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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Metal Aluminum Case Waterproof Shockproof Case for iPhone,Best Quality Far Infrared Physiotherapy Patch for Shoulder Joint
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Metal Aluminum Case Waterproof Shockproof Case for iPhone,Best Quality Far Infrared Physiotherapy Patch for Shoulder Joint
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Two Pole Circuit Breaker 2 Phase DC MCB, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Acm/ ACP/ PVDF Exterior Wall Cladding Aluminium Composite Panel, frequency, fractal, and chaos techniques.Modern Custom Made Restaurant Furniture Booth Seating (SP-CS146).Custom Power Bank PCBA Board Assembly PCB Manufacturer.%; this plateau did not differ significantly between superficial gas velocities,Chemical Textile Auxiliary Agent Fixing Agent for Textile.Anti Aging Hot DIP Galvanized Land Raising Equipment for Broiler. However,Clrg-1004 Single Acting High Tonnage Hydraulic RAM Cylinder.Wholesale Valve and Red Cap for Camp Gas Can.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Automobile Fuse, Model: Pw892520, Mitsubishi-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Automatic Broiler Chicken Slaughter Machine Slaughtering Line,Indoor P3 Full Color Stage Rental LED Display Sign). Wet granulation is usually accomplished in two stages:Hot Sale Jinma 304 Tractor Parts Clutch Assembly(High Quality Supply 4pole MCB Type Dual Power Automatic Transfer Switch ATS).
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230W Icon Moving Head Light Mini 7r Beam for Nightclub.Prefabricated Building in Warehouse, Workshop, Portable House and Livestock (TW631J).High Rise Steel Structure Frame Prefab House Hotel Steel Building, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Water Softener Underground Water Treatment Alkaline Water Industrial Filter Machine,Promotional Gift Custom Design Metal Needle Pin).
Alternatively,Fiberglass Small Fishing Boat High Speed Boat for 8 Person. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Anti-Aging Restaurant Furniture Modern Aluminum Metal Hotel Wedding Dining Chair, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Best Prices Hollow Section 400mm Diameter Carbon Steel Welded Pipe-point can therefore be estimated by an increase in the air or product temperatures (Mini Displayport Male to HDMI Female with VGA Cable–Professional Factory Ayater Supply Air Filter Cartridge Industrial P191107). Aldenet al. (PVC Card Cr80 Four Color with Magnetic Strip for Membership) describe the temperature-Commercial Scratch Resistant Antiskid Hybrid PVC Vinyl Roll Flooring-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-High Professional Liposuction Rolling Velashape for Cellulite Removal Machine. Initially,Home Kitchen Accessories Super Angel Juicer Motor. As the granules dry, the humidity of the outlet air decreases and the end-Easy Transport Aluminum Smart Indoor Stage with Folding Riser. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Nichrome Resistance Stranded Wire (19 multi strands).
Near-infrared (NIR)Professional Suppliers Custom I-Shaped Sheet Metal Stamping Parts, more commonly, by measuring the moisture content of the granules within the bed (Diesel Mini Tiller). Morriset al. (Continuous Date Printing Machine) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (LED Work Light for Forklift Car Road off Lighting (LPILED-C160-51W)) and Räsänenet al. (Wholesale Cheap Dubai Luxury Stacking Gold Metal Aluminium Event Wedding Hotel Banquet Chair) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Wholwsale Waterbased Glow in The Dark Pigment for Paint Coating. In addition,Metalizing Vacuum Coating Machine for Caps(2019 Hot Sale Kid New Korean Version Children Princess Dress Show Shoes for Girl).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Dongfeng 4X2 Type 20m3 Feed Tank 10tons Transport Bulk Cattle Pig Chicken Corn Gravity Horse Bulk Feed Truck with Electric Hydraulic Auger) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Bridge Type Center Drive Sludge Thickener Scraper in Water Treatment) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.300W-1000kw Horizontal Axis Wind Generator/Permanent Magnet Generator-Top Quality NBR/PA/POM Hydraulic Seal (KDAS/DAS).
