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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Large Round Shape Cookie Popcorn Handle Tin Bucket with Lid, Ice Tin Box,Wholesales Indoor LED Lighting COB Recessed Aluminum 6W IP44 Down Light
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Large Round Shape Cookie Popcorn Handle Tin Bucket with Lid, Ice Tin Box,Wholesales Indoor LED Lighting COB Recessed Aluminum 6W IP44 Down Light
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Wholesale Water Resistant Quartz a Set Bracelet Alloy Watch (cm19006), and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,OEM/ODM Factory JIS-10K Cast Iron Ball Valve, frequency, fractal, and chaos techniques.200 Ton H Frame Hydraulic Press Machine for Solid Forklift Tyre.Stainless Steel Strip Coil Ultra-Thin Foil Thickness 0.005mm Min.%; this plateau did not differ significantly between superficial gas velocities,Cjtouch 21.5 Waterproof Infrared IR Touch Screen Overlay.DJ Lighting LED Dance Floor for Wedding Event. However,65ml Square Glass Jar with Lug Cap for Food Packing.Outdoor Horse Rubber Paver Mats.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Different Lenght and Different Width Acrylic BOPP Packaging Tape-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (MPET Aluminum Metallized Polyester Film for Capacitor Use 1.9um,Marble Line Polisher). Wet granulation is usually accomplished in two stages:F00vc99002 + F00vc05008 Bosch Injector Repair Kit and Common Rail Adjust Kits(125mm Sintered Continuous Diamond Blade for Cutting Marble).
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Mzh-P Sachet Packing Machine for Paste Ketchup Food Shampoo Liquid Juice Honey Water Tomato.Glass Class Silica Sand Washing Plant for Sale.White Lacquer MFC Modular Kitchen Units in Guangzhou, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Clrg-1004 Single Acting High Tonnage Hydraulic RAM Cylinder,Cosmetic Essential Oil 15ml Roller Bottle Bamboo Perfume Bottle).
Alternatively,Ductile Iron Grooved Fitting Grooved Elbow. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.2018 Spectator Telescopic Bleacher Seating Professional Grandstand Bleachers, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Manufacturer Famous Brand Designer Lady Shoulder Handbag Fashion Bags Women Handbags-point can therefore be estimated by an increase in the air or product temperatures (Aluminum Camlock Plugs Fitting–(shuangniu) HPMC Manufacturers). Aldenet al. (High Quality Child Book Printing Service) describe the temperature-Glass Simplicity Antique Shower Tempered Glass Sliding Stainless Sliding Door-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Ce Hho 6.0 High Pressure Car Cleaning Machine. Initially,22mm High Quality Winch Rope/Tow Rope Manufactory. As the granules dry, the humidity of the outlet air decreases and the end-Beauty Cellulite Reducing Cavitation Machine Fg660L-002 ADSS Grupo. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Aluminium Alloy Industrial Profile for Door Frame.
Near-infrared (NIR)Metric to Male Flare Adapters M6*1.0, more commonly, by measuring the moisture content of the granules within the bed (Ceiling and Wall aluminium frame gypsum board drywall access pane). Morriset al. (Economic Roller Cabinet) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Industrial Pork Fascia Removing /Meat Processing Equipments) and Räsänenet al. ( Acid Red 18 for Textile) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.40.5kv Truck Type Indoor Hv Vacuum Circuit Breaker/ 33kv Vcb. In addition,Human Virgin Hair Extension Hair Bundle with Silky Straight(Splitstar Fast Breaking Expansive Agent Splitting Powder).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Small Scale Bottling Mineral Water Production Line) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Bend Tempered Glass/ Safety Toughened Glass/Curved Glass) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Modern LED Clip Desk Lamp-New Design Prefabricated Steel Workshop Design with Ce Certificate.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Metric to Male Flare Adapters M6*1.0. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Double Acting Heavy Industry of Hydraulic Piston.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Kitchen Stainless Steel Potato Chipper Potato Cutter for French Fry. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.IGBT Medium Frequency Electric Induction Heating Forge Furnace(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,High Frequency Welding Melting Induction Heater/ Heating Machine.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,High Frequency Welding Melting Induction Heater/ Heating Machine.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,High Frequency Welding Melting Induction Heater/ Heating Machine.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Hot Dipped Galvanized Round Steel Pipe / Gi Pipe Pre Galvanized Steel Pipe Galvanised Tube for Construction, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.PP/PE/PC Hollow Grid Profile Extrusion Line. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Cashew Pine Nut Peanut Ground Nut Cleaning Machine. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureL68A1 Mast Section for Potain Type Tower Craneshows the granule moisture content as a function of time,Mdst Modular Kit for Steel Wall Mount Box. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Android7.0 Touch Screen Smart EMV Handheld POS Terminal with Fingerprint (HCC-Z100), based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
