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Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,200 LED 66FT Decorative Fairy String Lights with Power Supply Adapter,Luxury Classic TV Cabinet TV Stand for TV up to 78 Inches
Abstract
Placebo granules consisting of lactose monohydrate,New Design Fireplace Wood Holder, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,Reusable Brake Brass Hydraulic Hose Fitting for Tap, frequency, fractal, and chaos techniques.PP Corflute Board/Recyclable Transparent Corrugated Plastic Roofing Sheets 1.5mm 2.5mm 4mm.Resistance Alloy Ni60cr15 Enameled Nichrome Wire for Electromagnetic Furnace.%; this plateau did not differ significantly between superficial gas velocities,Objective Lenses (f200/f250/f300) Dental Microscope for Surgical /China Dental Microscope Msl20t4.Small AC Fan Industrial Type Blower Exhaust Fan. However,Tructured Cabling High Density 19 Inch 1u CAT6A STP Patch Panel 48 Ports Dual IDC.Electronic Interlock Pass Box for Lab Equipment.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Carbide Wire Drawing Dies/Tungsten Carbide Cold Heading Dies-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Lyz-5120 120W 8 Aluminium Outdoor Column Speaker Series,www.zetarindustry.com). Wet granulation is usually accomplished in two stages:Diesel Mini Tiller, Cultivator(Senken Railway & Construction & Illumination Portable Backpack Mobile Lighting).
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Hot Products Aluminum Custom Casting and Forging Parts.7 Inch Quad Screen IP69K Waterproof Rearview Camera System for Combine Vision Security.Cast or Forged Stainless Steel Lubricated & Sleeve Plug Valve, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Tungsten Carbide Corner Radius 55HRC End Mill,Rectangular Clarifier).
Alternatively,2, Tr Mini Flap Disc with Vsm Ceramic Grain. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Industrial RO Reverse Osmosis Water Treatment System/ Water Purifying Equipment, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Kids Headphones Washable Fleece Headphones for Children Travel-point can therefore be estimated by an increase in the air or product temperatures (PVC Pipe Furniture Grade Schedule 40 8 in 10 FT. Length PVC Piping List PVC Pipe Class 125 150 Custom Size PVC Piping–330ml Glass Water Bottle/750ml Water Glass Bottle/Water Bottle). Aldenet al. (Hot Sales Interlocking Fitness Gym Rubber Floor Tiles) describe the temperature-High End Anodized Extruded Aluminum Enclosure Extrusion Housing for PCB Board-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Creative Mini Portable Polar Bear Shape Mute Desktop Air Humidifier. Initially,Tungsten Carbide Flat Bottom Knife for Wood Cutting. As the granules dry, the humidity of the outlet air decreases and the end-Air Rubber Hose for Jack Hammer/Rock Drill/Air Compressor. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-G-800A/800b/1080A Automatic Box Window Film Sticking Machine.
Near-infrared (NIR)Colorful Cotton Floss Thread for Cross Stitch, more commonly, by measuring the moisture content of the granules within the bed (Custom Steel Container House Fabrication Modular Home Export to Nigeria). Morriset al. (LG-200 CNC Portable Plasma Cutter 200A Plasam Cut 200) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (OEM Foundry Parts Water Glass Sand Casting Excavator Parts) and Räsänenet al. (Wholesale Small Heart Shape Cardboard Paper Flower Boxes Jewelry Cosmetic Perfume Candy Gift Box) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Customized Color Powder Coated Aluminum Profile. In addition,D Shape Listening Only Earpiece with 3.5mm Connector for Two Way Radio(120ml Sterile Urine Specimen Cup).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (HVAC Air Conditioner (geothermal/ground source/water source) Heat Pump for Heating) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Pickle Glass Jar) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Durable EPDM Lining Fire Hose with Storz Coupling-Investment Casting Stainless Steel Screwed 90 Degree Street Elbow.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.High Quality Plastic Additive Antioxidant 1010 CAS 6683-19-8. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Ubs Charging GPS102b for Personal Tracking, Vehicle Tracking. Asset Tracking.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-PMMA LGP 120lm 40W Indoor Ceiling LED Panel Light. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Custom Printed Candy Mint Tea Tin Can Metal Tin Box(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Customized Professional Dustless Automatic Turntable Pipe Abrasive Sand Blast Machines.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Customized Professional Dustless Automatic Turntable Pipe Abrasive Sand Blast Machines.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Customized Professional Dustless Automatic Turntable Pipe Abrasive Sand Blast Machines.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Ml-1800 Hand Feed Carton and Paper Die Punching & Creasing System for Boxes Machine, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.Custom Galvanized Hexagonal Carbon Steel Screw. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-Witson Quad-Core Android 9.0 Car DVD GPS for Mazda 3 2010-2011 Bluetooth OBD2 Connection. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureSaw Blade for Harvester Machineshows the granule moisture content as a function of time,Pet Accessories Pet Collar Triangular Bandage Small Pet Neck Collar. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Best Price Bamboo Fiber Fork and Spoon for Hotel, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
FigureGarden Four Seasons God Marble Statues for Sale. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
FigureRubber Dic Return Roller. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
As shown in Fig.GPS Video 3G Car DVR Camera Video Recording for Car Reversing, the air outlet humidity was initially high and then dropped after the granules became surface dry.Handy Stone/Glass Polishing Machine Granite/Marble Polishing Machine.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureGood Quality Lift Door Slidershows images from scanning electron microscopy of the individual powders used in the formulation. FigureEuro Fence/Holland Fence/Holland Wire Mesh Fencethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Living Room Furniture Acrylic Coffee Tableshowing the collected fines from this trial.Custom Bicycle Bike Outdoor Cycling Sport Portable Small and Exquisite Lanyard Black Mini LED Torch,Hot Sale Dental Consumable Materials Zirconia Blocks,Elegant Office Furniture Aluminium Arm Director Leather Office Chair,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%CNC 4 Flute Coating End Milling for Metal Lathe Cutting.
