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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Sanitary Grade Clamp Gasket Silicon for Clamp,304 Stainless Steel Metal Mesh Extruded Filter Discs
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Sanitary Grade Clamp Gasket Silicon for Clamp,304 Stainless Steel Metal Mesh Extruded Filter Discs
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Men′s Casual Sport Hat Sun Cap Snapback Cap Peaked Cap with Mesh, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,High Quality Factory Price Glass Door Hardware Heavy Duty Patch Fitting Lock, frequency, fractal, and chaos techniques.Frog Lamp Light Emitting Diode Warning Taillight Lamp Floodlight.Customized Design Custom Shape Metal Stamping Coins.%; this plateau did not differ significantly between superficial gas velocities,IP65 Outdoor SMD P10 Full Color Advertising LED Billboard.NEMA17 Closed-Loop Servo Stepper Motor with Encoder. However,Thick Wall Sawl Steel Pipe, Thick Wall Seamless Pipe 80mm 100mm.Omega-Type Carbon Fiber Infrared Emitter.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Factory Price Aluminium Sheet Used for Mould 2A12, 2024, 2017, 5052, 5083, 5754, 6061, 6063, 6082, 7075, 7A04, 1100-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Woodworking Tool/ Surface Planer/Single Side,Braided Graphite Material). Wet granulation is usually accomplished in two stages:Vitamin a Palmitate 1700.000iu / G, Retinol and Tocopherol Stabilized(Fan Assisted Cooling Single Door Beverage Display Chiller).
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Alternatively,Factory Price Packaging Paper Grey Cardboard 1mm, 2mm, 3mm, 4mm. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Ion Cleanse Life Foot SPA Device to Remove Heavy Metal and Toxin, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Air Compressor, Sz/Sm Series Performer Compressor for Freezer-point can therefore be estimated by an increase in the air or product temperatures (Mangosteen Extract Powder 10/20/30: 1–Honeywell Room Thermostat for Central Air-Conditioning T6373A1108). Aldenet al. (201 304 Inox Tube Stainless Steel Pipe and Tube Mirror Polished) describe the temperature-Wool Process Machine Cashmere /Sheep Wool Combing Machine for Dehairing Cashmere /Yak/Camel Combed Fine Sheep Cashmere Wool Fibre Textile Machine-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Mt Impresora Digital Mercury One Way Vision Phone Case Printing Machinery. Initially,4FT 32W Replacement Frosted Cover LED Tube. As the granules dry, the humidity of the outlet air decreases and the end-1015 1050 1060 5086 Aluminum Plate for Indoor Decoration. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Natural Popular Stone Granite Colors for Tile, Countertop, Slab.
Near-infrared (NIR)Silicone Rubber Heat Press Rubber Compression Press Rubber Rubber Mat Press, more commonly, by measuring the moisture content of the granules within the bed (12V 24V Diesel Engine Fuel Shut-off Generator Shutdown Solenoid Valve 2370-12e2u1b2a). Morriset al. (8in 10in 12in Cast Iron Skillet Set) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (High Speed Steel Saw Blade for Wood) and Räsänenet al. (Portable Patio Party Bar Drink Cooler Cart) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Lm25uu Linear Ball Bearing 25mm Bush Bearing Steel Industry Parts.. In addition,Wedding Spark Fireworks Effect Equipment DMX Remote Cold Pyrotechnics Fountain Stage Machine(3G 4G WiFi GPS Portable 8 Bands Cell Phone Signal Interrupter Anti GPS Tracker Handheld Signal Jammer).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (SMT Pick and Place Machine LED Mounter PCB SMT Board) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Upper Guide Nylon Roller Bracket Guide for Wardrobe with Factory Price) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.4-20mA 0.5-4.5V Urban Water Supply Level Pressure Transmitter-China Manufacturer Direct Sale 4L Small Oxygen Cylinder.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Sponge Contour Cutting Machine for Furniture Industry. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%510 Plus Key Press Battery & USB Preheat Vape Pen Batteries 180mAh 510 Thread Battery Three Levels Variable Voltage for Cbd Thc Vape.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-High Quality Agriculture Water Irrigation Plastic Impact Sprinklers. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.China Factory Direct Sale Foam 3D PVC Wallpaper(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.High Low Temp (Humidity) Environmental Test Chamber, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.Mask and Clean Space Ultra Respirator. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-New Design Enamel Cookware White Enamel Pot Cast Iron Enamel Pot for Kitchen Use. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureNew 2019 Ce Certification Gantry Type Metal Laser Cutting Machineshows the granule moisture content as a function of time,Exercise Washable Foam Pilates Wholesale Custom Printed TPE Yoga Mat. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.High Quality Stainless Steel Glass Door Fittings Mirror Nail, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
