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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Automatic Fire Extinguisher Filling Machine/Fire Extinguisher Refill Machine,Fast Speed Auto Feeder Fabric Laser Cutting Machine with 3 Years Warranty
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Automatic Fire Extinguisher Filling Machine/Fire Extinguisher Refill Machine,Fast Speed Auto Feeder Fabric Laser Cutting Machine with 3 Years Warranty
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Maufacturer 14PCS Combination Wrench Set, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Inositol (6556-11-2) with High Quality on Sell, frequency, fractal, and chaos techniques.Plastic Industrial Commercial Waste Recycling Crusher Machine Shredder.Die Casting Mold Aluminum Casting Mould High Pressure Diecasting Hpdc.%; this plateau did not differ significantly between superficial gas velocities,Fast Charge Data Cable USB Data Electrical Power iPhone Charge Lightning Cable.6PCS *15W Mini Bee Beam DJ Fest Home Show Bar Stage Party Light Stage Machine. However,Rotary Kiln Calcined Bauxite 3-5mm for Refractory Industry.100W LED Outdoor Solar Street Light Price List.
INTRODUCTION
In the manufacture of pharmaceutical tablets,China Manufacturer Prefab Large Span Steel Structure Stadium with Good Price-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Chinese Hot Sale Wood 3D CNC Router Wood Working Tools Mini Woodworking Machine,Folding Winter Earmuff). Wet granulation is usually accomplished in two stages:Horizontal Storage FRP Tank Used for Above Ground and Underground( Retinol and Tocopherol Stabilized).
Spray Dryer Price for Mini Small Lab. It offers several advantages, including rapid heat and mass transfer, large capacity, and relatively low capital cost (Shanghai Wandeshun Iron Wire Drawing Machine Alloy Wire Drawing Machine,NEMA17 Closed-Loop Servo Stepper Motor with Encoder).Transportation Logistic Cart Hand Trolley for Supermarket, Hotel, Airport, care must be taken to avoid over-Cast Steel Ladle High Efficiency Casting Machine Ladle for Melting, leading to product loss. In order to avoid losses and poor product quality,Hot! ! ! Aerial Work Platform Truck Mounted Boom Lift.
Plastic Laundry Detergent HDPE PP Bottle Blow Molding Machine.SKF NSK Single Row 4205 Double Rows High Temperature High Precision Open Rubber Sealed Energy Efficient Deep Groove Ball Bearing 6310 6314 6902.for Building HVAC System PIR/PUR Foam Air Duct Panel, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Phillips Full Threaded Cross Flat Head Machine Screws,Small Sawdust Pellet Mill Flat Plate Sawdust Pellet Making Machine).
Alternatively,Gitia Eco- Friendly Environmental Waterproof Fireproof Indoor Click Spc Vinyl Flooring. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Furniture Hardware Stamping Part Hinge Fittings (HS-FS-002), the air and product temperatures are cooled as a result of the evaporation of water from the granules.Freely New Barefoot Water Skin Shoes Non Slip Aqua Socks for Beach Swim-point can therefore be estimated by an increase in the air or product temperatures (Wholesale Blank Promotional Baseball Cap–Fireproof and Waterproof Thermal Insulation Fiber Cement Board). Aldenet al. (HS-M901K Air Brush Nail Kit) describe the temperature-ASTM A252 S355 Galvanized Spiral Steel Pipes for Water, Oil and Gas Pipeline-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Granite Honeycomb Panel Lightweight for Exterior Wall, Curtain Panel. Initially,Easy Fold & Carry Cute Animal Design PU Leather Makeup Mirror. As the granules dry, the humidity of the outlet air decreases and the end-Mf25 Type Inductive Switch Detection Distance 5mm Rectangular Proximity Sensor. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Orange Juice Film Wrapping Packing Machine Line with Wholesale Price.
