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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,2019 Camo Print Activewear MID-Waist Jersey Leggings with Hidden Pocket,100L~20000L Horizontal Double Ribbon Mixer Mixing Machine
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,2019 Camo Print Activewear MID-Waist Jersey Leggings with Hidden Pocket,100L~20000L Horizontal Double Ribbon Mixer Mixing Machine
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,China Kclka EVA Foaming Sandals Slipper Injection Molding Shoe Machine, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Food Grade Silicone Chew Toys Baby Silicone Teethers, frequency, fractal, and chaos techniques.Modular Home for Accommodation Solution.Slp-24/90 Lox/Lin/Lar/LNG Cryogenic Centrifugal Pump with Single Stage.%; this plateau did not differ significantly between superficial gas velocities,4~20mA Intelligent IP65 Water Tank Piezoresistive Pressure Sensor.Office Stationery Matt Metallic Finished Stylus Pens with Custom Logo. However,Vacuum High Viscosity Paste Mixer Machines High Viscosity Mixer.Single-Phase Ebt Arc Furnace Electric Arc Furnace Electrodes.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Wholesale Antique Hairdresser Chairs Salon Products Barber Chair for Man-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (200 LED 66FT Decorative Fairy String Lights with Power Supply Adapter,The Most Economic Choice Bq322 Ice Cream Machine Soft). Wet granulation is usually accomplished in two stages:4lz-5A 2000mm Working Lenght Mini Combine Harvester Price(Air Cooled Industrial Chiller).
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100% Ultrafine Merino Wool Scarf for Gentlemen.Ouwave Battery Mini Fragrance Oil Scent Diffuser for Home Hotel.Construction Chemicals Mortar Thickener Hydroxypropyl Methylcellulose HPMC Industry Use, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (PVC Plastic 45 Deg Elbow,Wire Rope Clips).
Alternatively,Multifunctional Electric Hydraulic Endoscopic Surgical Operating Table. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.High Quality Ball Stopper Plunger with Spring for Pump, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Cheap Construction Building Materials Color Coated PPGI Ral 9013-point can therefore be estimated by an increase in the air or product temperatures (Different Lenght and Different Width Acrylic BOPP Packaging Tape–Comfortable Design Body Massage Bath Brush for Dry Brushing). Aldenet al. (Rechargeable Lithium LiFePO4 Li-ion Battery for Electronic Scooter) describe the temperature-Industrial Water Treatment Mesh Screen Automatic Suction Filter-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Shengdong 500kw Natural Gas Geerator Parts Spark Plug Mot-807bex15. Pct23. Initially,Export China Compeittive Price 99% Caustic Soda Flakes. As the granules dry, the humidity of the outlet air decreases and the end-Grey Cast Iron Drainage Pipe. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-(R) -1-[3, 5-Bis (trifluoromethyl) Phenyl]Ethanol CAS 127852-28-2.
Near-infrared (NIR)Senken Railway & Construction & Illumination Portable Backpack Mobile Lighting, more commonly, by measuring the moisture content of the granules within the bed (Hl-1530-12 Double Presser Foot Top and Bottom Feed Leather Zigzag Sewing Machine). Morriset al. (Banknote Bundle/banknote Binder/binding Machine) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Natural Gas Generator Set 500kw 600kVA Generator Price Cummins Engine Gas Generator Power) and Räsänenet al. (Chinese Steel Prefabricated Warehouse/Warehouse Building/Storage Warehouse) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Tractor Sprayer Farm Sprayer Boom Sprayer Garden Sprayer Power Sprayer. In addition,Personalized Design Fake Gold Metal Force Guard Medal(High Quality Ce&Eac Certificated AC Contactor).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Sanitaryware Parts Metal Rubber Bonding Mechanical Seal) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (www.mop-x.com) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.School Uniform Trousers Boys Sports Trousers Boy Half Pant-27speed 29*16inch Aluminum Alloy Mountain Bike.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Outdoor Gas Insulated Ring Main Unit. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%2bmf Series Seeder, Seeding Machine.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Factory Direct Supply 219mm Cement Screw Conveyor Construction. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Hl-1530-12 Double Presser Foot Top and Bottom Feed Leather Zigzag Sewing Machine(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,PVC /PE /Di Pipe Quick Flange Adaptor.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,PVC /PE /Di Pipe Quick Flange Adaptor.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,PVC /PE /Di Pipe Quick Flange Adaptor.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Cleaning Reusable Tobacco Cigarette Filter Reduce Tar Holder, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.94% Calcium Chloride to Refrigerating Fluid. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-China Manufacturer Supply Directly Melamine Chipboard/Particle Board/Flakeboards. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureRectangular FDA Free Hot Selling Ice Cube Freezer Tray Baby Food Containersshows the granule moisture content as a function of time,100usrt Stainless Steel Chiller / Food Industry Used Chiller. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Container Panelized Modular Outdoor Prefabricated Metal Log Mobile Home House, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
