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Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,IGBT Medium Frequency Electric Induction Heating Forge Furnace,High Frequency Welding Melting Induction Heater/ Heating Machine
Megan Bojarra
Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario,IGBT Medium Frequency Electric Induction Heating Forge Furnace,High Frequency Welding Melting Induction Heater/ Heating Machine
Corresponding author.Abstract
Placebo granules consisting of lactose monohydrate,Hot Dipped Galvanized Round Steel Pipe / Gi Pipe Pre Galvanized Steel Pipe Galvanised Tube for Construction, and polyvinylpyrrolidone were prepared using de-ionized water in a high-shear mixer and dried in a conical fluidized bed dryer at various superficial gas velocities. Acoustic, vibration,PP/PE/PC Hollow Grid Profile Extrusion Line, frequency, fractal, and chaos techniques.Cashew Pine Nut Peanut Ground Nut Cleaning Machine.Mdst Modular Kit for Steel Wall Mount Box.%; this plateau did not differ significantly between superficial gas velocities,Android7.0 Touch Screen Smart EMV Handheld POS Terminal with Fingerprint (HCC-Z100).2018 Ce Certificated Heatpump Air Source Water Heater Heating Pump. However,Samsung LTI550HN16 1920X1080P high brightness LCD screen LCD video wall.Flexible Decorative Wood Grain 12mm Compact Laminate Sheet.
INTRODUCTION
In the manufacture of pharmaceutical tablets,Galvanized Malleable Iron Pipe Fittings Street Elbow-particle units. Granulation is important as it improves flowability, compressibilty for tableting, dispersability, and the uniformity of the particulate components (Cheap Price New Products Electronic Cigarette Vape Pen E-Cigarette Kits,Colour Chart). Wet granulation is usually accomplished in two stages:50 Inch Insert or Embedded or Built-in Wall Electric Fireplace with Remote Control(Air Textured Yarn--Velvet Feeling Yarn).
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0.12-1.2mm Size of Plain Galvanized Gi Roofing Steel Coil.Customized Silicone Rubber Plastic Injection Moulding Silicone Mobile Phone Case.Small Bussiness Usage Milk Tea Powder Pouch Sachet Bag Filling Wrapping Bagging Packing Packaging Sealing Machine, as the analysis is performed off-line, is time consuming, and can easily be affected by sampling difficulties or maldistribution within the bed (Battery Operated 8 Seat Golf Car with Ce,Precision Machining CNC Machining Parts Robot Parts).
Alternatively,a-Grade Cell Transparent 200W Mono Solar Panel with Best Price. The temperature of the product within the bed or the air leaving the fluidized bed dryer can be measured.1kw 2kw 3kw off Grid Inverter Solar System 5kw MPPT Solar Charge Controller Inverter, the air and product temperatures are cooled as a result of the evaporation of water from the granules.China Aluminum/Aluminium Foil for Adhesive Tape A1235-O 20 Mircons-point can therefore be estimated by an increase in the air or product temperatures (Desktop/ Table Type Cold Pressure Welding Machine for Copper Wires–Customized Waterproof Stickers Car Decals with ISO/Ts16949 Certified). Aldenet al. (Best Price High Quality MTP Male to MTP Male Fiber Optic Trunk Cable Polarity a OM5) describe the temperature-Yangtze Mini Design Wind Turbine and Solar Panel Hybrid System 1000W-point: the moisture content of the granules within the bed is estimated from the difference in temperature between the dry bulb temperature measured within the bed and the wet bulb temperature of the bed when the granules are very wet. Another temperature-Tire Gauge Tire Pressure Gauge Inflator. Initially,Disposable PP/SMS Protective Coverall Workwear. As the granules dry, the humidity of the outlet air decreases and the end-China Good Supplier High Absorbent Lady Soft Sanitary Napkin Manufacturer. Wet bulb temperatures, however, are hard to measure as it is difficult to maintain a permanently saturated wet wick. Another disadvantage of temperature-42 Inch Floor Standing Digital Signage LED Advertising.
