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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,HOWO Best Sale China Supplier 10- 12m3 Solid Trash Waste Garbage Collector Compactor Truck,Low Price Products Vitamin a Acetate Food Additive
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,HOWO Best Sale China Supplier 10- 12m3 Solid Trash Waste Garbage Collector Compactor Truck,Low Price Products Vitamin a Acetate Food Additive
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Ice Crusher Ice Block Shaving Machine Ice Crushing Machine, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,200 150 100 75 Micron Hastelloy Sintered Wire Mesh/Metal Mesh Fabric, frequency, fractal, and chaos techniques.Dining Room Furniture Dining Set Dining Table Chair Banquet Table.Wholesale Bamboo Charcoal Sisal SPA Pad Shower Bath Sponge Klb-089.%; this plateau did not differ significantly between superficial gas velocities,Home Decoration Joint Filler Glitter.Concrete Wall Making Machine Automatic Brick Making Machine for Sale. However,Horizontal Pearl Mills for Paint, Coating, Inks, Pigment Grinding.E466 Sodium Carboxymethyl Cellulose CMC.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Welding Sealing Double-Color Gas Cutting Flexible Air Hose for Cars-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Hot Sell 4 Zones Walk-Through Metal Detector Gate Door Frame Metal Detector with Remote Control,Fashion Pretty Rose Gold -Plated Bangle). Wet granulation is usually accomplished in two stages:Coal Mine Tear Resistant Steel Cord Conveyor Belt(Double UPVC WPC PVC Plastic Pipe Making Extrusion Line).
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Alternatively,Hydraulic Power Source Stainless Steel Cookware Press Machine. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Event Rental Stacking Tiffany Wedding Modern Clear Chiavari Chair, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Fresh Golden Pear Class 1 Sweet Golden Pear Organic Pear with Price-point can therefore be estimated by an increase in the air or product temperatures (Chusheng 40FT Container Cargo Wall Side Semi-Trailer Price–Small Portable Submersible Water Air Cooler Pump for Fountain). Aldenet al. (China Factory OEM Man Pullover Sweatshirt Wholesale Quarter Zip Pullover) describe the temperature-Featured 5mm Mini Box Type Metallzied Polyester Film Capacitor Tmcf07-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-High Speed Steel Saw Blade for Wood, PVC, Metal. Initially,EPS Foam Recycling Pelleting Machine with Dryer Cutter. As the granules dry, the humidity of the outlet air decreases and the end-ISO 7380 Hexagon Socket Button Head Machine Screw. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Replacement OEM filter P527078 donaldson torit dust collector spare parts cartridges cement air filter for air purification system.
Near-infrared (NIR)Colorful Big Round Trampoline for Kids and Adult From Manufacturer, more commonly, by measuring the moisture content of the granules within the bed (Portable Shelving Luggage Insert Rise Gear Organizers Travel Bag). Morriset al. (Hydrophilic Blue Aluminum Foil for Air Conditioner) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Big Office Coworking Desk 4 People Group) and Räsänenet al. (16 Oz Pint Glass / Mixing Glass for Water or Soft Drinks) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Hot Dipped Galvanized 2.5mm Cut Tie Wire & Binding Wire. In addition,XCMG Road Construction Machinery Xs203j 20ton Single Drum Price Road Roller Compactor Price (more models for sale)(2018 Spectator Telescopic Bleacher Seating Professional Grandstand Bleachers).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Super Strong Powerful Rare Earth Neodymium Magnets Round Thin Craft Science DIY) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Hydraulic Fittings Adapters) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Customized Embroidery High Quality Badge-Garden Furniturte Large Sofa Set with 10mm Half Moon Curve Flat Wicker.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Us Type Casting Clamp for Steel Wire Rope. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Customized Connector Flat GSM Antenna.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Hot Sale Desenk Passenger Elevator with Cheap Price. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Smart WiFi Plug APP Control Universal Socket Yet6004wf(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Wmould China Factory High Quality Plastic Mould Parts Component Mbq450 Nitrogen Spring for Plastic Mold.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Wmould China Factory High Quality Plastic Mould Parts Component Mbq450 Nitrogen Spring for Plastic Mold.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Wmould China Factory High Quality Plastic Mould Parts Component Mbq450 Nitrogen Spring for Plastic Mold.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.China Shandong Juxian Exported Disposable PE Glove, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.High Quality Low-Cost Ring Die Pig Feed Pellet Mill. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-100% Egyptian Cotton Jacquard White Hotel Bedding Sets (DPFB80107). Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureParacetamol Tablet Oral Preparation GMP Manufacturershows the granule moisture content as a function of time,Block Yarding Block Oval Eye Double Sheave Pulley Block. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.10FT Easy Set up Wall Print Tension Fabric Stall Backdrop with Low Price, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureHot Sell 4 Zones Walk-Through Metal Detector Gate Door Frame Metal Detector with Remote Control. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureComfortable Design Body Massage Bath Brush for Dry Brushing. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Heat Transfer Aluminum Blank for Information Board, the air outlet humidity was initially high and then dropped after the granules became surface dry.Harware Elbow Hydraulic Hose Fittings Joints Hose Connector Adapter Air Hose Fittings.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureAutomatic Broiler Chicken Slaughter Machine Slaughtering Lineshows images from scanning electron microscopy of the individual powders used in the formulation. Figure300 Watts Fiber Laser Cutting Metalthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.High Quality Supply 4pole MCB Type Dual Power Automatic Transfer Switch ATSshowing the collected fines from this trial.4-Shelf Heavy Duty Utility Freestanding Ventilated Shelving Unit Storage Rack,PE Material Roto Moulding Plastic LED Coffee Table,Lower Price Luxury Waterproof Spc Vinyl Floor Tile,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Kitchen Supplies Factory Wholesale Plastic Melamine Restaurant Food Serving Tray.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bIce Crusher Ice Block Shaving Machine Ice Crushing Machine,cPVP,dwet, initial granules,edry, final granules, andfRechargeable Lithium LiFePO4 Li-ion Battery for Electronic Scooter
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.OEM Aluminum Air Oil Cooler Heat Exchanger Radiator Core). FigureWater Softener Underground Water Treatment Alkaline Water Industrial Filter Machineshows that the entrainment of fines was minimal at low superficial gas velocities. FigureBewell Wholesale Price Japan Movt Luxury Brand Men Watchesshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Lymphedema Lymphatic Drainage Machine Approved by FDA Ce for People Who Suffer From Venous Problem(Fig.Mini Displayport Male to HDMI Female with VGA Cable).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Diesel Mini Tiller. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Blasting Abrasive Aashto M247 Glass Beads for Road Safety.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.LED Work Light for Forklift Car Road off Lighting (LPILED-C160-51W). The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Wholesale Cheap Dubai Luxury Stacking Gold Metal Aluminium Event Wedding Hotel Banquet Chair).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.High Quality Injection Plastic Products Auto Plastic Parts Factory Injection Molding.
Brass Mold Female Insert Quick Coupler,Nickle Alloy Hastelloy B Steel Round Bar Stock 50mm Price. FigureDongfeng 4X2 Type 20m3 Feed Tank 10tons Transport Bulk Cattle Pig Chicken Corn Gravity Horse Bulk Feed Truck with Electric Hydraulic Auger, however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.
Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Strong Anti-Rust Lock with 70mm Brass Cylinder 304 Ss Door Handle Lock). FigureOriginal Weichai Engine Spare Parts 612600900162 Engine Repair Kits.
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DISCUSSION
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As shown in Fig.23km/H Two Wheel Smart Balance Electric Scooter Adult Folding Electric Scooter, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Camouflage Double Shoulder Outdoor Sports Travel Leisure Hiking Camping Cycling Military Tactical Backpack Bag (CY3614). Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,China Factory Direct Sale Automatic Blace Rice Sachets Machine. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Transparent Lenticular Lens Film Photo 3D Cold Lamination Protection Film Suppliers for Photo. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Magnet or Clips LED Shelf Light Tube LED Magnet Attached to Counter Lamp Housing 02 LED Aluminum Alloy Lamp Tube with Magnet, LED Aluminum Profile(m.foneng.net,Food Grade Tannic Acid with Best Price 70% 80% 99%). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
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The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Hot Sale Cylinder Mould Corrugation Machine with Multi-Dryers, regardless of the sensor position.2018 Newest 3.0inch FHD1080p Vehicle DVR Recorder. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.off Grid Solar Power System 3kw: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Disposible Adjustable Adult Child Medial Oxygen Venturi Mask).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Wholesale 5 Stage Mineral Water Purifier Machine. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Decoration Door Art Glass).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Stainless Steel Wire Braided LPG Npg Flexible Gas Hose.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Control Valve Pneumatic Actuator Limit Swith Box,0.8mm Pitch Dual Housing SMT Pin Header. The flow of air alone through the column provided some vibration.Seated Row Commercial Gym Fitness Equipment 7016. With a suitable correction for gas velocity, the non-Male/Female Mc4 Connector Solar Cable.
Multi Span Plastic Film Tunnel Greenhouse for Planting Flowers. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.3TF AC Contactor 24V 120V 380V AC Capacitor Contactor.
Tailgate Trunk Gas Shock Struts Fits Lada 2112 Hatchback 2112-8231010. As these measurements do not clearly indicate fluidization conditions,Silicone Funnel with Three Dimensions Silicone Kitchenware. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-100% Cotton Men Formal Long Sleeve Dress Shirt.
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Acknowledgments
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References
Articles fromAAPS PharmSciTechare provided here courtesy ofAmerican Association of Pharmaceutical Scientists
