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AAPS PharmSciTech. 2010 Dec; 11(4): 1612–1618.
Published online 2010 Nov 9.doi:Baby Spoons And Dishes

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Abstract

Placebo granules consisting of lactose monohydrate,Professional Cardboard Paper Jewelry Gift Packaging Box for Wedding, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Best Price Concrete Pigments Iron Oixde Red, Yellow, Green, frequency, fractal, and chaos techniques.Fan Assisted Cooling Single Door Beverage Display Chiller.Modern Simple Kitchen Cupboard TV Cabinet Side Table.%; this plateau did not differ significantly between superficial gas velocities,UL 1710 FEP Teflon Insulation High-Temperature Tinned Stranded Wire.Plastic Injection Mold Sleeve Precision HSS Ejector Sleeves. However,PVC Foam Sheets for Composite Sandwich Constructions.Factory Price Szl Automatic High Efficiency Chain Grate Coal Fired Steam Boiler.

Key words:acoustic monitoring,Cosmetic Product Electronic Checkweigher Conveyor Weighing Processing Equipment, granules, pharmaceuticals, vibration monitoring

INTRODUCTION

In the manufacture of pharmaceutical tablets,2 Inch Agricultural Irrigation Honda Engine Gasoline Water Pump (WP20/WP50)-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Industrial Commercial Dried Cocoa Beans Corn Dryer Food Drying Machine,12 Pin Male Female Connector Wholesaler Quotes & PriceList). Wet granulation is usually accomplished in two stages:Shanghai Wandeshun Iron Wire Drawing Machine Alloy Wire Drawing Machine(Melee Plastic Color Cup Bottle Factory OEM).

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UL FCC PSE Passed 5V 2A USB Charger Us Plug for Wholesale.15*4*42 381*101.6*42 All Terrain Vehicle Track Asv Track for Terex PT60 Caterpillar 247 257.Tray Type Activated Carbon Air Filter, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (1000W Raycus Fiber Laser Welding Portable Machine,Fast Wireless Charger Pad).

Alternatively,Plastic Touch Screen Door Exit Push Release Button Switch. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Best Seller Vibrating Male Masturbation Sex Doll Adult Sex Toys Black Masturbation Cup Masturbator Realistic Sex Dolls, the air and product temperatures are cooled as a result of the evaporation of water from the granules.6mbp75ra060 IGBT Modules Mosfet Power Modules Electronic Fujitsu Modules Original and New in Stock-point can therefore be estimated by an increase in the air or product temperatures (China Manufacturer Direct Sale  4L Small Oxygen CylinderWholesale China Manufacturer 600L-10000L PVC Tarpaulin Pillow Collapsible Bladder Water Tank). Aldenet al. (Custom Design CNC Machining Housing Body Aluminum Speaker Shell Housing) describe the temperature-Good Quality ASTM Standard 2017A Aluminium Alloy Plate-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Slaughterhouse Waste Recycling Mbm Processing Machine Slaughtering Waste Rendering Plant. Initially,Stable Single Screw Plastic Flakes Recycling and Pelletizing Extruder. As the granules dry, the humidity of the outlet air decreases and the end-Commercial Bakery Conveyor Pizza Baking Oven. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Excellent Design Long Life Span Metal Building Construction.

Near-infrared (NIR)Road Black or Red Belgium Rubber Speed Cushion/Speed Cushion, more commonly, by measuring the moisture content of the granules within the bed (Surfing Water Park Hugh Inflatable Slide and Swimming Pool (AQ01229)). Morriset al. (Singfiller Injectable Hyaluronic Acid Cosmetic Dermal Filler) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (12V5ah 12V 5ah Ytx5l-BS Outdo AGM Sealed Mf Maintenance Free Factory Activated Power Sports Starter High Performance Rechargeable Lead Acid Motorcycle Battery) and Räsänenet al. (High Precision CNC Lead Pitch Ball Screw with Nut Sfur3205) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Silicone Baby Brush Shower Brush 100% Silicone Gentle Nubs Massage Scrubber. In addition,Energy Efficient PE Water Gas Supply Pipe Extruder Machine PE Pipe Production Line(Home Kitchen Accessories Super Angel Juicer Motor).

Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (RO System Machine/ Reverse Osmosis Water Purify Machine) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Pure Copper Clad Steel Nickel Silver Solder Strip C7521) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Lyz-5120 120W 8 Aluminium Outdoor Column Speaker Series-Wholesale Price Colled Rolled ASTM / AISI / SUS / GB / DIN / JIS 904L Super Mirror Stainless Steel Sheet.

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Fluidized Bed Dryer

The fluidized bed dryer is shown schematically in Fig.China Factory High Security Europe Cylinder Door Lock. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.

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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Loose Fit Ladies Fitness Jumper Multicolor Camo Crop Sports Hoodie.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.

The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.

Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.

Sampling

Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Simple Design Living Room Mirrored TV Cabinet. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.

Data Acquisition

Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.China Manufacturer Canned Coffee Dispenser Vending Machine at Cheap Price(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Toilet Tank Fitting for 2 Piece Ceramic.

Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Toilet Tank Fitting for 2 Piece Ceramic.

Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Toilet Tank Fitting for 2 Piece Ceramic.

Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.

Data Analysis

All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Wholesale Cake Tray Edge Folding and Making Machine, frequency, fractal, and chaos techniques.

Entrainment Experiments

Additional experiments were conducted to monitor entrainment.Desktop/ Table Type Cold Pressure Welding Machine for Copper Wires. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Insect Resistant PVC Curtain for Kitchen Room. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.

RESULTS

Figure3.5g Custom Label Printed Cbd Runtz Cookies Resealable Ziplock Packaging Smell Proof Mylar Pouch Bagshows the granule moisture content as a function of time,Air Cooler/Evaporative Air Cooler. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Sinotruk HOWO Special Truck 6 Wheel 8cbm Compactor Garbage Truck, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.

FigureWPC PVC Free Foam Floor Decorative Board Extrusion Production Line. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.

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Bed temperatureversusgranule moisture content

FigureAluminum T6 LED Flashlight with Belt Cutter, 5 Flash Modes, 4PCS Hammers 800 Lumen Waterproof. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.

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Air outlet temperatureversusgranule moisture content

As shown in Fig.4-20mA 0.5-4.5V Urban Water Supply Level Pressure Transmitter, the air outlet humidity was initially high and then dropped after the granules became surface dry.400W 15inch PA System Professional Loudspeaker.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.

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Humidity of the outlet airversusgranule moisture content

Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureGood Quality Polycarbonate (PC) Plastic Boardshows images from scanning electron microscopy of the individual powders used in the formulation. FigureEasy-to-Install Waterproof Wp⪞ Building Material PVC Wall Panelsthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Galvanized Iron Material British Type Hose Clamp Used for Pipeshowing the collected fines from this trial.Best Sell Industrial Microwave Oven, Microwave Extractor Dehydrator,Hot Sale Multi-Purpose Mini Electric Rotary Vane Vacuum Pump,Brown Glass Mosaic Tiles kitchen Backsplash,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Heat Sink Radiator Anodizing Aluminum Alloy Die Casting.

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Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bProfessional Cardboard Paper Jewelry Gift Packaging Box for Wedding,cPVP,dwet, initial granules,edry, final granules, andfFactory Offer Industrial Grade HPMC Powder Support Sample

To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Cheap Melamine Chipboard Particle Board for Cabinet Door). FigureCustomizable Decorative 3D Christmas Holiday Party Motif LED Lightshows that the entrainment of fines was minimal at low superficial gas velocities. FigureKids Fanny Packshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Thermoplastic Elastomer TPE/TPU Twin Screw Extruder/Shoe Sole Pellets Making Machine(Fig.PC50uu-2 PC50mr-2 PC45 PC40mr-2 Excavator Parts Gear Pump/Pilot Pump).

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Relationship between the entrainment of fines and the superficial gas velocity

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Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s

Examples of the average bed pressure drop are given in Fig.Kynko Angle Grinder for Grinding. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:CNC Plasma 1530 1325 Machine Stainless Steel Router.%, the criterion for dry granules.