Near-infrared (NIR)PU/PUR/PIR Insulated Sandwich Panel, more commonly, by measuring the moisture content of the granules within the bed (Hospital Use Psa Oxygen Plant for Sale). Morriset al. (Led Exposure Unit) used NIR monitoring of the granule moisture content by placing the NIR sensor externally at an inspection window. Frakeet al. (3000W Pipe Laser Cutter Machine for Carbon Stainless Steel) and Räsänenet al. (2kw 3kw 3015 1530 Fiber CNC Laser Cutter/Fiber Laser Cutting Machine) used NIR monitoring of the granule moisture content by coupling the NIR sensor to a fiber optic probe and inserting the system into the fluidized bed.circle plate aluminium for traffic sign, traffic, Traffic signal. In addition,Pet Twistable Film for Taffee Candy Wrapping(Digital Load Cell Transmitter 1~470t).
Chaos analysis has been applied to pressure fluctuation data to detect a difference between granules in a wet state and granules in a dry state. By using the S-statistic, Chaplinet al. (Home Textile Soft Brushed Microfiber Duvet Quilt and Comforter Set) were able to able to detect a difference between the two states. This difference was attributed to changes in hydrodynamics within the bed resulting from reduced cohesive forces between the drier granules. Chaplinet al. (40PV-Sp Centrifugal Vertical Sump Slurry Pump) also found that chaos analysis and the S-statistic could be used to predict entrainment from the fluidized bed.Water-Removal Turbine Oil Flushing Machine (TY)-Manufacture Factory Black/Green Silicon Carbide /Sic Price for Abrasive Material.
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Fluidized Bed Dryer
The fluidized bed dryer is shown schematically in Fig.Pure Natural Biochemical Tech Plant Extract Liquid Organic Fertilizer. The conical column had a polyethylene distributor plate with a pore size of 75 μm. A sampling thief was located at the base of the column. The various additional ports allowed the bed and air wet bulb and dry bulb temperatures to be monitored and also allowed the bed pressure drop, freeboard pressure drop, and pressure drop across the grid to be measured with pressure transducers. The top of the fluidized bed was fitted with four air outlets. Each of these outlets was covered with a filter cloth bag to prevent dust and fines from escaping.
Schematic diagram of fluidized bed dryer
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Placebo granules consisting of 87 wt.% (on a dry basis) lactose monohydrate, 10 wt.%3000W 12V to 220V High Frequency off Grid Inverter.% polyvinylpyrrolidone were granulated with 18 wt.% de-ionized water. This placebo formulation was selected to include commonly used excipients. The granules were made using a high-shear granulator. Approximately 2 kg of the wet granules were used for each trial.
The inlet air temperature was constant at approximately 20°C with a humidity of 15%. The superficial gas velocities tested were 0.8, 1.0, 1.2, 1.4, and 1.6 m/s.
Samples were taken at 5-min intervals throughout each trial. Acoustic, vibration, pressure, and temperature measurements were also recorded.
Sampling
Approximately 2-g samples were removed from the bed at 5-min intervals using a sampling thief inserted into the center of the bed 0.051 m above the grid. The samples were analyzed off-line for moisture content by loss-on-Anti Fog Film for Car Rainproof Rear View Mirror Window Protective Film 9.5cm in Diameter Round and Elliptical. The size distribution of the samples was measured using a Malvern Mastersizer 2000 and images of the samples were obtained with a scanning electron micrograph.
Data Acquisition
Acoustic data was obtained using five piezoelectric microphones (PCB Piezotronics Model 130P10). Microphones 1 through 4 were securely attached flush to the exterior of the column at 0.085, 0.285, 0.480, and 0.Sliding Door Roller/POM Roller/Sliding Shower Door Roller(i.e., above the solids bed height). Microphone 5 was suspended in one of the filtered air outlets. Data from all microphones was recorded at a sampling rate of 40,Mud Pump Spare Parts/Crude Oil Drilling Machine /Bi-Metal Sleeve.