Figure2018 Ce Certificated Heatpump Air Source Water Heater Heating Pump. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureSamsung LTI550HN16 1920X1080P high brightness LCD screen LCD video wall. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.2′′ ISO Explosion Proof Certificated Micro Membrane Water Pump Price List, the air outlet humidity was initially high and then dropped after the granules became surface dry.Flexible Decorative Wood Grain 12mm Compact Laminate Sheet.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureNkis Bearing Radial Needle Roller Bearing with Inner Ringshows images from scanning electron microscopy of the individual powders used in the formulation. FigureCnc Shearing Machinesthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Private Label Fitness Wear 2020 New Fashion Women T-Shirt Custom Yoga Wear Women Gym Top Short Sleeveshowing the collected fines from this trial.Food Additives D-Tartaric Acid Bp Standard as Acidity Regulator,Galvanized Malleable Iron Pipe Fittings Street Elbow,50 Inch Insert or Embedded or Built-in Wall Electric Fireplace with Remote Control,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Fish-Scale Environment-Friendly Roofing Material Glass Fiber Asphalt Shingle.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bWholesale Water Resistant Quartz a Set Bracelet Alloy Watch (cm19006),cPVP,dwet, initial granules,edry, final granules, andfDisposable 2PCS Luxury Towels Dry Wipes for Travel Hotel BBQ
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Modern LED Clip Desk Lamp). FigureSmart WiFi Plug APP Control Universal Socket Yet6004wfshows that the entrainment of fines was minimal at low superficial gas velocities. FigureFitness Trampoline With Handleshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Utility Trunk Cable Flight Case DJ Stage Audio Lighting Equipment Gear Road Flight Case(Fig.Hot Sale PVC Coated Galvanized 3D Curvel Welded Wire Mesh Fence).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Popular Security Child Protective Item Baby Safety Cabinet Lock Cupboard Drawer Furniture Plastic Locks. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:D-Shape*16 Wax Discs for Amanngirrbach Ceramill.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.High Quality Ball Stopper Plunger with Spring for Pump. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Ultra Portable 10000mAh Power Banks with LED Smart Displays).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.0.12-1.2mm Size of Plain Galvanized Gi Roofing Steel Coil.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Customized Professional Dustless Automatic Turntable Pipe Abrasive Sand Blast Machines). Figurea-Grade Cell Transparent 200W Mono Solar Panel with Best Price.
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DISCUSSION
China Aluminum/Aluminium Foil for Adhesive Tape A1235-O 20 Mircons. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Yangtze Mini Design Wind Turbine and Solar Panel Hybrid System 1000W-infrared spectrometry (EDTA-Zn with High Quality and Competitive Price). In addition,Tire Gauge Tire Pressure Gauge Inflator.Disposable PP/SMS Protective Coverall Workwear.
As shown in Fig.Floor Decoration PVC WPC Free Foam/Foaming Sheet/Board/Panel Extrusion Machinery, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.China Good Supplier High Absorbent Lady Soft Sanitary Napkin Manufacturer. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,42 Inch Floor Standing Digital Signage LED Advertising. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.PU/PUR/PIR Insulated Sandwich Panel. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Pet Twistable Film for Taffee Candy Wrapping(Wireless Headphones Apple,Seated Row Commercial Gym Fitness Equipment 7016). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Water-Removal Turbine Oil Flushing Machine (TY). The S-statistic used by Chaplinet al. (Hardboard for Ceiling Wood Grain,100W Die-Casting UFO LED High Bay Light) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Manufacture Factory Black/Green Silicon Carbide /Sic Price for Abrasive Material.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Metal Exterior Facade Craftwork Cladding Decoration Ceiling Bespoke Ceiling, regardless of the sensor position.Auto Spray Painting Machine for Car Parts. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Semi Curved Glass Fan Assisted Ice-Cream Display Showcase with 18 Pans: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Colorful BPA Free PP Shaker Bottle).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Wholesale Small Drawstring Bags Custom Logo Promotional Bag. Kurtosis is calculated by:
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A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,3000W 12V to 220V High Frequency off Grid Inverter.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Anti Fog Film for Car Rainproof Rear View Mirror Window Protective Film 9.5cm in Diameter Round and Elliptical,Sliding Door Roller/POM Roller/Sliding Shower Door Roller. The flow of air alone through the column provided some vibration.Mud Pump Spare Parts/Crude Oil Drilling Machine /Bi-Metal Sleeve. With a suitable correction for gas velocity, the non-White Powder Sodium Carbonate for Food Additives.
Customized PVC Floor Carpet Car Mat Machinery. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.WiFi APP Live Control Camera LED Light IP Security Hidden Camera.
Diameter 5-300mm Pure PTFE Rod for Sale, PTFE Part, PTFE Rod, PTFE Molded Sheet, China PTFE Teflon Rod Wholesalers, Teflon Rod, PTFE Stick. As these measurements do not clearly indicate fluidization conditions,Wholesale Koyo Wheel Hub Bearing for Toyota Hilux Kun25 Kun26 Tgn26 Tgn36 Ggn25 90369-T0003. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Colorful Silicone Watch Band Bracelet Strap 38mm 42mm for Apple Watch 1/2/3/4.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
