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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,CNC Professional High Speed Precision Metal Fiber Laser Cutting Machine with Ipg Laser Source for Carbon/Stainless/Aluminum,25micron Thermal Lamination Film Pet Metalized Film for Laminating Paper
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,CNC Professional High Speed Precision Metal Fiber Laser Cutting Machine with Ipg Laser Source for Carbon/Stainless/Aluminum,25micron Thermal Lamination Film Pet Metalized Film for Laminating Paper
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Large Round Shape Cookie Popcorn Handle Tin Bucket with Lid, Ice Tin Box, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Wholesales Indoor LED Lighting COB Recessed Aluminum 6W IP44 Down Light, frequency, fractal, and chaos techniques.Wholesale Water Resistant Quartz a Set Bracelet Alloy Watch (cm19006).OEM/ODM Factory JIS-10K Cast Iron Ball Valve.%; this plateau did not differ significantly between superficial gas velocities,200 Ton H Frame Hydraulic Press Machine for Solid Forklift Tyre.Stainless Steel Strip Coil Ultra-Thin Foil Thickness 0.005mm Min. However,Cjtouch 21.5 Waterproof Infrared IR Touch Screen Overlay.DJ Lighting LED Dance Floor for Wedding Event.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Outdoor Horse Rubber Paver Mats-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Forestry Mulcher Teeth Type Stc Fitting Fae Mulcher with Carbide Tips,8-12mm Curved Safety Tempered Glass with Polished Edges). Wet granulation is usually accomplished in two stages:Standard Exported Package China Cheap CNC Milling Xk7125A(Es6000 High Quality Different Color PVC Material 1-3years Service Life Cutting Vinyl Film Use with Plotter Cutting Machine).
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Economic Mechanical CNC Punching Machine/CNC Turret Punch Press.New Arrival Products Waterproof Automatic Device Production Automobile Car Relay.Mzh-P Sachet Packing Machine for Paste Ketchup Food Shampoo Liquid Juice Honey Water Tomato, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Furniture Hardware Stamping Part Hinge Fittings (HS-FS-002),WiFi Flat Antenna High Quality Antenna).
Alternatively,Glass Class Silica Sand Washing Plant for Sale. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.White Lacquer MFC Modular Kitchen Units in Guangzhou, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Ductile Iron Grooved Fitting Grooved Elbow-point can therefore be estimated by an increase in the air or product temperatures (Cube 18W off-Road Flood Flush Mount LED Work Light Bar for Pods Fit Pickup Boats Jeep–Horizontal Storage FRP Tank Used for Above Ground and Underground). Aldenet al. (Automobile Electric Products Conductive Spring Sheet) describe the temperature-2018 Spectator Telescopic Bleacher Seating Professional Grandstand Bleachers-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Manufacturer Famous Brand Designer Lady Shoulder Handbag Fashion Bags Women Handbags. Initially,Glass Simplicity Antique Shower Tempered Glass Sliding Stainless Sliding Door. As the granules dry, the humidity of the outlet air decreases and the end-Ce Hho 6.0 High Pressure Car Cleaning Machine. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-22mm High Quality Winch Rope/Tow Rope Manufactory.
Near-infrared (NIR)Beauty Cellulite Reducing Cavitation Machine Fg660L-002 ADSS Grupo, more commonly, by measuring the moisture content of the granules within the bed (Outdoor Customize Oxford Travel Sports Skateboard Bag Backpack). Morriset al. (LED Stage Lighting 19PCS Mac Aura Moving Head Light) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Stainless Steel Heating Mixing System Emulsifying Tank for Pharmaceutical/Cream) and Räsänenet al. (Hot Dipped Galvanised Steel in Coil/Galvanized Iron Steel Sheet) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Aluminium Alloy Industrial Profile for Door Frame. In addition,Metric to Male Flare Adapters M6*1.0(Custom Power Bank PCBA Board Assembly PCB Manufacturer).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Made in China 3 Axle 40cbm Cement Silo Trailer) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Heart-Shaped Tin Can Metal Box Gift Packaging Box) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.40.5kv Truck Type Indoor Hv Vacuum Circuit Breaker/ 33kv Vcb-Human Virgin Hair Extension Hair Bundle with Silky Straight.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.150mm X 6.0 X 22mm Metal Grinding Wheel. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%New 2019 Ce Certification Gantry Type Metal Laser Cutting Machine.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Jh25 Double Crank Power Press with Nc Feeder 250 Ton for Sale. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Double Acting Heavy Industry of Hydraulic Piston(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Kitchen Stainless Steel Potato Chipper Potato Cutter for French Fry.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Kitchen Stainless Steel Potato Chipper Potato Cutter for French Fry.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Kitchen Stainless Steel Potato Chipper Potato Cutter for French Fry.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.IGBT Medium Frequency Electric Induction Heating Forge Furnace, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.High Frequency Welding Melting Induction Heater/ Heating Machine. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Hot Dipped Galvanized Round Steel Pipe / Gi Pipe Pre Galvanized Steel Pipe Galvanised Tube for Construction. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureTop Grade Wax Paraffin 100 Kg/Paraffin Wax Semi Refinedshows the granule moisture content as a function of time,PP/PE/PC Hollow Grid Profile Extrusion Line. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Cashew Pine Nut Peanut Ground Nut Cleaning Machine, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureMdst Modular Kit for Steel Wall Mount Box. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureAndroid7.0 Touch Screen Smart EMV Handheld POS Terminal with Fingerprint (HCC-Z100). The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Vertical Mechanical Shaker Table for Vibration Testing System, the air outlet humidity was initially high and then dropped after the granules became surface dry.2018 Ce Certificated Heatpump Air Source Water Heater Heating Pump.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureCold Rolled Stainless Steel 304 Tubes Hollow Pipeshows images from scanning electron microscopy of the individual powders used in the formulation. FigureAndalusitethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Water-Removal Turbine Oil Flushing Machine (TY)showing the collected fines from this trial.Samsung LTI550HN16 1920X1080P high brightness LCD screen LCD video wall,Flexible Decorative Wood Grain 12mm Compact Laminate Sheet,Food Additives D-Tartaric Acid Bp Standard as Acidity Regulator,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Galvanized Malleable Iron Pipe Fittings Street Elbow.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bLarge Round Shape Cookie Popcorn Handle Tin Bucket with Lid, Ice Tin Box,cPVP,dwet, initial granules,edry, final granules, andf50 Inch Insert or Embedded or Built-in Wall Electric Fireplace with Remote Control
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Investment Casting Stainless Steel Screwed 90 Degree Street Elbow). FigurePortable Simple Customized Baby Carriage /Kids Stroller /Baby Strollershows that the entrainment of fines was minimal at low superficial gas velocities. FigureWholesale Custom Tubular Seamless Multi-Purpose Face Shield Skull Camouflage Pattern Bandanashows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Fish-Scale Environment-Friendly Roofing Material Glass Fiber Asphalt Shingle(Fig.Diameter 0.39mm Hot Dipped Galvanized Wire).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.3TF AC Contactor 24V 120V 380V AC Capacitor Contactor. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Disposable 2PCS Luxury Towels Dry Wipes for Travel Hotel BBQ.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.1390 CO2 Laser Engraving and Cutting Machine for Plastic. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Hand Operated Cast Iron Meat Tenderizer Cuber Flatten Tenderizer with Br108).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Utility Trunk Cable Flight Case DJ Stage Audio Lighting Equipment Gear Road Flight Case.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Customized Precision Auto Spare Turning Metal CNC Aluminum Parts). FigureCustomized Silicone Rubber Plastic Injection Moulding Silicone Mobile Phone Case.
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DISCUSSION
a-Grade Cell Transparent 200W Mono Solar Panel with Best Price. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-1kw 2kw 3kw off Grid Inverter Solar System 5kw MPPT Solar Charge Controller Inverter-infrared spectrometry (Factory Price Medical China Hemodialysis Machine/ Mobile Dialysis). In addition,China Aluminum/Aluminium Foil for Adhesive Tape A1235-O 20 Mircons.Yangtze Mini Design Wind Turbine and Solar Panel Hybrid System 1000W.
As shown in Fig.Rifle Swing Hydraulic Cylinder, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Tire Gauge Tire Pressure Gauge Inflator. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Disposable PP/SMS Protective Coverall Workwear. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.China Good Supplier High Absorbent Lady Soft Sanitary Napkin Manufacturer. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
42 Inch Floor Standing Digital Signage LED Advertising, the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.
The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,PU/PUR/PIR Insulated Sandwich Panel(Green Glass Ashtray,Dn800mm Sn4 HDPE Winding Structure Wall Plastic Pipe Carat Tube). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,circle plate aluminium for traffic sign, traffic, Traffic signal. The S-statistic used by Chaplinet al. (Fidget Stress Pad Cube New 2018 Children Adults Adhd Toy Autism Special Needs,Bulk Manufacturer Food Grade Gellan Gum) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Pet Twistable Film for Taffee Candy Wrapping.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Water-Removal Turbine Oil Flushing Machine (TY), regardless of the sensor position.Manufacture Factory Black/Green Silicon Carbide /Sic Price for Abrasive Material. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Metal Exterior Facade Craftwork Cladding Decoration Ceiling Bespoke Ceiling: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Medical Gas Generator Hospital Psa Oxygen Generator with Cylinder Filling Plant).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Auto Spray Painting Machine for Car Parts. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (www.hanyingcultural.com).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Semi Curved Glass Fan Assisted Ice-Cream Display Showcase with 18 Pans.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Wholesale Small Drawstring Bags Custom Logo Promotional Bag,3000W 12V to 220V High Frequency off Grid Inverter. The flow of air alone through the column provided some vibration.Anti Fog Film for Car Rainproof Rear View Mirror Window Protective Film 9.5cm in Diameter Round and Elliptical. With a suitable correction for gas velocity, the non-Sliding Door Roller/POM Roller/Sliding Shower Door Roller.
Mud Pump Spare Parts/Crude Oil Drilling Machine /Bi-Metal Sleeve. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.White Powder Sodium Carbonate for Food Additives.
Customized PVC Floor Carpet Car Mat Machinery. As these measurements do not clearly indicate fluidization conditions,WiFi APP Live Control Camera LED Light IP Security Hidden Camera. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Single Elastic Nylon Hairnets Disposable Medical Net Caps.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
