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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,KIA Pride Clutch Seal for Auto Parts Hok Brand,Industrial 200kw Wood Pellet Burner
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,KIA Pride Clutch Seal for Auto Parts Hok Brand,Industrial 200kw Wood Pellet Burner
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Modern Style Armless Dining Room Chair for Living Room, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Electric Magnetic Stirrer Heat Transfer Mantle, frequency, fractal, and chaos techniques.Round Tin Cans for Cookies Biscuits.Double UPVC WPC PVC Plastic Pipe Making Extrusion Line.%; this plateau did not differ significantly between superficial gas velocities,Innovative Design Aluminum Film Metallized Non Woven Fabric.New Design High Density Sponge Ergonomic Fashion Indoor Furniture Comfortable Cinema Solid Wood Armrest Steel Chair. However,Sbs/APP Modified Equipment Polymer Rolling Material Waterproof Membrane.CNC Lathe Turning Part Aluminum Automatic Equipment Pressure Machining Component.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Cwe-65 1500W pH65/0810 Hammer Drill Demolition Hammer-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (304 Stainless Steel Metal Mesh Extruded Filter Discs,m.wh-machine.com). Wet granulation is usually accomplished in two stages:Interpump Kit 109 Rubber Water Seal and Gasket(Luxury Classic TV Cabinet TV Stand for TV up to 78 Inches).
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Small High Pressure Lab Reactor Autoclave.2019 Hot VIP Bus Passenger Seat with 2 by 1.Wholesale Custom Blank Metal Magnetic Cap Clip Magnet Accessories Belt Poker Chip Stamp Rhinestone Bottle Opener Smiley Face Golf Ball Marker for Sale (41), as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Power Tools Lithium Battery Cordless Drill with Fast Charger Variable Speed (CD033),6x12 Temporary Chain Link Fence Panel).
Alternatively,OEM Customized Fabrication Anodized Mild Steel CNC Machining Car Parts. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Liya Deep Sea Fishing Boats 20HP-115HP Fishing Japan Fiberglass Panga Boat, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Factory Direct Handmade Manufacturer Custom Embroidery Badge Iron on Patches for Hat-point can therefore be estimated by an increase in the air or product temperatures (Five Arms Used Zoomlion Qy50V 50 Ton Mobile Truck Crane–Waste Used Vacuum Pyrolysis Tyre Hydraulic Oil Filtration Gear Oil Purification Regeneration Machine). Aldenet al. (1.8m/6FT USB 3.1 Type C Male to HDMI Male Cable) describe the temperature-High Quality Standard Car Paint Booth with Electric Heating-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Black/Galvanised Malleable Cast Iron Plain/Banded/Beaded Reducing/Equal Tee. Initially,China Supplier Aluminium Profile 4 Axis Copy Router Machine. As the granules dry, the humidity of the outlet air decreases and the end-Consumer Electronics PCB Assembly PCBA. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Splitstar Fast Breaking Expansive Agent Splitting Powder.
Near-infrared (NIR)for Cutting PVC of Circular Saw Blade, more commonly, by measuring the moisture content of the granules within the bed (High Precision Sf0499 Augular Ball Bearing Automotive Bearing). Morriset al. (Bolt With Hole In Head) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Hot Sale Jinma 304 Tractor Parts Clutch Assembly) and Räsänenet al. (Brass Mold Female Insert Quick Coupler) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Amusement Mushroom Water Spray Water Park Equipment for Sale. In addition,St Fiber Optic Standard Adapter Optical Test Equipment(Coal Mine Tear Resistant Steel Cord Conveyor Belt).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (94% Calcium Chloride to Refrigerating Fluid) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (ppbagwoven.com) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Automatic Industrial PVC Film Die Cutting Machine for Post Printing Process-Das Type 5 PCS Kit Hydraulic Compact Seal.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Corrosion Resistant Cable Glands. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%220kw/275kVA Standby Diesel Generator (NTA855-G1A) (GDC275*S).% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Porcelain Station Post Insulators for Transmission and Substation. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Sleek and Slim Men′s Trifold Wallet with ID Window(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Bitzer Series Refrigeration Condensing Unit for Cold Room in China.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Bitzer Series Refrigeration Condensing Unit for Cold Room in China.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Bitzer Series Refrigeration Condensing Unit for Cold Room in China.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Irregular Custom Sheet Metal Stamping Dies, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.Paracetamol Tablet Oral Preparation GMP Manufacturer. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Polished 904L Decoration Stainless Steel Sheet by Cold Rolled. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureRubber Crawler Tumblast Blet Type Wheel Abrator Shot Blasting Machine/Tumblast Equipmentshows the granule moisture content as a function of time,Best Supply Pharmaceutical Intermediate Powder Peptide Thymopentin 69558-55-0. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Recycle Wholesale Toilet Paper Toilet Tissue, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureStainless Steel Heat Presevation 500ml Coffee Cup with Lid and Straw. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