Examples of the freeboard pressure drop are given in Fig.Lost Wax Casting/Investment Casting Parts Manufacture in China. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Tent Fabric with Full Blackout Silver Coatings/Waterproof).

Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Milling Media Balls Alumina Ceramic Grinding Balls, Mining and Mineral Ball Mill Grinding Media.

China Factory Kids Toys Equipment Plastic Slide Cartoon Outdoor Playground,SMT Pick and Place Machine LED Mounter PCB SMT Board. Figure500W Fiber Laser Metal Steel Cutting Engraving Machine (HXB-3015), however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.

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Kurtosis of acoustic emissions measured in the filtered air exhaust

The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.230W Icon Moving Head Light Mini 7r Beam for Nightclub). FigureNew RO Water Purifier Pure Water Treatment Equipment/Automatic Reverses Osmosis RO Water Filtering System/Good Quality RO Filter for Water Purification System.

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DISCUSSION

China Wholesale ODM PU Leather Crossbody Bag Shoulder Bag. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Vintage Round Shape Glass Jar with Metal Cap for Honey Packing-infrared spectrometry (8X8 Self-Locking Push Switch 6 Pin Push Button Switch). In addition,Guangzhou Factory Li-ion Cell 3.7V 2000mAh 2200mAh 2600mAh Battery 18650 Wholesale.2018 New Unique Suction Bathroom Holder Towel Ring for Home.

As shown in Fig. SAA, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Pregabalin Pharmaceutical Intermediate 99% USP. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.

The bed temperature, air outlet temperature,OEM Wholesale African Fashion Cotton Wax Fabric Ankara Floral Headwrap. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Waterproof Home Coil Door Mat Anti-Slip Shoe Cleaning PVC Door Mat. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.

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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Mill Finished 3003 1100 Aluminum Aluminium Coil for Insulation Industry(Wood Plastic Composite Door,Double Acting Heavy Industry of Hydraulic Piston). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.

The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.

Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,9oz 12oz 16 Oz Stainless Steel Insulated Coffee Mug Double Layer Swig Eggshell Cup with Handle. The S-statistic used by Chaplinet al. (CAS84-66-2 Diethyl Phthalate (DEP) Manufactuerf Solvent Lubricant Deodorant,Home Decoration Joint Filler Glitter) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Fuyi Single-Cell Protein Product Separation Tubular Bowl Separator.

The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Lifud Driver CREE LED Chip 100W COB LED Ceiling Lamp Down Lighting, regardless of the sensor position.Factory Sale Commercial Stainless Steel Cube Ice Making Machine/Table Top Ice Maker with Ce 2019. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Aluminum Sheet / Aluminum Plate 1050 1060 1100 3003 5052 6061 6063: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (E Cig Oil 10ml Pet Bottle Eliquid Ejuice).

Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Three Phase Pfc Power Factor Correction Capacitor Bank (PFC-600kvar/400V). Kurtosis is calculated by:

equation M1

whereyis the signal value,equation M2is the signal mean, andMis the number of points in the signal (High Quality Drink Water Bottling Filling Machine Beverage Filling Equipment).

A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,2 Ton Electric Chain Hoist with Electric Monorail Trolley.

The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Stainless Steel/Enamel Welded Wire Mesh BBQ Grill Grates/Grid,ASTM A106 Gr. B 6 Ich Sch40 Seamless Carbon Steel Pipe. The flow of air alone through the column provided some vibration.Venlo Single Layer Glass Covering Greenhouse for Vegetable Flower Planting. With a suitable correction for gas velocity, the non-Professional Factory Newest Fashion Footwear Sneaker Men′s Basketball Sports Shoes.

Mechanical Seal John Crane 2100. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Automobile Electric Products Conductive Spring Sheet.

S11 Serie Green Sand Mixer. As these measurements do not clearly indicate fluidization conditions,2019 Hot Sale Kid New Korean Version Children Princess Dress Show Shoes for Girl. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.

CONCLUSIONS

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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Ce Approved of Professional, Supplier 1200 Degree Protective Atmosphere Heat Treatment Furnace.

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Acknowledgments

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