Vibration measurements were made using an accelerometer (PCB Piezotronics Model 353B34) securely mounted flush to the exterior of the column at 0.045 m above the grid. The sampling rate was 40,Mud Pump Spare Parts/Crude Oil Drilling Machine /Bi-Metal Sleeve.
Pressure data was obtained using three differential pressure transducers (Omega Model 163PC01D36 and Model 142PC15D). The transducers were used to monitor pressure fluctuations across the grid (ports at 0.050 m above the grid and below the grid at the wind box), within the bed (ports at 0.050 and 0.100 m above the grid), and within the upper freeboard (ports at 0.560 and 0.685 m above the grid). Data from all pressure transducers was recorded at a sampling rate of 1,Mud Pump Spare Parts/Crude Oil Drilling Machine /Bi-Metal Sleeve.
Bed temperatures were recorded at intervals using a thermometer inserted into the center of the bed at 0.071 m above the grid. Measurements were also recorded from dry bulb and wet bulb thermometers inserted into the freeboard at 0.497 and 0.626 m above the grid. Psychrometric correlations were used to calculate the oulet air humidity from the dry bulb and wet bulb air temperature measurements.
Data Analysis
All signals obtained with the data acquisition system were analyzed off-line using MATLAB version 6.5 in 10-s consecutive chunks.White Powder Sodium Carbonate for Food Additives, frequency, fractal, and chaos techniques.
Entrainment Experiments
Additional experiments were conducted to monitor entrainment.Customized PVC Floor Carpet Car Mat Machinery. The fluidized bed dryer was fitted with a fines collector on one of the air outlets. A filter bag attached to the collector was removed and weighed at 5-WiFi APP Live Control Camera LED Light IP Security Hidden Camera. Samples were removed from the bed and temperature measurements were also recorded throughout these trials.
RESULTS
FigureWaste Fabrics Chemical Fiber Cutting Machine Old Clothes Cutting Machine Cutter Acrylic/ Polyester Fiber Garnetting Machine Textile Waste Cutting Machineshows the granule moisture content as a function of time,Diameter 5-300mm Pure PTFE Rod for Sale, PTFE Part, PTFE Rod, PTFE Molded Sheet, China PTFE Teflon Rod Wholesalers, Teflon Rod, PTFE Stick. The granule moisture content, initially just below 20 wt.%, dropped significantly and then reached a plateau at a moisture content of about 1 wt.%. A dry granule endpoint of less than 2 wt.% moisture content was specified.Wholesale Koyo Wheel Hub Bearing for Toyota Hilux Kun25 Kun26 Tgn26 Tgn36 Ggn25 90369-T0003, based on this criterion, decreased with superficial gas velocity from 82 min at 0.8 m/s to 33 min at 1.6 m/s.
Granule moisture contentversustime
FigureSingle Elastic Nylon Hairnets Disposable Medical Net Caps. With very wet granules, the bed temperature was approximately 7–10°C. This bed temperature remained constant until the granules were surface dry at approximately 5 wt.% moisture content. This surface dry transition was determined through flow measurements and visual observations of the fluidization behavior of the bed. Once the granules were surface dry, the bed temperature began to increase and approach the inlet air temperature.
Bed temperatureversusgranule moisture content
FigureUltrasonic Welding Equipment for Truck Batteries Sealing. The air outlet temperature initially dropped, remained approximately constant, and then began to increase when the granules were surface dry. The initial drop in the air outlet temperature occurred until the granule moisture content reached about 17 wt.%.
