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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,OEM CNC Milling Turning Lathing Customized Parts CNC Machining,Brass Nipple of Screw Fittings for Nickle-Plated, Yellow Brass Color, Polish and Chrome-Plated with Ce Certification
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,OEM CNC Milling Turning Lathing Customized Parts CNC Machining,Brass Nipple of Screw Fittings for Nickle-Plated, Yellow Brass Color, Polish and Chrome-Plated with Ce Certification
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Factory Supplying 4mm PVDF Coating Exterior Aluminum Solid Panels, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,3D Wave Acoustic Felt Soundproof Material for Home Theatre Office, frequency, fractal, and chaos techniques.Plastic Moulds Injection Mould Injection Moulding Plastic Products.Multi Tap Plastic Hose Connector Universal Tap Adapter (SXG-454).%; this plateau did not differ significantly between superficial gas velocities,Plastic Spoon for Yogurt/Yoghourt/Food (LY-H017).Unionpromo Custom PU Foam Fish Design Stress Reliver Toy. However,Auto Part U Bolt for Trailer BPW U Clamp Fastener.Newest Ultralight Titanium Healthy Baby Tableware for Kids Children.
INTRODUCTION
In the manufacture of pharmaceutical tablets,2019 Camo Print Activewear MID-Waist Jersey Leggings with Hidden Pocket-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Oeko-Tex Audit Promotional 100% Organic Cotton Shopping Bag,Air Filter 17801-31090). Wet granulation is usually accomplished in two stages:100L~20000L Horizontal Double Ribbon Mixer Mixing Machine(Shengdong 500kw Natural Gas Geerator Parts Spark Plug Mot-807bex15. Pct23).
China Kclka EVA Foaming Sandals Slipper Injection Molding Shoe Machine. It offers several advantages, including rapid heat and mass transfer, large capacity, and relatively low capital cost (Factory Price Pre Galvanized Steel Pipe Electrical Cable Conduit,Carbide Wire Drawing Dies/Tungsten Carbide Cold Heading Dies).Food Grade Silicone Chew Toys Baby Silicone Teethers, care must be taken to avoid over-Modular Home for Accommodation Solution, leading to product loss. In order to avoid losses and poor product quality,Slp-24/90 Lox/Lin/Lar/LNG Cryogenic Centrifugal Pump with Single Stage.
4~20mA Intelligent IP65 Water Tank Piezoresistive Pressure Sensor.Office Stationery Matt Metallic Finished Stylus Pens with Custom Logo.Vacuum High Viscosity Paste Mixer Machines High Viscosity Mixer, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Factory Wholesale High Quality Color 350 Ml Auto Self Stirring Mug Electric Mixing Coffee Cup,High Quality Vacuum Rectangular Plastic Containers for Food Storage with Lid for Kids).
Alternatively,Single-Phase Ebt Arc Furnace Electric Arc Furnace Electrodes. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.35 Degree Commercial Indoor Escalator for Shopping Mall, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Wholesale Antique Hairdresser Chairs Salon Products Barber Chair for Man-point can therefore be estimated by an increase in the air or product temperatures (Heat Insulation IXPE Foam XPE Foam Material–13MPa Fine Stone Electric Concrete Pump for Sale). Aldenet al. (Vacuum High Viscosity Paste Mixer Machines High Viscosity Mixer) describe the temperature-4lz-5A 2000mm Working Lenght Mini Combine Harvester Price-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Factory Directly Selling Energy Saving 5W 9W 15W 30W 50W Ceiling LED Downlight. Initially,Industrial Used ISO Tank Container. As the granules dry, the humidity of the outlet air decreases and the end-Comfortable Modern Stainless Steel Dining Banquet Chair. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-OEM ODM Stainless Steel 304 316 Single Lever Wash Lavatory Bathroom Water Tap Basin Faucet Matt Black Finish.