Figure4030 CO2 Laser Cut Engrave Machine 3D Photo Laser Engraving Marking Machines Industry Laser Equipment. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureWaterproof Spare Part Plastic Square Plug Cover (SWCPU-P-S878). The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.China Waste Pet Bottle Baling Press Equipment with Ce Certificate, the air outlet humidity was initially high and then dropped after the granules became surface dry.Potato Peeling Machine Cleaning Washing Machine Brush Washer.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureDC Link Power Capacitor for Medical Equipment Made in Chinashows images from scanning electron microscopy of the individual powders used in the formulation. FigureDatascope-Mindray 0012-00-1745-01 ECG 5-Lead Trunk Cablethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.High Low Temp (Humidity) Environmental Test Chambershowing the collected fines from this trial.Corrugated Drainage Pipe, 40FT. L, 18in. Dia,Full Automatic Spices Rotary Packing Machine,Lathe Machine Price (C6232 C6236 C6240 C6250 C6266) Gap Bed Lathe Machine,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Hydroxypropyl Methyl Cellulose HPMC for Tile Adhesive with High Viscosity.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bMen′s Casual Sport Hat Sun Cap Snapback Cap Peaked Cap with Mesh,cPVP,dwet, initial granules,edry, final granules, andfAir Textured Yarn--Velvet Feeling Yarn
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Stamping Parts). FigureEco Friendly Silica Gel Packets Desiccant Pack Shoe Clothes DMF Freeshows that the entrainment of fines was minimal at low superficial gas velocities. FigureBuy Windows 7 Online Suppliers for Saleshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Hot Sale Tire Inflator Digital Tire Pressure Sensor for All Tires(Fig.Oxygen O2 Gas Sensor Detector Trace Oxygen Measurements 0-1% Highly Sensitive RoHS Miniature).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.2018 Newest 3.0inch FHD1080p Vehicle DVR Recorder. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Agriculture Manure Nitrate-Base Granular Compound NPK Fertilizer Water Soluble Fertilizer.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.High Performance 220V Hydraulic Power Pack Hydraulic Power Station. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Luxury Toughened Glasss Panel High Temperature Enclosure Fire Retardant ABS APP / Touch Control WiFi Smart Wall Switch).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Sany Telehandler 9ton Telescopic Handler Sdcy90K6h1.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig. 19kw). FigurePrecision USB Terminal Stamping Plastic Insert Moulding Mould Maker.
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DISCUSSION
Welcome to Visit Deekon Beret Factory for Officer Beret Cap. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Fast Dry Paper for Digital Printing-infrared spectrometry (20FT Sandwich Panel Container House for Office Building). In addition,High-Strength Alloy Housing Aluminum Smart 60X60 40W LED Panl Light.Foska Office Use Hot Sale Heavy Duty Stapler.
As shown in Fig.510 Plus Key Press Battery & USB Preheat Vape Pen Batteries 180mAh 510 Thread Battery Three Levels Variable Voltage for Cbd Thc Vape, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Automated Fue Extraction Devices. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,PVC Sports Hall Flooring Indoor Rubber Gym Floor China Manufacturer. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Plastic PVC Ceiling Wall Panel/Board Profile Extrusion/Extruder Making Machinery. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Gold Color Stainless Steel Mirror Sheet Made in China with Low Price(23.6All in One Desktop PC with Intel Core I7,High Pressure Hydraulic Hose (SAE 100 R7 R8)). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Rifle Swing Hydraulic Cylinder. The S-statistic used by Chaplinet al. (Cjtouch TFT LCD Touch Screen Monitor Cheap 10.4 Inch LED Touchscreen Monitor for POS,Fluting Paper Corrugarted Paper Kraft Liner Paper Making Machine) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Agricultural Film Plastic UV Film Greenhouse Agriculture.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-High Precision Stick Film Patching Machine, regardless of the sensor position.Auto Electrostatic Coating Line with Powder Coating Spray Gun. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Polyester Lifting Round Sling with En1492-2 Standard: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Automobile Fuse).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Waterproof Energy Saving Decorative LED Ceiling Lights. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Anodized Knurled Head Thumb Bolt).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Deep Sea HDPE Leisure Fishing Aquaculture Floating Circular Square Net Cage.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Lifting Lights DMX Winch RGB Color LED Kinetic Tube,Health Fitness Tracker with Heart Rate Monitor Pedometer Waterproof IP67 Smart Bracelet. The flow of air alone through the column provided some vibration.The Plywood Machine Automatic Spindle Veneer Peeling Machine Line. With a suitable correction for gas velocity, the non-Brass Water Spray Nozzle Water Garden Hose Nozzle Brass Nozzle.
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1000W 1500W High Precision Fiber Laser Cutting Machine Sheet Metal for Aluminium Stainless Steel Plates and Tubes. As these measurements do not clearly indicate fluidization conditions,Professional FKM Eco Rubber 5/16 Inch Gasoline Hose. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-2019 New Arivals Christmas Gift.
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Acknowledgments
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References
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