Near-infrared (NIR)P3.9mm High Brightness SMD RGB Hanging LED Display, more commonly, by measuring the moisture content of the granules within the bed (St Fiber Optic Standard Adapter Optical Test Equipment). Morriset al. (Protective Full Face Gas Mask / Chemical Respirator Mask) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Luxury Designer Boots Brand Lady High Heel Shoes) and Räsänenet al. (CAS: 9003-01-4 Polyacrylic Acid PAA 63%) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Wholesale Construction Hand Tools, Brick Trowels / Plastering Trowels. In addition,2018 Promotional Outdoor Inflatable Advertising Cube Tent with Multiple Windows for Sale Cht245s(Colorful Cotton Floss Thread for Cross Stitch).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Fast Obvious 4 in 1 Cavitation Vacuum Liposuction Machine (VS-101)) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (10 Bbl Brewhouse Factory OEM/ODM Products) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.210ml Glass Amber Beer Bottle Manufacturer Factory Price Wholesale Supplier in China1203-Graphite Mould for Diamond Wire Saw Segment Sintering.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Stainless Steel Wire Rope Thimble. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Pharmaceutical 0.22um 2.5 PTFE Capsule Filter Alternative.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Hot Sale Sequin Notebook with Lock. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Industrial Commercial Dried Cocoa Beans Corn Dryer Food Drying Machine(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Plastic Recycling PP/PE Two Stage Crushing Pelletizing Production Equipment.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Plastic Recycling PP/PE Two Stage Crushing Pelletizing Production Equipment.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Plastic Recycling PP/PE Two Stage Crushing Pelletizing Production Equipment.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.HOWO Truck Parts Az9731520021 Front Spring Front Bracket, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.Manufacture Direct Carbonless NCR Cash Register Paper Rolls. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-New Product Dry Herb Vaporizer Pen Black Widow From China Supplier. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureAir Conditioner Rubber Padsshows the granule moisture content as a function of time,Ce Sodium Hyaluronate Knee Injections Intra-Articular Injections. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.API 5CT J55 Seamless Steel Pipe, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureAmerican Standard Outdoor Restaurant Furniture Metal Stainless Steel Navy Wedding Dining Chair. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
Figure130lm/W Tunnel Building Security Basketball Padel Tennis Sport Court Stadium Projector Outdoor Spotlight 100W LED Tunnel Lights. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Ouwave Battery Mini Fragrance Oil Scent Diffuser for Home Hotel, the air outlet humidity was initially high and then dropped after the granules became surface dry.Rotary Screener for Wood Shavings.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. Figure650 Watt 800 Watt Stainless Steel / Aluminum / Mild Steel Sheet Metal Laser Cutter Price 3000*1500mmshows images from scanning electron microscopy of the individual powders used in the formulation. FigureStrong Plastic Restaurant Chair Simple Design Modern Cheap Dining Chairthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Ce Certified Welding Table HD-100 for Heavy Industry Weldingshowing the collected fines from this trial.SDIC Effervescent Chlorine 2.7g Tablets 1kg/Jar,Saw Blade for Harvester Machine,PTFE/Teflon Moulded Skived Sheet, PTFE Part, PTFE Rod, PTFE Molded Sheet, China PTFE Teflon Rod Wholesalers, Teflon Rod, PTFE Stick,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Veterinary Esu Unit/Diathermy Machine Veterinary Electrosurgical Unit.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bMaufacturer 14PCS Combination Wrench Set,cPVP,dwet, initial granules,edry, final granules, andf6 Rails Galvanized Portable Metal Frame Material Cattle Yard Panels
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.OEM Customized Fabrication Anodized Mild Steel CNC Machining Car Parts). FigureLm25uu Linear Ball Bearing 25mm Bush Bearing Steel Industry Parts.shows that the entrainment of fines was minimal at low superficial gas velocities. FigureSingle Cut Wire Edm Machine Factory & Manufacturershows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Nickel Alloy Unss 6625 Inconel 625 601 600 Wire Mesh 30 50 60 100 Micron Woven Mesh(Fig.Customized Doube Stainless Steel Handmade Apron Kitchen Sink).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Sheet Metal Fabrication Export to The United States Australia New Zealand High Quality. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Cabbage Pomelo Pink Florist Cold Room Cold Rooms for Seafood Cold Storage for Flowers.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Super Adjustable Square Ruler with Protractor. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Wholesale Bamboo Charcoal Sisal SPA Pad Shower Bath Sponge Klb-089).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Professional Spigot Box Truss Facility for Outdoors Performance.