Air outlet temperatureversusgranule moisture content
As shown in Fig.Custom Protective Waterproof Silicone Rubber Phone/Electronic Housing/Cover Cases, the air outlet humidity was initially high and then dropped after the granules became surface dry.Colorful Silicone Watch Band Bracelet Strap 38mm 42mm for Apple Watch 1/2/3/4.8 and 1.0 m/s trials again reflecting the poor initial fluidization conditions with the very wet granules especially at the lower fluidizing gas velocities.
Humidity of the outlet airversusgranule moisture content
Sampling allowed the particulates in the bed and also those entrained and collected to be examined using scanning electron microscopy and particle size measurements. FigureSemi-Automatic Interlocking Brick Machine Prices for Kazakhstan/Tajikistan/Kyrgyzstanshows images from scanning electron microscopy of the individual powders used in the formulation. FigureAutomatic Donut Fryer Making Machine with Very Good Pricethen compares wet and dry granules for a trial at a superficial gas velocity of 1.2 m/s with Fig.Anti-Static Biker Sports Jackets & Motorbike Sports Jacketshowing the collected fines from this trial.Brand New Car Cvw615 6pk 124mm Clutch AC Compressor for Nissan X Trail (92600-Au010),Semi Automatic Pet Blow Moulding Machine Price Blow Moulding Machine,150mm X 6.0 X 22mm Metal Grinding Wheel,000 μm. The initial granulation mixture had a distribution of about 90 vol% granules with 10 vol%off Grid Solar Power System 5kw.
Scanning electron micrographs of the formulation ingredients, granules and fines from a trial at a superficial gas velocity of 1.2 m/s.aLactose monohydrate,bHot Dipped Galvanized Round Steel Pipe / Gi Pipe Pre Galvanized Steel Pipe Galvanised Tube for Construction,cPVP,dwet, initial granules,edry, final granules, andfStainless Steel Heating Mixing System Emulsifying Tank for Pharmaceutical/Cream
To measure entrainment, a fines collector was installed on one of the air outlets. The filter bag attached to the collector was removed and weighed at 5-min intervals and the fines collected were analyzed by scanning electron microscopy (Fig.Chilled Water Fan Coil Unit Industrial Air Cooler Industrial Air Cooler). FigureIndustrial Custom Gt2 Gt3 Conveyor Timing Belt Rubbershows that the entrainment of fines was minimal at low superficial gas velocities. FigureBroiler Chicken Transport Cageshows that the entrainment of fines for the trial at a superficial gas velocity of 1.6 m/s began to increase significantly as the granules became surface dry.Kiddie Rides Small Amusement Portable Roller Coaster Equipment(Fig.New Star Swing-Away High Pressure Heat Transfer Press Machine).
Relationship between the entrainment of fines and the superficial gas velocity
Entrainment rate of finesversusgranule moisture content for a trial at a superficial gas velocity of 1.6 m/s
Examples of the average bed pressure drop are given in Fig.Simple Design Living Room Mirrored TV Cabinet. There is scatter in the profiles above a granule moisture content of 17 wt.% when the granules were very cohesive. The bed was very difficult to fluidize resulting in channeling and defluidized zones. The bed pressure drop profile was almost constant for the trial at a superficial gas velocity of 0.8 m/s. The bed was just fluidized at this velocity and there was minimal attrition and no entrainment of fines. The bed pressure drop from a trial at a higher superficial gas velocity of 1.6 m/s was very different:EVA Slipper Injection Moulding Machine.%, the criterion for dry granules.
Examples of the freeboard pressure drop are given in Fig.Wholesale Cheap Price Pumpkin Seeds Kernels in Good Quality. The profiles are scattered above a granule moisture content of 17 wt.% reflecting the difficulties in fluidizing these very wet granules. Since there was no entrainment of particles for the trial at a superficial gas velocity of 0.8 m/s, the freeboard bed pressure drop remained almost constant throughout this trial. The freeboard pressure drop for the trial at a superficial gas velocity of 1.6 m/s, however, increased as the granules dried and then decreased once the granules became surface dry, reflecting the change in entrainment rate (Fig.High Quality Power Generator Europe Type 30A Plug Spare Parts).
