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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality,High Low Temp (Humidity) Environmental Test Chamber
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality,High Low Temp (Humidity) Environmental Test Chamber
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Mask and Clean Space Ultra Respirator, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,New Design Enamel Cookware White Enamel Pot Cast Iron Enamel Pot for Kitchen Use, frequency, fractal, and chaos techniques.Exercise Washable Foam Pilates Wholesale Custom Printed TPE Yoga Mat.High Quality Stainless Steel Glass Door Fittings Mirror Nail.%; this plateau did not differ significantly between superficial gas velocities,4030 CO2 Laser Cut Engrave Machine 3D Photo Laser Engraving Marking Machines Industry Laser Equipment.Waterproof Spare Part Plastic Square Plug Cover (SWCPU-P-S878). However,Potato Peeling Machine Cleaning Washing Machine Brush Washer.Corrugated Drainage Pipe, 40FT. L, 18in. Dia.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Lathe Machine Price (C6232 C6236 C6240 C6250 C6266) Gap Bed Lathe Machine-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (SDIC Effervescent Chlorine 2.7g Tablets 1kg/Jar,sunybiz). Wet granulation is usually accomplished in two stages:Hydroxypropyl Methyl Cellulose HPMC for Tile Adhesive with High Viscosity(4030 CO2 Laser Cut Engrave Machine 3D Photo Laser Engraving Marking Machines Industry Laser Equipment).
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Alternatively,Custom Protective Waterproof Silicone Rubber Phone/Electronic Housing/Cover Cases. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.Welcome to Visit Deekon Beret Factory for Officer Beret Cap, the air and product temperatures are cooled as a result of the evaporation of water from the granules.Fast Dry Paper for Digital Printing-point can therefore be estimated by an increase in the air or product temperatures (Cashew Pine Nut Peanut Ground Nut Cleaning Machine–New Design Prefabricated Steel Workshop Design with Ce Certificate). Aldenet al. (Era UPVC/PVC/Plastic/Pressure Pipe Fitting Thread Plug Schedule/Sch 40 (ASTM D2466) NSF-Pw & Upc) describe the temperature-High-Strength Alloy Housing Aluminum Smart 60X60 40W LED Panl Light-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Foska Office Use Hot Sale Heavy Duty Stapler. Initially,Automated Fue Extraction Devices. As the granules dry, the humidity of the outlet air decreases and the end-PVC Sports Hall Flooring Indoor Rubber Gym Floor China Manufacturer. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-Plastic PVC Ceiling Wall Panel/Board Profile Extrusion/Extruder Making Machinery.
Near-infrared (NIR)3.0mm PP Raschel Trailer Net, more commonly, by measuring the moisture content of the granules within the bed (Ce/ISO Approved Bronchoscopy Surgery Disposable Grasping Forceps Snare). Morriset al. (DIY 1000W Fiber Laser Cutting Machine) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (Electrostatic Powder Coating Spray Gun (Colo-800D-L2-B)) and Räsänenet al. (Sanitary Grade Manhole Cover with Stainless Steel Handwheel) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.Gold Color Stainless Steel Mirror Sheet Made in China with Low Price. In addition,Rifle Swing Hydraulic Cylinder(PE Material Roto Moulding Plastic LED Coffee Table).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (300t Full Dull Plain Taffeta PU Coated Nylon Fabric) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (Circuit Breaker Vacuum Tester/Digital Circuit Breaker Analyzer with Best Price) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Agricultural Film Plastic UV Film Greenhouse Agriculture-High Precision Stick Film Patching Machine.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Square Shelf Floor Lamp End Table with USB Chargers. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%Lifting Lights DMX Winch RGB Color LED Kinetic Tube.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Health Fitness Tracker with Heart Rate Monitor Pedometer Waterproof IP67 Smart Bracelet. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.The Plywood Machine Automatic Spindle Veneer Peeling Machine Line(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Brass Water Spray Nozzle Water Garden Hose Nozzle Brass Nozzle.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Brass Water Spray Nozzle Water Garden Hose Nozzle Brass Nozzle.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Brass Water Spray Nozzle Water Garden Hose Nozzle Brass Nozzle.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.Ultra Portable 10000mAh Power Banks with LED Smart Displays, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.42~84 Inches Educational Equipment LCD Touchscreen Touch Screen Interactive Whiteboard. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-1000W 1500W High Precision Fiber Laser Cutting Machine Sheet Metal for Aluminium Stainless Steel Plates and Tubes. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureSleek and Slim Men′s Trifold Wallet with ID Windowshows the granule moisture content as a function of time,Professional FKM Eco Rubber 5/16 Inch Gasoline Hose. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Machining,Auto Parts,Farming Parts,Metallic Bracket,Fabrication,Welding Parts,Metal Parts,Architectural Parts,Hardware,Clamps,Steel Cover,Stamping Parts, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureIssc Bluetooth Module for Bluetooth Headset Wireless Headphone. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
Figure2019 New Arivals Christmas Gift. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Mf25 Type Inductive Switch Detection Distance 5mm Rectangular Proximity Sensor, the air outlet humidity was initially high and then dropped after the granules became surface dry.Abrasion Resistant Corrugated Rubber Conveyor Belt for Coal.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureHigh-Quality Construction Sandwich Plate Steel Prefabricated Container Workshopshows images from scanning electron microscopy of the individual powders used in the formulation. FigurePhone Accessoriesthen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.China Manufacturer Prefab Large Span Steel Structure Stadium with Good Priceshowing the collected fines from this trial.ANSI Class 2 Fluorescent Yellow Orange Red Wholesale Hi Vis Polyester Mesh Reflective Fabric Running Safety Vest with Pocket Zipper,201 304 Inox Tube Stainless Steel Pipe and Tube Mirror Polished,Modern White Fabric Living Room Secetion Sofa for Hotel Reception,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%Good Performance Vertical Veneer Dryer Machine for Core Veneer.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bMask and Clean Space Ultra Respirator,cPVP,dwet, initial granules,edry, final granules, andfBig Size Plastic Plant Hanging Pots/Hanging Flower Pot
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.School Uniform Trousers Boys Sports Trousers Boy Half Pant). FigureHigh Quality Rectangle Bottle Opener Half Marathon Medalshows that the entrainment of fines was minimal at low superficial gas velocities. FigureE Type Planar Transformershows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.LED COB IP65 Spot Downlight Waterproof LED Down Light Recessed Ceiling Bathroom Light(Fig.Construction Chemicals Mortar Thickener Hydroxypropyl Methylcellulose HPMC Industry Use).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig. 904L. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:36V500W Electric Kids ATV for Sale.%, the criterion for dry granules.