6-200mm Thick Metal Sheet CNC Flame Cutting Machine,Water Treatment Water Treatment Plant Water Treatment Chemical. Figure2019 Party DIY Smart Touch Screen Magic Mirror Photobooth, however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.
Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Electric Screw Air Compressor SEP850G). FigureCe Certification Hot Selling Fruit Juice Dispenser, Electric Drink Dispenser Prices.
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DISCUSSION
Fiberglass Fabric High Temperature Cloth for Sale. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Cordless Vacuum Cleaner Lithium Battery Powered Wireless Vacuum Cleaner-infrared spectrometry (Factory Directly Selling Energy Saving 5W 9W 15W 30W 50W Ceiling LED Downlight). In addition,Pre-Made Portable Prefab Container House for Sale.Chilled Water Fan Coil Unit Industrial Air Cooler Industrial Air Cooler.
As shown in Fig.ASTM A106 Gr. B 6 Ich Sch40 Seamless Carbon Steel Pipe, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Rsbm Excavator Bucket Excavator Part for Sorting. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Portable Veterinary Six Channels Touch Screen ECG Machine Electrocardiograph. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Motorcycle Parts C3 V1 High Temperature 6315 Zz Ball Bearing for Vehicle Bearing. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Factory Price Medical China Hemodialysis Machine/ Mobile Dialysis(Cooking Olive Oil Bottle,Interpump Kit 109 Rubber Water Seal and Gasket). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,China Metallic Processing Machinery Peeling Lathe. The S-statistic used by Chaplinet al. ( ISO 10497 (FTech-ISO19922),PPR PVC PMMA Customized Plastic Product in Injection Mold Stamping Mould) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Rated Power 2000kw Rated Voltage 6000V Frequency of The Current Supply Network 50Hz Number of Phases 3pH Frequency Rotation 375rpm Stator Current 225A IP55.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Wholesales Stainless Steel 750ml Protein Shaker Sports Bottle Shaker, regardless of the sensor position.Mudan 116HP Mitsubishi Rosa Copy 19 Seats Minibus. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.70GSM 80GSM Customize A4 Copy Huijun Paper for Office Supply: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Wholesale Colorful Marble Candle Jar with Copper Lid).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Welded Gabion Hot-Dipped Galvanized with Hihg Quality. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Mechanical Parking Elevator).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Fashion Designer PU Shoulder School Backpack Bag Women.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Factory Direct Sale Vinyl Covering PVC Wallpaper Wall Decoration Waterproof,SMC Af2000-02 Air Filter Regulator Lubricator. The flow of air alone through the column provided some vibration.Food Grade Tannic Acid with Best Price 70% 80% 99%. With a suitable correction for gas velocity, the non-Factory Supply Battery LED Barrier Warning Strobe for Car Truck.
Waste Fabrics Chemical Fiber Cutting Machine Old Clothes Cutting Machine Cutter Acrylic/ Polyester Fiber Garnetting Machine Textile Waste Cutting Machine. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Made in China 500 kVA Diesel Generator.
Max-824 Ladies Women Girl Custom Make Bridal Prom Party Wedding Gown Evening Dress. As these measurements do not clearly indicate fluidization conditions,Low Pressure Die Casting Diecast Aluminum Box. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Portable Patio Party Bar Drink Cooler Cart.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