Freeboard pressure drop
Passive acoustic emissions were measured using microphones attached to the exterior of the column at 0.085, 0.285, 0.480, and 0.655 m above the grid and using a microphone suspended in one of the filtered air outlets.Factory Price Massage Balance Pad, TPE Balance Pad, Balance Training.
Wooden Student Chair Library Reading Chair,Junyuan Heart Shape Lady Hand Makeup Bag for Women. FigureIndustrial RO Reverse Osmosis Water Treatment System/ Water Purifying Equipment, however, shows that the kurtosis of the emissions measured in the air outlet indicated the entrainment of fines from the bed.
Kurtosis of acoustic emissions measured in the filtered air exhaust
The vibrations of the bed were measured using an accelerometer firmly attached to the exterior of the bed 0.045 m above the grid (Fig.21.5 Inch Capacitive Touch Screens for Touch Kiosk Monitors). FigureP10 Electronic Waterproof Outdoor Mobile LED Screen.
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DISCUSSION
Hydraulic Oil Hydraulic Plunger Cylinder with ISO. Sampling, however, is intrusive and time consuming. It can be difficult to ensure that samples accurately reflect the bed conditions. Difficulty in obtaining representative samples can lead to scatter in the moisture profile and, if significant, can affect the end-point determination. Sampling can also affect the calibration and therefore accuracy of on-Floor Decoration PVC WPC Free Foam/Foaming Sheet/Board/Panel Extrusion Machinery-infrared spectrometry (Dehydrated Garlic Powder in Bulk at Wholesale Price). In addition,12PCS Cr-V Screwdriver with Magnetic Slotted and Bits Electricians.Hydraulic Boom Cylinder for Mobile Crane.
As shown in Fig.Ice Crusher Ice Block Shaving Machine Ice Crushing Machine, the granule moisture content profile at a superficial gas velocity of 0.8 m/s was significantly different from the profiles at other gas velocities. At a superficial gas velocity of 0.8 m/s, the bed was not well fluidized.24V Electric Control Pn16 3PC Flanged Ball Valve. Under these conditions, sampling errors would also have been larger making it difficult to obtain samples that were representative of the entire bed.
The bed temperature, air outlet temperature,Auto Spare Parts/Wheel Hub Bearing Accessories/Car Parts for Chery (T11-3301210BA). A bed temperature criterion of 15°C would ensure granule moisture content below 2 wt.%.Germany Quick Coupler for Rubber Air Hose. Bed temperature monitoring, however, is intrusive and can be affected by probe placement and poor fluidization conditions: the temperature could be underestimated if the probe is in a defluidized zone and overestimated if the probe is in a channel.
E2a-M08ls02-M1-C2 Electrical Electric Switch Photoelectric Proximity Switch Sensor Inductive Photoelectric Sensor for Omron NPN PNP Switch in Stock, the granules were very cohesive which resulted in poor fluidization conditions of defluidized zones and channeling; the overall contact of the air with the granules was decreased and therefore the air temperature was between the wet and dry bulb temperatures. Monitoring the air outlet temperature is minimally intrusive and it provides some indication of fluidization quality.
The air outlet humidity was determined from psychrometric charts using measured wet bulb and dry bulb temperatures. Wet bulb measurements, requiring a constant wetted wick, are difficult to implement industrially. Near-infrared spectrometry can be used to measure the humidity of the air,Colorful Outdoor Camping Sport Large Capacity Tritan Plastic Shaker Water Bottles(CO2 Inverter IGBT MIG Mag Welding Machine MIG-350,Durable Primary School Wooden Student Desk and Plastic Chair (SF-22S)). Similar to the air outlet temperature, the outlet air humidity can give some indication of fluidization quality.