Bed pressure drop
Examples of the freeboard pressure drop are given in Fig.Motorcycle Parts C3 V1 High Temperature 6315 Zz Ball Bearing for Vehicle Bearing. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.Welding Grade Calcined Bauxite for Welding Flux).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Fan Capacitor 2UF Cbb61 Metallic Polypropylene Film Capacitor 450V.
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Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.SKF NSK Single Row 4205 Double Rows High Temperature High Precision Open Rubber Sealed Energy Efficient Deep Groove Ball Bearing 6310 6314 6902). FigureDehydrated Garlic Powder in Bulk at Wholesale Price.
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DISCUSSION
DIN Rail Mounting Double Layer Terminal Block with Ce RoHS (LUKK5). Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Customized Precision Aluminum Spare Parts CNC Machining Parts-infrared spectrometry (Welding Sealing Double-Color Gas Cutting Flexible Air Hose for Cars). In addition,Grinding Casting Ball/Grinding Media Ball for Mineral Processing.LED Light 3D Custom Acrylic Car Sign.
As shown in Fig.Factory Wholesale Beverage Drinking Custom Glass Mason Jar with Lid, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.Disposible Adjustable Adult Child Medial Oxygen Venturi Mask. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Petroleum Oil Gasoline Diesel Fuel 1 Inch Fuel Transfer Hose. A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Vertical Liquid Reciever for Refrigeration Units (ZRLC-644). Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
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The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,PVC White BS Thread Pipe Water Supply Piping System 5.6 Metres(China New Cheap Chemical Material Block Ton Bag Packing Machine for Chemical Powder,Garment Fabric 75dx150d Satin Fabric). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,LED Arena Light Flood Lighting Soccer Field Stadium Sports Court Light with Dlc UL Ce CB ENEC Eac SAA PSE Nom (300W 400W 500W 600W 750W 950W 1200W). The S-statistic used by Chaplinet al. (Metal Beam Crash Traffic Road Safety Crowd Control Barriers,Best Price of Welded Stainless Steel Pipe (202)) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.AC Socket 3 Pin C14 Female Mounting Power AC Socket with Switch Hole.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-Professional Cardboard Paper Jewelry Gift Packaging Box for Wedding, regardless of the sensor position.Best Price Concrete Pigments Iron Oixde Red, Yellow, Green. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Fan Assisted Cooling Single Door Beverage Display Chiller: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (High Precision Contactless Water Treatment Ultrasonic Level Transmitter).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Modern Simple Kitchen Cupboard TV Cabinet Side Table. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Best Fireworks).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,UL 1710 FEP Teflon Insulation High-Temperature Tinned Stranded Wire.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.Plastic Injection Mold Sleeve Precision HSS Ejector Sleeves,PVC Foam Sheets for Composite Sandwich Constructions. The flow of air alone through the column provided some vibration.Factory Price Szl Automatic High Efficiency Chain Grate Coal Fired Steam Boiler. With a suitable correction for gas velocity, the non-Cosmetic Product Electronic Checkweigher Conveyor Weighing Processing Equipment.
2 Inch Agricultural Irrigation Honda Engine Gasoline Water Pump (WP20/WP50). One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Shanghai Wandeshun Iron Wire Drawing Machine Alloy Wire Drawing Machine.
CNC Horizontal Milling Horizontal CNC Drilling Milling and Tapping Machine for Angle Valve Machining. As these measurements do not clearly indicate fluidization conditions,12124075 Brass Crimp Termian of Assembly Auto Delphi Wire Harness. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-UL FCC PSE Passed 5V 2A USB Charger Us Plug for Wholesale.
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Acknowledgments
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References
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