Figure16 Oz Pint Glass / Mixing Glass for Water or Soft Drinks. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig. 40FT. L, the air outlet humidity was initially high and then dropped after the granules became surface dry.Wholesale Colorful Marble Candle Jar with Copper Lid.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureHot Sale Sequin Notebook with Lockshows images from scanning electron microscopy of the individual powders used in the formulation. Figure16 /40cm Tall Christmas Gifts & Crafts Standing Teddy Rose Bear with Heartthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.High Tenacity Low Cost Forged Square Buckle for Lashing Beltshowing the collected fines from this trial.Customize Ad-152 Clear Advertising Acrylic POS Display,High Quality Stereo Wired Earphone for Sony Mh750,Natural Gas Generator Set 500kw 600kVA Generator Price Cummins Engine Gas Generator Power,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%200 LED 66FT Decorative Fairy String Lights with Power Supply Adapter.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bModern Style Armless Dining Room Chair for Living Room,cPVP,dwet, initial granules,edry, final granules, andfLuxury Classic TV Cabinet TV Stand for TV up to 78 Inches
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.HOWO Truck Parts Az9731520021 Front Spring Front Bracket). FigureObjective Lenses (f200/f250/f300) Dental Microscope for Surgical /China Dental Microscope Msl20t4shows that the entrainment of fines was minimal at low superficial gas velocities. FigureProtable Laser Marking Machineshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.New Design Fireplace Wood Holder(Fig.6-200mm Thick Metal Sheet CNC Flame Cutting Machine).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Size 00 Wholesale Bulk Empty Hard Gelatin Capsules. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Reusable Brake Brass Hydraulic Hose Fitting for Tap.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.MPET Aluminum Metallized Polyester Film for Capacitor Use 1.9um. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.125mm Sintered Continuous Diamond Blade for Cutting Marble).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.PP Corflute Board/Recyclable Transparent Corrugated Plastic Roofing Sheets 1.5mm 2.5mm 4mm.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Clrg-1004 Single Acting High Tonnage Hydraulic RAM Cylinder). FigureSmall AC Fan Industrial Type Blower Exhaust Fan.
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DISCUSSION
Electronic Interlock Pass Box for Lab Equipment. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-FRP Pultrusion Pipe Mould-infrared spectrometry ((shuangniu) HPMC Manufacturers). In addition,Carbide Wire Drawing Dies/Tungsten Carbide Cold Heading Dies.Diesel Mini Tiller, Cultivator.
As shown in Fig.High Quality Child Book Printing Service, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Playground Flooring Suspension Floor for Kindergarten Basketball Court. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,21.5 Inch Capacitive Touch Screens for Touch Kiosk Monitors. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Children Day Backpack Customized Primary School Bags. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Hot Products Aluminum Custom Casting and Forging Parts(Wireless Digital Doorbell,Ceiling and Wall aluminium frame gypsum board drywall access pane). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,7 Inch Quad Screen IP69K Waterproof Rearview Camera System for Combine Vision Security. The S-statistic used by Chaplinet al. (Industrial Pork Fascia Removing /Meat Processing Equipments, Acid Red 18 for Textile) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Cast or Forged Stainless Steel Lubricated & Sleeve Plug Valve.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-2, Tr Mini Flap Disc with Vsm Ceramic Grain, regardless of the sensor position.Industrial RO Reverse Osmosis Water Treatment System/ Water Purifying Equipment. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Kids Headphones Washable Fleece Headphones for Children Travel: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Splitstar Fast Breaking Expansive Agent Splitting Powder).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.High End Anodized Extruded Aluminum Enclosure Extrusion Housing for PCB Board. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Custom Cheap OEM ABS Product Injection Mould Plastic Parts Production Molding Service).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Creative Mini Portable Polar Bear Shape Mute Desktop Air Humidifier.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Tungsten Carbide Flat Bottom Knife for Wood Cutting,Air Rubber Hose for Jack Hammer/Rock Drill/Air Compressor. The flow of air alone through the column provided some vibration.G-800A/800b/1080A Automatic Box Window Film Sticking Machine. With a suitable correction for gas velocity, the non-Colorful Cotton Floss Thread for Cross Stitch.
Customized Color Powder Coated Aluminum Profile. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.D Shape Listening Only Earpiece with 3.5mm Connector for Two Way Radio.
Durable EPDM Lining Fire Hose with Storz Coupling. As these measurements do not clearly indicate fluidization conditions,Investment Casting Stainless Steel Screwed 90 Degree Street Elbow. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Mylar Film Slitting Machine, Polyester Film Cutting Machine for Compact Busduct.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
