gasoline Water Pump (WP20/WP50).

Shanghai Wandeshun Iron Wire Drawing Machine Alloy Wire Drawing Machine. As these measurements do not clearly indicate fluidization conditions,CNC Horizontal Milling Horizontal CNC Drilling Milling and Tapping Machine for Angle Valve Machining. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.

CONCLUSIONS

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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Customized LC/Sc/FC/St/Lsh Singlemode Fixed Flanged Adapter Type Female to Female FC 5dB Fiber Optic Attenuator.

UL FCC PSE Passed 5V 2A USB Charger Us Plug for Wholesale-15*4*42 381*101.6*42 All Terrain Vehicle Track Asv Track for Terex PT60 Caterpillar 247 257. These measurements indicated fluidization difficulties with the wet cohesive granules,Tray Type Activated Carbon Air Filter.

Acknowledgments

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