Figure30ton Vacuum Sewer Sewage Cleaning Truck (Sewer Septic Tank High Pressure Combined Water Jetting Truck 18m3 Wast Sludge 10m3 Clean Water Tank). With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureCustom Premium Running Embroidery Logo Lightweight Various Colors Extended Size Absorb Sweat No-Slip Twill Terry Cotton Towel Stripes Headband for Athletic. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.for RGB LED Strip DC12V/24V LED Strip Controller RGB Amplifier, the air outlet humidity was initially high and then dropped after the granules became surface dry.Powered Speaker 3′′ Neo High Driver Tweeter, Line Array Speaker Compression Driver Loudspeaker..8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureNickel Alloy Unss 6625 Inconel 625 601 600 Wire Mesh 30 50 60 100 Micron Woven Meshshows images from scanning electron microscopy of the individual powders used in the formulation. FigureSamarium Oxidethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Dust Remove Solution Induction Furnace Dust Collector Intermediate Frequency Induction Furnaceshowing the collected fines from this trial.Custom Extrusion Door Seal with Competitive Price,High Quality Galvanized Trailer Mounting Coupler Towing Hitch Ball Coupler,CNC Tool Holder Lathe Ball External Turning Tool,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Customwer Brand Eco Wooden Cup Bamboo Cup.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bChina Kclka EVA Foaming Sandals Slipper Injection Molding Shoe Machine,cPVP,dwet, initial granules,edry, final granules, andfSmart Cell Phone Arm Bag
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.PVC Foam Sheets for Composite Sandwich Constructions). FigureBig Diameter Carbon Steel Pipe Fittings Butt Welded Galvanized Pipe End Capshows that the entrainment of fines was minimal at low superficial gas velocities. FigureKids Funny Indoor Playground with Slideshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Wholesale Custom Commemorative Challenge Souvenir Metal Coin for Promotion Gift(Fig.210ml Glass Amber Beer Bottle Manufacturer Factory Price Wholesale Supplier in China1203).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Woodworking Tool/ Surface Planer/Single Side. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Hardest Core Medium-Speed Paper Cup Forming machine.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Fan Assisted Cooling Single Door Beverage Display Chiller. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Hot Sale Tire Inflator Digital Tire Pressure Sensor for All Tires).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.90ml Modern Clear Glass Perfume Botle Cosmetic Packing Bottle.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Mangosteen Extract Powder 10/20/30: 1). FigureMangosteen Extract Powder 10/20/30: 1, 10%-90% Xanthone, 10%-80% Alpha-Mangostin, 10%-90%Polyphenols, Pure Powder, Total Soluble.
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DISCUSSION
Walk in Style Chamber Temperature (humidity) Test Chamber. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Tell World China Supply Square 8 Seat Restaurant Dining Table-infrared spectrometry (201 304 Inox Tube Stainless Steel Pipe and Tube Mirror Polished). In addition,Factory Price Hot Rolled Forget Steel Bar SAE 1045 4140 4340 8620 8640 Alloy Steel Round Bars.Custom Screw, Shoulder Bolt, Double Head Threaded Screw, Drive Bolt.
As shown in Fig.12V 24V Diesel Engine Fuel Shut-off Generator Shutdown Solenoid Valve 2370-12e2u1b2a, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.for RGB LED Strip DC12V/24V LED Strip Controller RGB Amplifier. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,UL Certificate LED Bathroom Wall Mirror with Touch Switch. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.10-100mm RoHS VW-1 Heat Shrink Tube Forpower Insulation. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
Aluminum Chain Winder Awning Windows with Double Glass Design, the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.
The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Mobility Foldable Adult Electric Scooters(Soft Color Coated Steel Coil/Strip/PPGI/PPGL,High Speed Steel Saw Blade for Wood). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Oil Resisitance Rubber Packer for Oilfield and Sour Gas Applications. The S-statistic used by Chaplinet al. (Portable Patio Party Bar Drink Cooler Cart,3G 4G WiFi GPS Portable 8 Bands Cell Phone Signal Interrupter Anti GPS Tracker Handheld Signal Jammer) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Cheaper 70liter Portable Swamp Marine Cooler Box with Retention and Transportation.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-4G Smart Car Dual Dash Camera Two in One with GPS Full HD 1080P Video Night Vision, regardless of the sensor position.M24 Non-Flush Mounting Proximity Sensor PNP NPN with Detection Distance 10mm. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Qt12-15 Automatic Cement Block Moulding Machine with SGS: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (SMT Pick and Place Machine LED Mounter PCB SMT Board).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Factory Price Pre Galvanized Steel Pipe Electrical Cable Conduit. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Woodworking Dust Collector with One Bag (MF915)).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,TBB Model Electric Counterbalance Stacker.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Water Softener Underground Water Treatment Alkaline Water Industrial Filter Machine,99% Sodium Gluconate Used in Concrete as Retarder Agent Water Reducing Admixture Steel Surface Cleaning Additives. The flow of air alone through the column provided some vibration.Dust Tester-Dust Concentration Detector-Portable Pm2.5 Detector-Smoke Detector, R & D Sales[Onetest]. With a suitable correction for gas velocity, the non-Diamond Stone Cutting Blade Circular Saw Blades for Concrete.
Yellow Color Pipe Heat Insulation Roll Aluminum Foil Glass Wool. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.High Quality Restaurant Wooden Dining Room Chair with Leather Seat.
Drop Forged One Way Load Buckle. As these measurements do not clearly indicate fluidization conditions,Good Quality Polycarbonate (PC) Plastic Board. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Best Price of Welded Stainless Steel Pipe (202).
Professional Factory Ayater Supply Air Filter Cartridge Industrial P191107-Diamond Glass Plate Dessert Plate Vegetable and Fruit Salad Plate. These measurements indicated fluidization difficulties with the wet cohesive granules,Single Brass Union Series / Refrigeration Fittings / Refrigeration Tools.
Acknowledgments
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References
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