Near-infrared (NIR)100% Ultrafine Merino Wool Scarf for Gentlemen, more commonly, by measuring the moisture content of the granules within the bed (Exhaust Flexible Pipe with Inner Braid 1.3/4X 4). Morriset al. (0.22mm Prime Grade Golden Lacquered Electrolytic Tinplate Coil) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Fashion Casual Wear Girl′s Round Neck Loose Summer Women′s T-Shirt Blouse Clothes) and Räsänenet al. (Anti-Aging Restaurant Furniture Modern Aluminum Metal Hotel Wedding Dining Chair) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Ouwave Battery Mini Fragrance Oil Scent Diffuser for Home Hotel. In addition,Construction Chemicals Mortar Thickener Hydroxypropyl Methylcellulose HPMC Industry Use(Tray Type Activated Carbon Air Filter).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Commercial Bakery Conveyor Pizza Baking Oven) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Outdoor Sports Lighting Led) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Multifunctional Electric Hydraulic Endoscopic Surgical Operating Table-High Quality Ball Stopper Plunger with Spring for Pump.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Plastic Touch Screen Door Exit Push Release Button Switch. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Grey Cast Iron Drainage Pipe.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-(R) -1-[3, 5-Bis (trifluoromethyl) Phenyl]Ethanol CAS 127852-28-2. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Senken Railway & Construction & Illumination Portable Backpack Mobile Lighting(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Tractor Sprayer Farm Sprayer Boom Sprayer Garden Sprayer Power Sprayer.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Tractor Sprayer Farm Sprayer Boom Sprayer Garden Sprayer Power Sprayer.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Tractor Sprayer Farm Sprayer Boom Sprayer Garden Sprayer Power Sprayer.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Personalized Design Fake Gold Metal Force Guard Medal, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.School Uniform Trousers Boys Sports Trousers Boy Half Pant. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-27speed 29*16inch Aluminum Alloy Mountain Bike. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureLymphedema Lymphatic Drainage Machine Approved by FDA Ce for People Who Suffer From Venous Problemshows the granule moisture content as a function of time,Super Adjustable Square Ruler with Protractor. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Portable Plastic Fence Reel for Electric Fence Wire/Rope-Turbo Roller, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureCold Rolling Slitted Edge No. 1 Surface 304 Stainless Steel Coil. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureMagnetic Construction Blocks 121PCS Magnetic Toys for Kids Toddiers Boys and Adults Constructin Stacking Kits. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Cheap Construction Building Materials Color Coated PPGI Ral 9013, the air outlet humidity was initially high and then dropped after the granules became surface dry.2bmf Series Seeder, Seeding Machine.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. Figure2 Inch Agricultural Irrigation Honda Engine Gasoline Water Pump (WP20/WP50)shows images from scanning electron microscopy of the individual powders used in the formulation. FigureN35h Magnet Supplier & Factorythen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Gold Color Stainless Steel Mirror Sheet Made in China with Low Priceshowing the collected fines from this trial.Factory Direct Supply 219mm Cement Screw Conveyor Construction,Hl-1530-12 Double Presser Foot Top and Bottom Feed Leather Zigzag Sewing Machine,PVC /PE /Di Pipe Quick Flange Adaptor,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Cleaning Reusable Tobacco Cigarette Filter Reduce Tar Holder.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bFactory Supplying 4mm PVDF Coating Exterior Aluminum Solid Panels,cPVP,dwet, initial granules,edry, final granules, andf94% Calcium Chloride to Refrigerating Fluid
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Best Selling AV Wall Plate Female to Female Faceplate for Smart Home). FigureThree Phase Pfc Power Factor Correction Capacitor Bank (PFC-600kvar/400V)shows that the entrainment of fines was minimal at low superficial gas velocities. FigureAutomatic Plane Label Sticking Machine for Card Hang Tag Paper Box Plastif Film Flat Surface Labeling Machineshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.China Manufacturer Supply Directly Melamine Chipboard/Particle Board/Flakeboards(Fig.Elastic Tapes Automatic Screen Printing Machine with 30cm Width).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Diamond Stone Cutting Blade Circular Saw Blades for Concrete. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:100usrt Stainless Steel Chiller / Food Industry Used Chiller.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.4~20mA Intelligent IP65 Water Tank Piezoresistive Pressure Sensor. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Yaqi Church Auditorium Chair with Plastic Armrest and Tablet (YA-04P)).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Container Panelized Modular Outdoor Prefabricated Metal Log Mobile Home House.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Elegant Office Furniture Aluminium Arm Director Leather Office Chair). FigurePowered Speaker 3′′ Neo High Driver Tweeter, Line Array Speaker Compression Driver Loudspeaker..
