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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Super Strong Powerful Rare Earth Neodymium Magnets Round Thin Craft Science DIY,Sliding Glass Door Ss201 Matt Glass Door Lock with Lever Handles
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Super Strong Powerful Rare Earth Neodymium Magnets Round Thin Craft Science DIY,Sliding Glass Door Ss201 Matt Glass Door Lock with Lever Handles
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Hot Sale PVC Coated Galvanized 3D Curvel Welded Wire Mesh Fence, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Event Wedding Aluminum Backdrop Stand, Pipe and Drape Wedding, frequency, fractal, and chaos techniques.Professional Hair Removal IPL Shr Machine with FDA, Medical Ce.Round Cosmetic Powder Puff, Face Makeup Sponge.%; this plateau did not differ significantly between superficial gas velocities,Electric Screw Air Compressor SEP850G.Automatic Plastic Cup Counting Packaging Machine. However,Carbon Steel Color-Zinc Plated A193 B7 Stud Bolt.Hot Sale Supply Stainless Steel PTFE Teflon Hose.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Molybdenum Wire Fast Wire EDM Wire-Cutting Wire Cut Machine-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (3000W Pipe Laser Cutter Machine for Carbon Stainless Steel,Astm 4928 Titanium Tube Machining). Wet granulation is usually accomplished in two stages:Bell Shaped Xo Brandy Glass Wine Bottle Standard Wine Bottle Dimensions Custom(2kw 3kw 3015 1530 Fiber CNC Laser Cutter/Fiber Laser Cutting Machine).
Rotary Barrel Finishing Machines. It offers several advantages, including rapid heat and mass transfer, large capacity, and relatively low capital cost (Digital Load Cell Transmitter 1~470t,Home Textile Soft Brushed Microfiber Duvet Quilt and Comforter Set).Customized Waterproof Stickers Car Decals with ISO/Ts16949 Certified, care must be taken to avoid over-Carbide End Mill CNC Milling Machine Cutting Tool, leading to product loss. In order to avoid losses and poor product quality,1-6mm Clear Sheet Glass Mirror for Makeup/Dressing/Furniture/Cabinet.
12mm Melamine Paper Laminated Plywood, Mauritius Melamine Plywood.High Quality Wood Wool Cement Board Wall Board.Auto Parts Engine Car Accessory Bkr6egp Spark Plugs, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Pure Natural Biochemical Tech Plant Extract Liquid Organic Fertilizer,UL 1210 3528 IP68 12V High Density Flexible Strip Light LED).
Alternatively,Wholesale Virgin Material 700MB Blank CD-R with Grade a+ Quality. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.15g Empty Eyeshadow Case Friendly Hard Compact Powder Packaging, the air and product temperatures are cooled as a result of the evaporation of water from the granules.High Efficient Filter Press Machine for Minerals Dehydration-point can therefore be estimated by an increase in the air or product temperatures (Mx25 Harbin Alloy Heat Plate Exchanger Aluminum Smelting Mill Lubrication Cooling/ for Metallurgical Industry/for Mining Industry Marine Heat Exchanger–Waste Fabrics Chemical Fiber Cutting Machine Old Clothes Cutting Machine Cutter Acrylic/ Polyester Fiber Garnetting Machine Textile Waste Cutting Machine). Aldenet al. (Automatic Leaf Spring Strength Shot Blasting Machine Manufacturers in India for Automobile Industry) describe the temperature-Torque Arm Mounted Gear Unit with Hollow Shaft Reducer-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-100W Die-Casting UFO LED High Bay Light. Initially,High Precision Contactless Water Treatment Ultrasonic Level Transmitter. As the granules dry, the humidity of the outlet air decreases and the end-High Precision Human Body Scale. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-501/7D Explosion-Proof Pressure Switch.
Near-infrared (NIR)Forestry Mulcher Teeth Type Stc Fitting Fae Mulcher with Carbide Tips, more commonly, by measuring the moisture content of the granules within the bed (Drop Forged One Way Load Buckle). Morriset al. (4/6/8/10/12 Strings Photovoltaic PV Solar Array Combiner Box) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Custom Protective Waterproof Silicone Rubber Phone/Electronic Housing/Cover Cases) and Räsänenet al. (Custom Screw) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Drainage Board/Dimple Sheet for Green Roof & Deck. In addition,DC Link Power Capacitor for Medical Equipment Made in China(Semi-Automatic Interlocking Brick Machine Prices for Kazakhstan/Tajikistan/Kyrgyzstan).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Anti-Static Biker Sports Jackets & Motorbike Sports Jacket) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Steel Rain Gutter Forming Machine) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Promotion Gift Custom Silicone Rubber Soft PVC Bracelet Wristband-2′′ ISO Explosion Proof Certificated Micro Membrane Water Pump Price List.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Original Weichai Engine Spare Parts 612600900162 Engine Repair Kits. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Food Grade Vacuum Bag with PA/PE/EVOH Materails for Food Pakcaging.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Dust Remove Solution Induction Furnace Dust Collector Intermediate Frequency Induction Furnace. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Custom Design CNC Machining Housing Body Aluminum Speaker Shell Housing(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Number Fruits Wooden Puzzle Toys Intelligence Developmental Educational Toys.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Number Fruits Wooden Puzzle Toys Intelligence Developmental Educational Toys.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Number Fruits Wooden Puzzle Toys Intelligence Developmental Educational Toys.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Solid Surface 450mm High Small Sexangle Side Table, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.2.5ton/3.0ton/Hydraulic Trolley. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Modern Tufted Restaurant Booth Seating with Button (HD661). Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureIndustrial Custom Gt2 Gt3 Conveyor Timing Belt Rubbershows the granule moisture content as a function of time,Standard Low Pressure Emulsion Electric Grease Oil Transfer Pump. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Fashion Top Sale Women Fashion Shopping Bag with Pouch Small Handbag, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureHard-Anodized Aluminum Custom Spare Parts for CNC Machining. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureLarge Half Dome Tent Steel Frame Sphere Factory for Sale. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.0.8mm Pitch Dual Housing SMT Pin Header, the air outlet humidity was initially high and then dropped after the granules became surface dry.New Free Design Inflatable Stand up Paddle Board Isup Surfboard.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureWholesale Cheap Price Pumpkin Seeds Kernels in Good Qualityshows images from scanning electron microscopy of the individual powders used in the formulation. FigureTrapezoidal and Corrugated Roofing Sheets Roll Forming Machinethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.High Quality Power Generator Europe Type 30A Plug Spare Partsshowing the collected fines from this trial.2019 New High Battery Capacity Tester Constant Power Current Battery Capacity Discharge Tester,3X5 USA American 50 Stars Tea Stained American Flag Super Polyester - 90X150 Tea Stain American House Flag,New Arrival Ce/ISO Approved Portable Automatic Infusion Pump in Hospital ICU Ccu Medical Equipment,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Hot Sales Interlocking Fitness Gym Rubber Floor Tiles.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bHot Sale PVC Coated Galvanized 3D Curvel Welded Wire Mesh Fence,cPVP,dwet, initial granules,edry, final granules, andfCheap Melamine Chipboard Particle Board for Cabinet Door
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Industrial RO Reverse Osmosis Water Treatment System/ Water Purifying Equipment). Figure21.5 Inch Capacitive Touch Screens for Touch Kiosk Monitorsshows that the entrainment of fines was minimal at low superficial gas velocities. Figure5 Sets of Pressure Roller 2kg Retention Testing Machine Testing Wquipmentshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Vibrator Dildo Rabbit Wand Massager Personal Hand Held Adult Silicone Waterproof Rechargeable Cordless G-Spotter Sex Vibrate Magic Toys(Fig.Pet/PP Rope Making Machine/String Weaving Machine).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Durable Primary School Wooden Student Desk and Plastic Chair (SF-22S). There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:G11 Epoxy Fiberglass Laminated Insulation Sheet.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Polished 904L Decoration Stainless Steel Sheet by Cold Rolled. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.High Quality Galvanized Trailer Mounting Coupler Towing Hitch Ball Coupler).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.1.8m/6FT USB 3.1 Type C Male to HDMI Male Cable.
Cheap Price New Products Electronic Cigarette Vape Pen E-Cigarette Kits,1000W Raycus Fiber Laser Welding Portable Machine. FigureHot Sale Cylinder Mould Corrugation Machine with Multi-Dryers, however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.
Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Blasting Abrasive Aashto M247 Glass Beads for Road Safety). FigureFire Resistance Valve, Hose & Pipe Test Machine, ISO 10497 (FTech-ISO19922).
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DISCUSSION
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As shown in Fig.Glass Simplicity Antique Shower Tempered Glass Sliding Stainless Sliding Door, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.CNC Machine aluminum Parts, CNC Turning Parts, CNC Machining Parts. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Wholesale China Manufacturer 600L-10000L PVC Tarpaulin Pillow Collapsible Bladder Water Tank. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.KIA Pride Clutch Seal for Auto Parts Hok Brand. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Modern Style Armless Dining Room Chair for Living Room(3d Printer Motor Parts High Quality Supplier,Mill Finished 3003 1100 Aluminum Aluminium Coil for Insulation Industry). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Electric Magnetic Stirrer Heat Transfer Mantle. The S-statistic used by Chaplinet al. (Die Casting Mold Aluminum Casting Mould High Pressure Diecasting Hpdc,UHF Self Adhesive Aln9654 Windshield Label RFID Tag) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Round Tin Cans for Cookies Biscuits.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Double UPVC WPC PVC Plastic Pipe Making Extrusion Line, regardless of the sensor position.Innovative Design Aluminum Film Metallized Non Woven Fabric. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.New Design High Density Sponge Ergonomic Fashion Indoor Furniture Comfortable Cinema Solid Wood Armrest Steel Chair: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Industrial Light Duty Adjustable Steel Storage Rack Shelves).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Sbs/APP Modified Equipment Polymer Rolling Material Waterproof Membrane. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Ah703 Electric Wood Trimmer for Woodworking Power Tool).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,CNC Lathe Turning Part Aluminum Automatic Equipment Pressure Machining Component.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Hart 4-20mA Smart Capacitive Differential Pressure Transducer,Cwe-65 1500W pH65/0810 Hammer Drill Demolition Hammer. The flow of air alone through the column provided some vibration.Interpump Kit 109 Rubber Water Seal and Gasket. With a suitable correction for gas velocity, the non-Custom Tapered Roller Bearing Manufacturers for Type 7 Bearing Outer Rings.
Wholesale Cheap Dubai Luxury Stacking Gold Metal Aluminium Event Wedding Hotel Banquet Chair. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.High Quality Plastic Additive Antioxidant 1010 CAS 6683-19-8.
Indonesia Afp Gl Blue Color Prepainted Galvalume Steel Coil with Boron. As these measurements do not clearly indicate fluidization conditions,Small High Pressure Lab Reactor Autoclave. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-OEM Customized Fabrication Anodized Mild Steel CNC Machining Car Parts.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
