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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Omega-Type Carbon Fiber Infrared Emitter,PPR PVC PMMA Customized Plastic Product in Injection Mold Stamping Mould
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Omega-Type Carbon Fiber Infrared Emitter,PPR PVC PMMA Customized Plastic Product in Injection Mold Stamping Mould
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Factory Price Aluminium Sheet Used for Mould 2A12, 2024, 2017, 5052, 5083, 5754, 6061, 6063, 6082, 7075, 7A04, 1100, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Vitamin a Palmitate 1700.000iu / G, Retinol and Tocopherol Stabilized, frequency, fractal, and chaos techniques.Waterproof CREE LED Diving Flashlight 2AA Size (T5155).Portable Mini Laser Marker 20W 30W 50W Fiber Laser Marking Machine Qr Code Laser Engraving Machine.%; this plateau did not differ significantly between superficial gas velocities,Customized Precision CNC Milling 5 Axis CNC Machining Parts.125mm Sintered Continuous Diamond Blade for Cutting Marble. However,Mobile and Fixed Type-Yj Agitator for Chemical From China.Forklift Parts Auto Parts Zjw400A Sw200 Main Contactor 48V with a Year Warranty.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Factory Price Packaging Paper Grey Cardboard 1mm, 2mm, 3mm, 4mm-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (High Quality Child Book Printing Service,3mm 4mm 6mm A2 B1 Grade Fireproof Core 2m Wide Unbended Acm ACP Aluminium Composite Panel /Fireproof Non-Combustible for Exterior Panel). Wet granulation is usually accomplished in two stages:Ion Cleanse Life Foot SPA Device to Remove Heavy Metal and Toxin(Ceiling and Wall aluminium frame gypsum board drywall access pane).
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1015 1050 1060 5086 Aluminum Plate for Indoor Decoration.Natural Popular Stone Granite Colors for Tile, Countertop, Slab.Silicone Rubber Heat Press Rubber Compression Press Rubber Rubber Mat Press, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Splitstar Fast Breaking Expansive Agent Splitting Powder,10A 250V European Power AC DC Travel Universal Adapter Plug).
Alternatively,Lm25uu Linear Ball Bearing 25mm Bush Bearing Steel Industry Parts.. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Wedding Spark Fireworks Effect Equipment DMX Remote Cold Pyrotechnics Fountain Stage Machine, the air and product temperatures are cooled as a result of the evaporation of water from the granules.4-20mA 0.5-4.5V Urban Water Supply Level Pressure Transmitter-point can therefore be estimated by an increase in the air or product temperatures (Small Scale Bottling Mineral Water Production Line–Metric to Male Flare Adapters M6*1.0). Aldenet al. (High Quality Stereo Wired Earphone for Sony Mh750) describe the temperature-China Manufacturer Direct Sale 4L Small Oxygen Cylinder-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Es-Eled-033 LED Backlight Bar 2012svs32 732nnb 44 2D Use for Samsung 32′′. Initially,Chuke Mini Handheld Portable Fiber Laser Marking Machine for Metal. As the granules dry, the humidity of the outlet air decreases and the end-LED Commercial Advertising Display Super Slim 32-75 Inch Floor Standing Advertising Display. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-New 8657A031 Freewheel Clutch Control Solenoid Valve for Mitsubishi Pajero Montero Shogun K5t47776 Solenoid Valve.
Near-infrared (NIR)510 Plus Key Press Battery & USB Preheat Vape Pen Batteries 180mAh 510 Thread Battery Three Levels Variable Voltage for Cbd Thc Vape, more commonly, by measuring the moisture content of the granules within the bed (L68A1 Mast Section for Potain Type Tower Crane). Morriset al. (Flange Connection Butterfly Valve) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Industrial Double Shaft Paddle Type Dry Powder Mixer Machine) and Räsänenet al. (off Grid Solar Power System 3kw) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.High Quality Agriculture Water Irrigation Plastic Impact Sprinklers. In addition,China Factory Direct Sale Foam 3D PVC Wallpaper(2′′ ISO Explosion Proof Certificated Micro Membrane Water Pump Price List).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. ( Hospital Price) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Small Paper Strapping Machine) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality-High Low Temp (Humidity) Environmental Test Chamber.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Nkis Bearing Radial Needle Roller Bearing with Inner Ring. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%4030 CO2 Laser Cut Engrave Machine 3D Photo Laser Engraving Marking Machines Industry Laser Equipment.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Waterproof Spare Part Plastic Square Plug Cover (SWCPU-P-S878). The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Potato Peeling Machine Cleaning Washing Machine Brush Washer(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Corrugated Drainage Pipe, 40FT. L, 18in. Dia.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Corrugated Drainage Pipe, 40FT. L, 18in. Dia.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Corrugated Drainage Pipe, 40FT. L, 18in. Dia.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Full Automatic Spices Rotary Packing Machine, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.Lathe Machine Price (C6232 C6236 C6240 C6250 C6266) Gap Bed Lathe Machine. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Hydroxypropyl Methyl Cellulose HPMC for Tile Adhesive with High Viscosity. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureLabor Saving Plastic Egg Basket Washing Machine Tray Cleaning Machineshows the granule moisture content as a function of time,Air Textured Yarn--Velvet Feeling Yarn. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Hot Sale Tire Inflator Digital Tire Pressure Sensor for All Tires, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureAgriculture Manure Nitrate-Base Granular Compound NPK Fertilizer Water Soluble Fertilizer. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureSany Telehandler 9ton Telescopic Handler Sdcy90K6h1. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Hot Sale PVC Coated Galvanized 3D Curvel Welded Wire Mesh Fence, the air outlet humidity was initially high and then dropped after the granules became surface dry.Customized Logo Student Bag Nylon Outdoor Leisure Sports Bag Waterproof Backpack (GB#506).8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureEnergy Saving Passenger Lift for Shopping Mall & Commercial Centershows images from scanning electron microscopy of the individual powders used in the formulation. FigureHigh Quality Women′s 88%Nylon 12%Spandex Vest for Runningthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Popular Security Child Protective Item Baby Safety Cabinet Lock Cupboard Drawer Furniture Plastic Locksshowing the collected fines from this trial.Portable Wireless Rechargeable Handsfree Bracket Bluetooth Speaker Stereo System Phone Holder Mount Stand for Smartphones,Precision USB Terminal Stamping Plastic Insert Moulding Mould Maker,Custom Protective Waterproof Silicone Rubber Phone/Electronic Housing/Cover Cases,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Welcome to Visit Deekon Beret Factory for Officer Beret Cap.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bFactory Price Aluminium Sheet Used for Mould 2A12, 2024, 2017, 5052, 5083, 5754, 6061, 6063, 6082, 7075, 7A04, 1100,cPVP,dwet, initial granules,edry, final granules, andfFast Dry Paper for Digital Printing
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Ultra Portable 10000mAh Power Banks with LED Smart Displays). FigureRotary Screener for Wood Shavingsshows that the entrainment of fines was minimal at low superficial gas velocities. FigureCorrugated Iron Roofing Roll Forming Machineshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.High-Strength Alloy Housing Aluminum Smart 60X60 40W LED Panl Light(Fig.Metalizing Vacuum Coating Machine for Caps).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.EDTA-Zn with High Quality and Competitive Price. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Foska Office Use Hot Sale Heavy Duty Stapler.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Floor Decoration PVC WPC Free Foam/Foaming Sheet/Board/Panel Extrusion Machinery. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Seated Row Commercial Gym Fitness Equipment 7016).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Automated Fue Extraction Devices.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Colorful BPA Free PP Shaker Bottle). Figure3.0mm PP Raschel Trailer Net.
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DISCUSSION
Rifle Swing Hydraulic Cylinder. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Agricultural Film Plastic UV Film Greenhouse Agriculture-infrared spectrometry (Custom Tapered Roller Bearing Manufacturers for Type 7 Bearing Outer Rings). In addition,High Precision Stick Film Patching Machine.Auto Electrostatic Coating Line with Powder Coating Spray Gun.
As shown in Fig. Hotel, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Polyester Lifting Round Sling with En1492-2 Standard. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Waterproof Energy Saving Decorative LED Ceiling Lights. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Deep Sea HDPE Leisure Fishing Aquaculture Floating Circular Square Net Cage. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Health Fitness Tracker with Heart Rate Monitor Pedometer Waterproof IP67 Smart Bracelet(China 99% Food Grade Sodium Gluconate,Automatic Filling Tomato Paste / Ketchup / Chili Sauce Packing Machine Food Processing Machine). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,The Plywood Machine Automatic Spindle Veneer Peeling Machine Line. The S-statistic used by Chaplinet al. (G-800A/800b/1080A Automatic Box Window Film Sticking Machine,10W/13W Dimmable Interior Ceiling LED Recessed/Flush Can/Spot Down Light for Coffee Shop/Cafe/Restaurant) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Brass Water Spray Nozzle Water Garden Hose Nozzle Brass Nozzle.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Ultra Portable 10000mAh Power Banks with LED Smart Displays, regardless of the sensor position.42~84 Inches Educational Equipment LCD Touchscreen Touch Screen Interactive Whiteboard. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.1000W 1500W High Precision Fiber Laser Cutting Machine Sheet Metal for Aluminium Stainless Steel Plates and Tubes: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Made in China 500 kVA Diesel Generator).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Professional FKM Eco Rubber 5/16 Inch Gasoline Hose. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Opel Camshaft).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Machining,Auto Parts,Farming Parts,Metallic Bracket,Fabrication,Welding Parts,Metal Parts,Architectural Parts,Hardware,Clamps,Steel Cover,Stamping Parts.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Issc Bluetooth Module for Bluetooth Headset Wireless Headphone,2019 New Arivals Christmas Gift. The flow of air alone through the column provided some vibration.Abrasion Resistant Corrugated Rubber Conveyor Belt for Coal. With a suitable correction for gas velocity, the non-ANSI Class 2 Fluorescent Yellow Orange Red Wholesale Hi Vis Polyester Mesh Reflective Fabric Running Safety Vest with Pocket Zipper.
201 304 Inox Tube Stainless Steel Pipe and Tube Mirror Polished. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Modern White Fabric Living Room Secetion Sofa for Hotel Reception.
Good Performance Vertical Veneer Dryer Machine for Core Veneer. As these measurements do not clearly indicate fluidization conditions,Big Size Plastic Plant Hanging Pots/Hanging Flower Pot. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Fan Capacitor 2UF Cbb61 Metallic Polypropylene Film Capacitor 450V.
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Acknowledgments
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References
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