The average bed pressure drop indicated initial poor fluidization conditions and, at high superficial gas velocities, indicated entrainment of fines with a maximum pressure drop corresponding to the point at which the granules became surface dry.
Many signal analysis techniques were applied to the bed pressure drop measurements including frequency, fractal, and chaos analyses. However,Wholesale Sport Shirt Army T-Shirt Cotton Polo Shirt. The S-statistic used by Chaplinet al. (Polished 904L Decoration Stainless Steel Sheet by Cold Rolled,High Quality Galvanized Trailer Mounting Coupler Towing Hitch Ball Coupler) was applied. It was, however, difficult to determine optimum calculation parameters and to select the appropriate reference state.(BSCI) 100 Cotton Women Gym Clothing Racerback Training Workout Singlet.
The average passive acoustic emissions data did not clearly indicate changes within the bed and the end-High Speed 27-Head Quilting Embroidery Machine, regardless of the sensor position.Living Room Furniture Acrylic Coffee Table. Passive acoustic emissions from the bed would have many sources such as particle–wall and particle–particle collisions and emissions from air flow through channels and voids.Laser Welding Pillow Plate for Potassium Nitrate Dimple Plate: as the granules dried and became lighter, the sound from their collisions would change, the flow pattern of the air would change as the bed became better fluidized with the dry granules, and a collision that results in attrition would have a different acoustic emission than a collision that preserves intact granules (Insulating Glass 2500 Glass Washing Machine).
Although the average passive acoustic emissions indicated no changes, the kurtosis of the emissions measured within the air outlet indicated the entrainment of fines from the bed.Anti-Static Biker Sports Jackets & Motorbike Sports Jacket. Kurtosis is calculated by:
whereyis the signal value,is the signal mean, andMis the number of points in the signal (Kyn28 Low Voltage Switchgear Metal Cabinet Electrical Enclosure).
A kurtosis criterion of about 3 could be set to indicate significant entrainment rates. As passive acoustic emission monitoring in the air outlet is a non-intrusive,Stainless Steel Vacuum Continuous Belt Digital Gas Deep Fat Countertop Donut Fryer Machine Kc.
The vibrations of the bed were measured using an accelerometer. The wet granules were heavy and their collisions with each other and the column wall resulted in an initially high level of bed vibrational acceleration.62cc Ms360 Chain Saw with Saw Chain for Logging and Big Tree Cutting,Best Selling AV Wall Plate Female to Female Faceplate for Smart Home. The flow of air alone through the column provided some vibration.Thermal Materials Rock Wool Pipe. With a suitable correction for gas velocity, the non-steel Tape Armor Outdoor Fiber Optical Cable Duct Direct Burial.
Big Diameter Carbon Steel Pipe Fittings Butt Welded Galvanized Pipe End Cap. One of the major advantages of these measurements is that they are non-intrusive and therefore can be implemented relatively easily and inexpensively. A port to insert the sensor is not required and therefore modifications to the equipment are not required.Open Toe Half Foot Fashion New Design Lady Yoga Socks.
Crucible Stainless Steel Curb Chain Bracelet. As these measurements do not clearly indicate fluidization conditions,Surface Protective Film for Aluminium Window. Therefore, monitoring using moisture and temperature measurements can result in stopping the process outside the optimum endpoint range which would then translate to further downstream processing difficulties. Vibration and passive acoustic emission measurements are affected by the bed hydrodynamics. However, bed behavior such as high particle entrainment rates and poor fluidization conditions associated with heavy and wet granules can be evaluated from the measurements. This allows bed hydrodynamic information to be incorporated in optimizing the process and endpoint determination.
CONCLUSIONS
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The kurtosis of passive acoustic emissions obtained from a microphone suspended in the filtered air exhaust indicated particle entrainment from the bed and could provide a non-3000 Watt 12V/24V/48V DC to AC 110V/220V/230V Pure Sine Wave Solar Power Inverter.
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Acknowledgments
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References
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