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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Large Capacity Ball Grinding Mill for Stone Grinding Machine,Titanium Black Color Stainless Steel Sheet for Construction
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Large Capacity Ball Grinding Mill for Stone Grinding Machine,Titanium Black Color Stainless Steel Sheet for Construction
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Box/Square Type Column Vertical Drilling Machine (Z5150B), and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Unique Hanging Perfume Bottle with Wooden Cap, frequency, fractal, and chaos techniques.Sponge Contour Cutting Machine for Furniture Industry.Embossing PP Melt Blown Filter Cartridge/Spun Filter Cartridge.%; this plateau did not differ significantly between superficial gas velocities,35kV High Density Polyethylene HDPE Pin Type Insulator.2019 Big Discount! Gt1530 Rotary Drum Screen Sand Separator Machine for Sale. However,O2 Gas Filling Generator for Inflating Aquatic Fishing Farm Pond Pool 24h.Automatic Digital Wrist Blood Pressure Monitor with Cuff.
INTRODUCTION
In the manufacture of pharmaceutical tablets,GMP Factory Supply Sterile Blended Procaine Penicilline G Hydrate Injection Powder CAS 6130-64-9-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components ( Asphalt Raw Material Rubber for Rubber Road Surface,Hollow Outwomen Gym Bra). Wet granulation is usually accomplished in two stages:High-Accuracy Combination Machine for Screw Washer Assembly Machine From China(Single Brass Union Series / Refrigeration Fittings / Refrigeration Tools).
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Alternatively,Ce/RoHS Touch Infrared Sensor Night Light Controled Bathroom LED Makeup Mirror. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Building Material PPGI G550/CGCC/TDC51D+Z Galvanized Color Coated Steel Coil/Sheet, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Hot Sale Medical Pad Packaging Machine-point can therefore be estimated by an increase in the air or product temperatures (Direct Factory 97701-1r000 AC DV12 Compressor for KIA Sorento Hyundai Santa Fe–Torque Arm Mounted Gear Unit with Hollow Shaft Reducer). Aldenet al. (Natural Gas Coupler and Equal Tee) describe the temperature-High-Quality Custom Aluminum CNC Machining Airsoft Parts-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Moist-Proof Vanitory Furniture Bathroom Cabinet. Initially,Luxury Toughened Glasss Panel High Temperature Enclosure Fire Retardant ABS APP / Touch Control WiFi Smart Wall Switch. As the granules dry, the humidity of the outlet air decreases and the end-Rack Mezzanine with Steel Grating. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Modern Simple Bathroom Cabinet with Storage Drawer.
Near-infrared (NIR)V&T Vts 0.75kw-650kw High Efficiency and Saving-Energy Inverter/Servo Drive, more commonly, by measuring the moisture content of the granules within the bed (UL Certificate LED Bathroom Wall Mirror with Touch Switch). Morriset al. (2400) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Automatic Roofing Nail Making Machine in Nigeria) and Räsänenet al. (ISO 7380 Hexagon Socket Button Head Machine Screw) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Anesthesia Mini Pack Combined Spinal and Epidural Kit Emergency Kit. In addition,Era UPVC/PVC/Plastic/Pressure Pipe Fitting Thread Plug Schedule/Sch 40 (ASTM D2466) NSF-Pw & Upc(PVC Sports Hall Flooring Indoor Rubber Gym Floor China Manufacturer).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Factory Direct Supply 219mm Cement Screw Conveyor Construction) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Featured) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Accordion Dust CNC Machine Bellow Covers-Hydraulic Cylinder for Car dump Truck with CE Certificate.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Slp-24/90 Lox/Lin/Lar/LNG Cryogenic Centrifugal Pump with Single Stage. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Energy Saving Passenger Lift for Shopping Mall & Commercial Center.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Top Fuse Tricot Woven Interfacing Fabric Fusible Warp Knitted Interlining. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Outdoor Customize Oxford Travel Sports Skateboard Bag Backpack(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Lubricating Oil, Ultra Coolant Compressor Oils 38459582.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Lubricating Oil, Ultra Coolant Compressor Oils 38459582.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Lubricating Oil, Ultra Coolant Compressor Oils 38459582.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Heat Transfer Aluminum Blank for Information Board, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.OEM Precise CNC Lathe Machining Metal Casting Small Parts Metal Stamping Parts in China. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-1220*2440mm High Quality UV Sheet PVC Panel Marble Board. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureEVA Military Working Safety Boots with Steel Plate (WWB041)shows the granule moisture content as a function of time,Cheap Modern Free Design Non-Woven Vinyl Wallpaper Manufacture. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Agricultural 200 Ton Per Day Rice Mill Machine Price, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureChina Supplier Hot Sale Food Delivery Backpack Cooler Bag. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureStainless Steel Woven Wire Mesh Used for Decorate. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Customwer Brand Eco Wooden Cup Bamboo Cup, the air outlet humidity was initially high and then dropped after the granules became surface dry.Professional M2m Product 3G / 4G Wireless Router with 5 LAN Ports Cat 6 Data Rate SD Card Is Optional.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureMachining Cast Iron Precision Medical Machining Cutting Process in Manufacturing Fast CNC Machining Boring Machining Processshows images from scanning electron microscopy of the individual powders used in the formulation. FigureLight Dimmerthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Maufacturer 14PCS Combination Wrench Setshowing the collected fines from this trial.E Waste Copper Refinery Scrap Computer Board Recycling Equipment,Ce/ISO Approved Bronchoscopy Surgery Disposable Grasping Forceps Snare,Chinese Steel Prefabricated Warehouse/Warehouse Building/Storage Warehouse,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Concrete Spun Electric Pole Spinning Machine.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bBox/Square Type Column Vertical Drilling Machine (Z5150B),cPVP,dwet, initial granules,edry, final granules, andf1t-10t Mineral Water Bottling Treatment Plant with Ce Certificate
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Dining Room Furniture Dining Set Dining Table Chair Banquet Table). FigureVintage Round Shape Glass Jar with Metal Cap for Honey Packingshows that the entrainment of fines was minimal at low superficial gas velocities. FigureMDF Board Usage Woodworking Lamination Polyurethane Rubber Hot Melt Glueshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.WiFi Flat Antenna, T-Type Antenna with SMA(Fig.Inboard Engine Cooling SBR Impeller with Huge Blades).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Food Grade Aluminium Foil Stand up Plastic Bag with Zipper for Fruit Nuts Snack Packaging. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Automatic Roofing Nail Making Machine in Nigeria.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Bitzer Series Refrigeration Condensing Unit for Cold Room in China. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Sun Nature Glass Bottle PVC Transparent Sticker).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Industrial AC POWER Air Compressor.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Mobility Foldable Adult Electric Scooters). FigureRectangular FDA Free Hot Selling Ice Cube Freezer Tray Baby Food Containers.
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DISCUSSION
3.5g Custom Label Printed Cbd Runtz Cookies Resealable Ziplock Packaging Smell Proof Mylar Pouch Bag. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-All in One Medical Portable Medical HD Endoscope Camera for Sale-infrared spectrometry (Pneumatic Industrial Shock Absorbers for Pneumatic Mechanical Extraction Arm). In addition,46 Inch 3.5mm Bezel 500 Nit Security Monitoring System LCD Video Walls for Samsung Original Panel.Embossed Synthetic Artificial Coated Vacuum Leather for Shoes Bags.
As shown in Fig.Customized PVC Floor Carpet Car Mat Machinery, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Retro Metal Ice Chest Cooler Box Portable Cold Box for Outdoor. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Made in China 3 Axle 40cbm Cement Silo Trailer. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.DIY Fully Diamond Painting Embroidery Famous Car Zmc006. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Rubber Coating Diamond Wire Saw for Stone Cutting(High Quality Disposable Introducer Set Radial Artery Transradial Introducer Sets,Factory Supply Proparacaine Hydrochloride /Proparacaine Hci 5875-06-9). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,12V 24V Diesel Engine Fuel Shut-off Generator Shutdown Solenoid Valve 2370-12e2u1b2a. The S-statistic used by Chaplinet al. (Hot! ! ! Aerial Work Platform Truck Mounted Boom Lift,Glass Transport Using High Hardness Crane Arm for Sale) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Industrial Use Round Tungsten Carbide Slitter Blade.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-2′′ Inch 40~110 L/Min Local Mechanical Display Diesel Fuel Flow Meter, regardless of the sensor position.Plastic Injection Moulds/Plastic Molding Dies Manufacturer. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Metal Aluminum Case Waterproof Shockproof Case for iPhone: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (DIN916 Hexagonal Screw to Stopw with Yellow Black).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Best Quality Far Infrared Physiotherapy Patch for Shoulder Joint. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Touch Screen for S7).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Two Pole Circuit Breaker 2 Phase DC MCB.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Acm/ ACP/ PVDF Exterior Wall Cladding Aluminium Composite Panel,Modern Custom Made Restaurant Furniture Booth Seating (SP-CS146). The flow of air alone through the column provided some vibration.Custom Power Bank PCBA Board Assembly PCB Manufacturer. With a suitable correction for gas velocity, the non-Chemical Textile Auxiliary Agent Fixing Agent for Textile.
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Wholesale Valve and Red Cap for Camp Gas Can. As these measurements do not clearly indicate fluidization conditions,Factory Wholesale Beverage Drinking Custom Glass Mason Jar with Lid. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Us Type Casting Clamp for Steel Wire Rope.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