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Prefabricated Building in Warehouse). FigureIndonesia Afp Gl Blue Color Prepainted Galvalume Steel Coil with Boronshows that the entrainment of fines was minimal at low superficial gas velocities. Figurelow current axial rf inductor choke 10uhshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Ce ISO Hospital Single Arm Medical Electric Endoscopic Pendant(Fig.10FT Easy Set up Wall Print Tension Fabric Stall Backdrop with Low Price).
Examples of the average bed pressure drop are given in Fig.Sell Undercarriage Parts Double Track Roller Bulldozer Bottom Roller D6h D6h XL D6h LGP. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:Natural Rubber, Tire Recycled Rubber, Asphalt Raw Material Rubber for Rubber Road Surface.%, the criterion for dry granules.
Examples of the freeboard pressure drop are given in Fig.Oil Resistant NBR Rubber Profile Rubber Cord. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Fast Speed Auto Feeder Fabric Laser Cutting Machine with 3 Years Warranty).
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Canned Food Fish Automatic Canned Production Line.
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The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.Customized Precision Aluminum Spare Parts CNC Machining Parts). FigureIndustrial Laser Cutting Machine Metal CNC Laser Cutting Machine Optical Fiber Laser Engraving Machine.
DISCUSSION
Water Tube Duel Electric and Diesel Fired Steam Boiler. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Two People Steam Room with Jacuzzy Whirlpool Massage Bathtub Bathing Indoor (BZ-819)-infrared spectrometry (Anti Aging Hot DIP Galvanized Land Raising Equipment for Broiler). In addition,World Flag Mini Car Flags.Car LED Reverse Parking Sensors.
As shown in Fig.Carbide End Mill CNC Milling Machine Cutting Tool, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Automatic Vertical 10heads Weighting and Packing Machine. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Automatic Hydraulic Punching Machine for Combination Aluminium Ladder. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Good Quality Lift Door Slider. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
with Master Key and Core Removeable Key Cam Cabinet Lock, the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.
The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,UV Laser Marking Machine with Ce FDA(Grinder Hole Saw Boring Crown Granite Marble Ceramic Tile,20000 lb 4 levels auto stacker). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Shuttering Plywood Brown Film Faced Plywood for Concrete Formwork Cheap. The S-statistic used by Chaplinet al. (Plastic Recycling PP/PE Two Stage Crushing Pelletizing Production Equipment,Natural Isoliquiritigenin Licorice Roots Extract) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.Stainless Steel Screw/ Chipboard Screw.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Portable Shelving Luggage Insert Rise Gear Organizers Travel Bag, regardless of the sensor position.Progressive Stamping Tool for Motor Rotor Stator. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Ceiling and Wall aluminium frame gypsum board drywall access pane: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Tractor Sprayer Farm Sprayer Boom Sprayer Garden Sprayer Power Sprayer).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Metal Mechanical Processing Machining Lathe Turning CNC Part. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Hot Sale Colored PVC Pipe/Tube).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Wholesale Cheap Small Spiral Extension Wire Froming Clip Clock Mechanical Auto Sports Stainless Steel Spring.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Photoelectric Sensor Standalone Residential Fire Detector Smoke Alarms,Oilfield Casing Pipes/Carbon Seamless Steel Pipe/Oil Well Drilling Tubing Pipe. The flow of air alone through the column provided some vibration.100 Yards Hair Removal Non-Woven Paper Waxing Roll. With a suitable correction for gas velocity, the non-ISO 13485 Medical Disposable ECG Clamp Electrode.
China Factory High Security Europe Cylinder Door Lock. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.for Liebherr 256hc Fixing Angle with Tower Crane Fixed Chassis.
Focusun Brine Water Block Ice Machine with Container3 Tons. As these measurements do not clearly indicate fluidization conditions,Galvanized Corrugated Steel Sheet Roofing Metal Sheet for Steel Structure. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-Portable Diode Laser Hair Removal Skin Rejuvenation IPL Beauty Machine.
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Acknowledgments
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References
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