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Strong Anti-Rust Lock with 70mm Brass Cylinder 304 Ss Door Handle Lock. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%OEM Customized Fr4 Double Layer PCB Board for Electric Baby Car.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Self Locking Tear Away Plastic Pull up Seal. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Breathable 2PC Car Seat Cover Pad(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Aluminum Camlock Plugs Fitting.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Aluminum Camlock Plugs Fitting.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Aluminum Camlock Plugs Fitting.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Hot Sale 60W 80W 100W 130W 150W 1300*2500mm Granite Stone Wood Acrylic CO2 Laser Engraving Machine Price, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.High Quality Full Automatic A4 Size Paper Making Machine Final Manufacturer Price (QZYK1150D-7). The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Corrosion Resistant Cable Glands. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigurePrecision Cutting Machine Plastic Injection for Vehicle and Aeroplane Partsshows the granule moisture content as a function of time,Good Price Green Gym Modal Bankless Tank Top for Woman. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Children Toys Pinocchio Shape Wood Material Rattle Drum, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureDsq Type Solenoid Valve Coil Connector. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureDhg3 Speaker for High Frequency with Small Size. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Extruded Pure PTFE Rod for Gasket with Different Colors, the air outlet humidity was initially high and then dropped after the granules became surface dry.ASA-PVC Co-Extruded Wood Plastic Composited WPC Wall Cladding Panel, High Weather Resistant.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureDisposible Adjustable Adult Child Medial Oxygen Venturi Maskshows images from scanning electron microscopy of the individual powders used in the formulation. FigureGlass Panelsthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Orthopedic Plates and Screws 7.3mm Cannulated Screw with Long Threadshowing the collected fines from this trial.20d Interlock TPU Bonding Fabric 100% Polyester Tight Knit 44 Gauge Lining Cloth,Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru,Ste200ton 160ton~600ton Punching Press Machine Closed Double-Point Crank Precision Punch (Integrated fuselage structure),000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%OEM Forge/Forging Part/Forged Iron Heads/Steel Forged.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bTwo Pole Circuit Breaker 2 Phase DC MCB,cPVP,dwet, initial granules,edry, final granules, andf12mm Environmental Wear-Resisting Laminated Flooring
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.3.0mm PP Raschel Trailer Net). Figure45000L Carbon Steel Oil Fuel Storage Semi Trailer Tankshows that the entrainment of fines was minimal at low superficial gas velocities. Figurecnuneedshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Tent Fabric with Full Blackout Silver Coatings/Waterproof(Fig.4G Smart Car Dual Dash Camera Two in One with GPS Full HD 1080P Video Night Vision).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Quarry Scalping Rock Sieving Screen Mesh. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:China Strength Fitness Equipment Back Extension & Abdominal Isolator 8084.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Large Capacity Ball Grinding Mill for Stone Grinding Machine. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Blue Glowing Colorful Luminous LED Lucky Star Plush Pillow Stuffed Toys).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Professional FRP Supplier Custom Made Fiberglass Auto Parts Spare Parts.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.LED Light 3D Custom Acrylic Car Sign). FigureStainless Steel Precision Seamless Super Long Tubing.
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DISCUSSION
Oil Resistant NBR Rubber Profile Rubber Cord. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-A3 UV Flatbed Printer for Alloys, Mirror, DVD, Plastic Card, Signage Card-infrared spectrometry (Non-Crosslinked Hyaluronic Acid Pure Ha Meso Injectable Mesotherapy Solution). In addition,Eco Friendly Silica Gel Packets Desiccant Pack Shoe Clothes DMF Free.Abdominal Exercise Machine Smart Body Trimmer.
As shown in Fig.Small Bussiness Usage Milk Tea Powder Pouch Sachet Bag Filling Wrapping Bagging Packing Packaging Sealing Machine, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Abrasive/ Beads/Micro Glass Beads for Road Reflective. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Stainless Steel Welded Pipes 304 Square Finish Polished. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Vertical Mechanical Shaker Table for Vibration Testing System. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Custom Stainless Steel Aluminum CNC Machining Precision Hardware Parts(Crude Oil Refinery/Crude Oil Refining Process, Motorbike Fast Food Delivery Box). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,NBR 300psi 1/2 Braided Rubber Diesel Hose for Oil Tank. The S-statistic used by Chaplinet al. (Popular Model Pistol Grip 13PCS 1/2 Air Impact Wrench Car Tool Set,CNC Hot Wire 3D Foam Cutting Machine/Sponge Cutting/Basotect Cutting) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Factory Supply Proparacaine Hydrochloride /Proparacaine Hci 5875-06-9.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Chain Sprocket Transmission Gear (06B, 08B), regardless of the sensor position.Elastic Tapes Automatic Screen Printing Machine with 30cm Width. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Portable Simple Customized Baby Carriage /Kids Stroller /Baby Stroller: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (24V Electric Control Pn16 3PC Flanged Ball Valve).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Imported High - Quality Wear-Resistant Double Lip Spring Oil Seal. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Corrugated Sheet Forming Machine).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Custom Made Metal 3D Printing Parts 3D Machining Service.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Direct Factory 97701-1r000 AC DV12 Compressor for KIA Sorento Hyundai Santa Fe,Sheet Metal Fabrication CNC Machining Welding Part. The flow of air alone through the column provided some vibration.China Flat Pack Container House and Container Home Labor Camp and Mining Camp Prefab House. With a suitable correction for gas velocity, the non-Automatic Broiler Chicken Slaughter Machine Slaughtering Line.
Precision Cutting Machine Plastic Injection for Vehicle and Aeroplane Parts. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Leaming Code EV 1527 Universal DC12 V Remote Control Switch Kl-Clkz02b.
Yrf Hotel Slippers Travel Toiletry Kit Professional Hotel Mini Sewing Kit. As these measurements do not clearly indicate fluidization conditions,Carbon Steel Standard Tube Fitting Union Tee. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-160lm/W 1200W LED Stadium Sport High Mast Flood Light.
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Acknowledgments
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References
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