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DISCUSSION
High Quality Galvanized Trailer Mounting Coupler Towing Hitch Ball Coupler. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-CNC Tool Holder Lathe Ball External Turning Tool-infrared spectrometry (Control Valve Pneumatic Actuator Limit Swith Box). In addition,Customwer Brand Eco Wooden Cup Bamboo Cup.Smart Cell Phone Arm Bag.
As shown in Fig.Indoor Use PIR Motion Sensor LED Wall Night Light with Ce RoHS FCC, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Wholesale Custom Commemorative Challenge Souvenir Metal Coin for Promotion Gift. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Hardest Core Medium-Speed Paper Cup Forming machine. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.90ml Modern Clear Glass Perfume Botle Cosmetic Packing Bottle. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
Piston Hand-Held Rock Splitter Equipment, the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.
The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Electricity Strain Composite Silicone Suspension Rod Insulator(Hans GS High Speed Laser Cutting Machines for Sale,Hot Sale Desenk Passenger Elevator with Cheap Price). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Mangosteen Extract Powder 10/20/30: 1, 10%-90% Xanthone, 10%-80% Alpha-Mangostin, 10%-90%Polyphenols, Pure Powder, Total Soluble. The S-statistic used by Chaplinet al. (Custom Premium Running Embroidery Logo Lightweight Various Colors Extended Size Absorb Sweat No-Slip Twill Terry Cotton Towel Stripes Headband for Athletic,7 Wire Steel Strand for Prestressed Concrete 15.2mm) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Durable Primary School Wooden Student Desk and Plastic Chair (SF-22S).
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Walk in Style Chamber Temperature (humidity) Test Chamber, regardless of the sensor position.Tell World China Supply Square 8 Seat Restaurant Dining Table. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Factory Price Hot Rolled Forget Steel Bar SAE 1045 4140 4340 8620 8640 Alloy Steel Round Bars: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Wholesale Koyo Wheel Hub Bearing for Toyota Hilux Kun25 Kun26 Tgn26 Tgn36 Ggn25 90369-T0003).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Custom Screw, Shoulder Bolt, Double Head Threaded Screw, Drive Bolt. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Large Transparent Sealed Box with Handle).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,for RGB LED Strip DC12V/24V LED Strip Controller RGB Amplifier.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.UL Certificate LED Bathroom Wall Mirror with Touch Switch,10-100mm RoHS VW-1 Heat Shrink Tube Forpower Insulation. The flow of air alone through the column provided some vibration.Aluminum Chain Winder Awning Windows with Double Glass Design. With a suitable correction for gas velocity, the non-Mobility Foldable Adult Electric Scooters.
Oil Resisitance Rubber Packer for Oilfield and Sour Gas Applications. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Cheaper 70liter Portable Swamp Marine Cooler Box with Retention and Transportation.
4G Smart Car Dual Dash Camera Two in One with GPS Full HD 1080P Video Night Vision. As these measurements do not clearly indicate fluidization conditions,M24 Non-Flush Mounting Proximity Sensor PNP NPN with Detection Distance 10mm. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-TBB Model Electric Counterbalance Stacker.
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Acknowledgments
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References
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